Selective laser melted equiatomic CoCrFeMnNi high-entropy alloy: Microstructure, anisotropic mechanical response, and multiple strengthening mechanism

One of the major challenges of equiatomic CoCrFeMnNi HEA is to manufacture parts with complex geometry that have higher yield strength. Equiatomic CoCrFeMnNi HEA was successfully fabricated in the present study with selective laser melting. The unique microstructure and mechanical anisotropy that ge...

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Veröffentlicht in:Journal of alloys and compounds 2019-10, Vol.805, p.680-691
Hauptverfasser: Kim, Young-Kyun, Choe, Jungho, Lee, Kee-Ahn
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Choe, Jungho
Lee, Kee-Ahn
description One of the major challenges of equiatomic CoCrFeMnNi HEA is to manufacture parts with complex geometry that have higher yield strength. Equiatomic CoCrFeMnNi HEA was successfully fabricated in the present study with selective laser melting. The unique microstructure and mechanical anisotropy that generally appear in additive manufactured materials were investigated. SLM-built HEA has strongly oriented grains, dislocation networks, and nano-sized oxides. In addition, the average grain sizes were measured as 15.66 μm, 12.93 μm, and 5.98 μm on the plane perpendicular to the scanning direction (SD), transverse direction (TD), and building direction (BD), respectively. A compressive test measured outstanding yield strengths (YS) of 778.4 MPa, 766.4 MPa, and 703.5 MPa in the loading axis of SD, TD, and BD, respectively. These outstanding YSs are the result of a combination of fine grain sizes, high dislocation density and nano-sized oxides. In addition, anisotropy in mechanical properties are result from different values of Taylor factor and grain size according to the loading axis. After a compression test, the geometrically necessary dislocation density was found to differ about 2.5 times on each plane parallel to the loading axis in the same macro strain. Based on such findings, the relationship among microstructure, mechanical anisotropy and deformation mechanism are discussed in the present paper. Furthermore, the mechanical properties of SLM-built equiatomic CoCrFeMnNi HEA are predicted by using multiple strengthening mechanisms considering the microstructural characteristics. [Display omitted] •SLM-built HEA shows hierarchical microstructure, dislocation network, and nano-sized oxides.•SLM-built HEA shows outstanding yield strength about ∼778.4 MPa.•Anisotropic mechanical response was observed in SLM-built HEA.•Mechanical properties of SLM-built HEA was predicted by using multiple strengthening mechanism.
doi_str_mv 10.1016/j.jallcom.2019.07.106
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Equiatomic CoCrFeMnNi HEA was successfully fabricated in the present study with selective laser melting. The unique microstructure and mechanical anisotropy that generally appear in additive manufactured materials were investigated. SLM-built HEA has strongly oriented grains, dislocation networks, and nano-sized oxides. In addition, the average grain sizes were measured as 15.66 μm, 12.93 μm, and 5.98 μm on the plane perpendicular to the scanning direction (SD), transverse direction (TD), and building direction (BD), respectively. A compressive test measured outstanding yield strengths (YS) of 778.4 MPa, 766.4 MPa, and 703.5 MPa in the loading axis of SD, TD, and BD, respectively. These outstanding YSs are the result of a combination of fine grain sizes, high dislocation density and nano-sized oxides. In addition, anisotropy in mechanical properties are result from different values of Taylor factor and grain size according to the loading axis. After a compression test, the geometrically necessary dislocation density was found to differ about 2.5 times on each plane parallel to the loading axis in the same macro strain. Based on such findings, the relationship among microstructure, mechanical anisotropy and deformation mechanism are discussed in the present paper. Furthermore, the mechanical properties of SLM-built equiatomic CoCrFeMnNi HEA are predicted by using multiple strengthening mechanisms considering the microstructural characteristics. [Display omitted] •SLM-built HEA shows hierarchical microstructure, dislocation network, and nano-sized oxides.•SLM-built HEA shows outstanding yield strength about ∼778.4 MPa.•Anisotropic mechanical response was observed in SLM-built HEA.•Mechanical properties of SLM-built HEA was predicted by using multiple strengthening mechanism.</description><identifier>ISSN: 0925-8388</identifier><identifier>EISSN: 1873-4669</identifier><identifier>DOI: 10.1016/j.jallcom.2019.07.106</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Anisotropy ; Compression tests ; Deformation mechanisms ; Dislocation density ; Grain size ; High entropy alloys ; High-entropy alloy ; Laser beam melting ; Mechanical analysis ; Mechanical properties ; Microstructure ; Rapid prototyping ; Selective laser melting ; Strain ; Strengthening mechanisms ; Yield strength</subject><ispartof>Journal of alloys and compounds, 2019-10, Vol.805, p.680-691</ispartof><rights>2019</rights><rights>Copyright Elsevier BV Oct 15, 2019</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c403t-baefc07833566fa34aab9d9a1cd841e59f72ae1735b527f5dd2490460da842a73</citedby><cites>FETCH-LOGICAL-c403t-baefc07833566fa34aab9d9a1cd841e59f72ae1735b527f5dd2490460da842a73</cites><orcidid>0000-0002-7463-1759 ; 0000-0003-2149-3871</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0925838819326039$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65534</link.rule.ids></links><search><creatorcontrib>Kim, Young-Kyun</creatorcontrib><creatorcontrib>Choe, Jungho</creatorcontrib><creatorcontrib>Lee, Kee-Ahn</creatorcontrib><title>Selective laser melted equiatomic CoCrFeMnNi high-entropy alloy: Microstructure, anisotropic mechanical response, and multiple strengthening mechanism</title><title>Journal of alloys and compounds</title><description>One of the major challenges of equiatomic CoCrFeMnNi HEA is to manufacture parts with complex geometry that have higher yield strength. Equiatomic CoCrFeMnNi HEA was successfully fabricated in the present study with selective laser melting. The unique microstructure and mechanical anisotropy that generally appear in additive manufactured materials were investigated. SLM-built HEA has strongly oriented grains, dislocation networks, and nano-sized oxides. In addition, the average grain sizes were measured as 15.66 μm, 12.93 μm, and 5.98 μm on the plane perpendicular to the scanning direction (SD), transverse direction (TD), and building direction (BD), respectively. A compressive test measured outstanding yield strengths (YS) of 778.4 MPa, 766.4 MPa, and 703.5 MPa in the loading axis of SD, TD, and BD, respectively. These outstanding YSs are the result of a combination of fine grain sizes, high dislocation density and nano-sized oxides. In addition, anisotropy in mechanical properties are result from different values of Taylor factor and grain size according to the loading axis. After a compression test, the geometrically necessary dislocation density was found to differ about 2.5 times on each plane parallel to the loading axis in the same macro strain. Based on such findings, the relationship among microstructure, mechanical anisotropy and deformation mechanism are discussed in the present paper. Furthermore, the mechanical properties of SLM-built equiatomic CoCrFeMnNi HEA are predicted by using multiple strengthening mechanisms considering the microstructural characteristics. [Display omitted] •SLM-built HEA shows hierarchical microstructure, dislocation network, and nano-sized oxides.•SLM-built HEA shows outstanding yield strength about ∼778.4 MPa.•Anisotropic mechanical response was observed in SLM-built HEA.•Mechanical properties of SLM-built HEA was predicted by using multiple strengthening mechanism.</description><subject>Anisotropy</subject><subject>Compression tests</subject><subject>Deformation mechanisms</subject><subject>Dislocation density</subject><subject>Grain size</subject><subject>High entropy alloys</subject><subject>High-entropy alloy</subject><subject>Laser beam melting</subject><subject>Mechanical analysis</subject><subject>Mechanical properties</subject><subject>Microstructure</subject><subject>Rapid prototyping</subject><subject>Selective laser melting</subject><subject>Strain</subject><subject>Strengthening mechanisms</subject><subject>Yield strength</subject><issn>0925-8388</issn><issn>1873-4669</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><recordid>eNqFkc9qGzEQxkVpoK7TRygIeu060mr_qZdSTJwUkuaQ9CxkadbWopU2kjbgF8nzRo7dc0_DDL9vhm8-hL5SsqKENlfDapDWKj-uSkL5irR53HxAC9q1rKiahn9EC8LLuuhY131Cn2McCMkkowv0-ggWVDIvgK2MEPAINoHG8DwbmfxoFF77ddjAvftj8N7s9gW4FPx0wPmmP_zA90YFH1OYVZoDfMfSmeiPRJaOoPa5V9LiAHHyLr4DGo-zTWaygLMQ3C7twRm3-8fH8RJd9NJG-HKuS_R3c_20vi3uHm5-r3_dFaoiLBVbCb0ibcdY3TS9ZJWUW665pEp3FYWa920pgbas3tZl29dalxUnVUO07KpStmyJvp32TsE_zxCTGPwcXD4pypIznr9H60zVJ-roNAboxRTMKMNBUCKOEYhBnCMQxwgEafO4ybqfJx1kCy8GgojKgFOgTchPF9qb_2x4A1e2loo</recordid><startdate>20191015</startdate><enddate>20191015</enddate><creator>Kim, Young-Kyun</creator><creator>Choe, Jungho</creator><creator>Lee, Kee-Ahn</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><orcidid>https://orcid.org/0000-0002-7463-1759</orcidid><orcidid>https://orcid.org/0000-0003-2149-3871</orcidid></search><sort><creationdate>20191015</creationdate><title>Selective laser melted equiatomic CoCrFeMnNi high-entropy alloy: Microstructure, anisotropic mechanical response, and multiple strengthening mechanism</title><author>Kim, Young-Kyun ; Choe, Jungho ; Lee, Kee-Ahn</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c403t-baefc07833566fa34aab9d9a1cd841e59f72ae1735b527f5dd2490460da842a73</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Anisotropy</topic><topic>Compression tests</topic><topic>Deformation mechanisms</topic><topic>Dislocation density</topic><topic>Grain size</topic><topic>High entropy alloys</topic><topic>High-entropy alloy</topic><topic>Laser beam melting</topic><topic>Mechanical analysis</topic><topic>Mechanical properties</topic><topic>Microstructure</topic><topic>Rapid prototyping</topic><topic>Selective laser melting</topic><topic>Strain</topic><topic>Strengthening mechanisms</topic><topic>Yield strength</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kim, Young-Kyun</creatorcontrib><creatorcontrib>Choe, Jungho</creatorcontrib><creatorcontrib>Lee, Kee-Ahn</creatorcontrib><collection>CrossRef</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of alloys and compounds</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kim, Young-Kyun</au><au>Choe, Jungho</au><au>Lee, Kee-Ahn</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Selective laser melted equiatomic CoCrFeMnNi high-entropy alloy: Microstructure, anisotropic mechanical response, and multiple strengthening mechanism</atitle><jtitle>Journal of alloys and compounds</jtitle><date>2019-10-15</date><risdate>2019</risdate><volume>805</volume><spage>680</spage><epage>691</epage><pages>680-691</pages><issn>0925-8388</issn><eissn>1873-4669</eissn><abstract>One of the major challenges of equiatomic CoCrFeMnNi HEA is to manufacture parts with complex geometry that have higher yield strength. Equiatomic CoCrFeMnNi HEA was successfully fabricated in the present study with selective laser melting. The unique microstructure and mechanical anisotropy that generally appear in additive manufactured materials were investigated. SLM-built HEA has strongly oriented grains, dislocation networks, and nano-sized oxides. In addition, the average grain sizes were measured as 15.66 μm, 12.93 μm, and 5.98 μm on the plane perpendicular to the scanning direction (SD), transverse direction (TD), and building direction (BD), respectively. A compressive test measured outstanding yield strengths (YS) of 778.4 MPa, 766.4 MPa, and 703.5 MPa in the loading axis of SD, TD, and BD, respectively. These outstanding YSs are the result of a combination of fine grain sizes, high dislocation density and nano-sized oxides. In addition, anisotropy in mechanical properties are result from different values of Taylor factor and grain size according to the loading axis. After a compression test, the geometrically necessary dislocation density was found to differ about 2.5 times on each plane parallel to the loading axis in the same macro strain. Based on such findings, the relationship among microstructure, mechanical anisotropy and deformation mechanism are discussed in the present paper. Furthermore, the mechanical properties of SLM-built equiatomic CoCrFeMnNi HEA are predicted by using multiple strengthening mechanisms considering the microstructural characteristics. [Display omitted] •SLM-built HEA shows hierarchical microstructure, dislocation network, and nano-sized oxides.•SLM-built HEA shows outstanding yield strength about ∼778.4 MPa.•Anisotropic mechanical response was observed in SLM-built HEA.•Mechanical properties of SLM-built HEA was predicted by using multiple strengthening mechanism.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jallcom.2019.07.106</doi><tpages>12</tpages><orcidid>https://orcid.org/0000-0002-7463-1759</orcidid><orcidid>https://orcid.org/0000-0003-2149-3871</orcidid></addata></record>
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subjects Anisotropy
Compression tests
Deformation mechanisms
Dislocation density
Grain size
High entropy alloys
High-entropy alloy
Laser beam melting
Mechanical analysis
Mechanical properties
Microstructure
Rapid prototyping
Selective laser melting
Strain
Strengthening mechanisms
Yield strength
title Selective laser melted equiatomic CoCrFeMnNi high-entropy alloy: Microstructure, anisotropic mechanical response, and multiple strengthening mechanism
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