Determination of Volatile Low-Molecular-Weight Amines in Water by Capillary Electrophoresis after Headspace Microextraction
A method for the simultaneous determination of ammonium and seven volatile alkylamines (methylamine, dimethylamine, trimethylamine, ethylamine, n -propylamine, isopropylamine, and diethylamine) in aqueous media by capillary electrophoresis after headspace microextraction into a 5-μL drop of a 0.01 M...
Gespeichert in:
| Veröffentlicht in: | Journal of analytical chemistry (New York, N.Y.) N.Y.), 2019-07, Vol.74 (Suppl 1), p.27-31 |
|---|---|
| Hauptverfasser: | , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 31 |
|---|---|
| container_issue | Suppl 1 |
| container_start_page | 27 |
| container_title | Journal of analytical chemistry (New York, N.Y.) |
| container_volume | 74 |
| creator | Malinina, Yu Kamentsev, M. Ya Timofeeva, I. I. Moskvin, L. N. Yakimova, N. M. Kuchumova, I. D. |
| description | A method for the simultaneous determination of ammonium and seven volatile alkylamines (methylamine, dimethylamine, trimethylamine, ethylamine,
n
-propylamine, isopropylamine, and diethylamine) in aqueous media by capillary electrophoresis after headspace microextraction into a 5-μL drop of a 0.01 M solution of H
3
PO
4
was developed. A solution containing 2 mM acridine, 20 mM acetic acid, and 0.05% Tween 20 was chosen as a background electrolyte for indirect photometric detection. Hydrodynamic sample injection was used. The method was tested using the samples of drinking water with the addition of ammonium and alkylamines. The accuracy of the results was confirmed by a standard addition method. The method developed provides an analytical range from 0.003 to 20 mg/L. |
| doi_str_mv | 10.1134/S1061934819070153 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2281216223</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2281216223</sourcerecordid><originalsourceid>FETCH-LOGICAL-c316t-5baf5bf7202f6b0970e4fadfcce047293ed3e9001796011a9b2a946e8a97a1a13</originalsourceid><addsrcrecordid>eNp1kE9PwzAMxSMEEmPwAbhF4lyIky5tjtMYDGmIA392rNLO2TJ1TUk6wcSXJ9WQOCBOtuTfe882IZfArgFEevMMTIISaQ6KZQxG4ogMQLI8EaDUcezjOOnnp-QshA1jTOUgB-TrFjv0W9vozrqGOkPfXB37GuncfSSPrsZqV2ufLNCu1h0dRxQDtQ1d6Cik5Z5OdGvriOzpNMKdd-3aeQw2UG16ZIZ6GVpdIX20lXf42Xld9Wnn5MToOuDFTx2S17vpy2SWzJ_uHybjeVIJkF0yKrUZlSbjjBtZMpUxTI1emqpClmZcCVwKVIxBpiQD0KrkWqUSc60yDRrEkFwdfFvv3ncYumLjdr6JkQXnOXCQnItIwYGKO4bg0RStt9t4VgGs6H9c_Plx1PCDJkS2WaH_df5f9A0iQH-Y</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2281216223</pqid></control><display><type>article</type><title>Determination of Volatile Low-Molecular-Weight Amines in Water by Capillary Electrophoresis after Headspace Microextraction</title><source>SpringerNature Journals</source><creator>Malinina, Yu ; Kamentsev, M. Ya ; Timofeeva, I. I. ; Moskvin, L. N. ; Yakimova, N. M. ; Kuchumova, I. D.</creator><creatorcontrib>Malinina, Yu ; Kamentsev, M. Ya ; Timofeeva, I. I. ; Moskvin, L. N. ; Yakimova, N. M. ; Kuchumova, I. D.</creatorcontrib><description>A method for the simultaneous determination of ammonium and seven volatile alkylamines (methylamine, dimethylamine, trimethylamine, ethylamine,
n
-propylamine, isopropylamine, and diethylamine) in aqueous media by capillary electrophoresis after headspace microextraction into a 5-μL drop of a 0.01 M solution of H
3
PO
4
was developed. A solution containing 2 mM acridine, 20 mM acetic acid, and 0.05% Tween 20 was chosen as a background electrolyte for indirect photometric detection. Hydrodynamic sample injection was used. The method was tested using the samples of drinking water with the addition of ammonium and alkylamines. The accuracy of the results was confirmed by a standard addition method. The method developed provides an analytical range from 0.003 to 20 mg/L.</description><identifier>ISSN: 1061-9348</identifier><identifier>EISSN: 1608-3199</identifier><identifier>DOI: 10.1134/S1061934819070153</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Acetic acid ; Alkylamines ; Amines ; Analytical Chemistry ; Aqueous solutions ; Capillary electrophoresis ; Chemistry ; Chemistry and Materials Science ; Drinking water ; Electrophoresis ; Photometry ; Trimethylamine</subject><ispartof>Journal of analytical chemistry (New York, N.Y.), 2019-07, Vol.74 (Suppl 1), p.27-31</ispartof><rights>Pleiades Publishing, Ltd. 2019</rights><rights>Copyright Springer Nature B.V. 2019</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-5baf5bf7202f6b0970e4fadfcce047293ed3e9001796011a9b2a946e8a97a1a13</citedby><cites>FETCH-LOGICAL-c316t-5baf5bf7202f6b0970e4fadfcce047293ed3e9001796011a9b2a946e8a97a1a13</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S1061934819070153$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S1061934819070153$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>315,781,785,27929,27930,41493,42562,51324</link.rule.ids></links><search><creatorcontrib>Malinina, Yu</creatorcontrib><creatorcontrib>Kamentsev, M. Ya</creatorcontrib><creatorcontrib>Timofeeva, I. I.</creatorcontrib><creatorcontrib>Moskvin, L. N.</creatorcontrib><creatorcontrib>Yakimova, N. M.</creatorcontrib><creatorcontrib>Kuchumova, I. D.</creatorcontrib><title>Determination of Volatile Low-Molecular-Weight Amines in Water by Capillary Electrophoresis after Headspace Microextraction</title><title>Journal of analytical chemistry (New York, N.Y.)</title><addtitle>J Anal Chem</addtitle><description>A method for the simultaneous determination of ammonium and seven volatile alkylamines (methylamine, dimethylamine, trimethylamine, ethylamine,
n
-propylamine, isopropylamine, and diethylamine) in aqueous media by capillary electrophoresis after headspace microextraction into a 5-μL drop of a 0.01 M solution of H
3
PO
4
was developed. A solution containing 2 mM acridine, 20 mM acetic acid, and 0.05% Tween 20 was chosen as a background electrolyte for indirect photometric detection. Hydrodynamic sample injection was used. The method was tested using the samples of drinking water with the addition of ammonium and alkylamines. The accuracy of the results was confirmed by a standard addition method. The method developed provides an analytical range from 0.003 to 20 mg/L.</description><subject>Acetic acid</subject><subject>Alkylamines</subject><subject>Amines</subject><subject>Analytical Chemistry</subject><subject>Aqueous solutions</subject><subject>Capillary electrophoresis</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Drinking water</subject><subject>Electrophoresis</subject><subject>Photometry</subject><subject>Trimethylamine</subject><issn>1061-9348</issn><issn>1608-3199</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><recordid>eNp1kE9PwzAMxSMEEmPwAbhF4lyIky5tjtMYDGmIA392rNLO2TJ1TUk6wcSXJ9WQOCBOtuTfe882IZfArgFEevMMTIISaQ6KZQxG4ogMQLI8EaDUcezjOOnnp-QshA1jTOUgB-TrFjv0W9vozrqGOkPfXB37GuncfSSPrsZqV2ufLNCu1h0dRxQDtQ1d6Cik5Z5OdGvriOzpNMKdd-3aeQw2UG16ZIZ6GVpdIX20lXf42Xld9Wnn5MToOuDFTx2S17vpy2SWzJ_uHybjeVIJkF0yKrUZlSbjjBtZMpUxTI1emqpClmZcCVwKVIxBpiQD0KrkWqUSc60yDRrEkFwdfFvv3ncYumLjdr6JkQXnOXCQnItIwYGKO4bg0RStt9t4VgGs6H9c_Plx1PCDJkS2WaH_df5f9A0iQH-Y</recordid><startdate>20190701</startdate><enddate>20190701</enddate><creator>Malinina, Yu</creator><creator>Kamentsev, M. Ya</creator><creator>Timofeeva, I. I.</creator><creator>Moskvin, L. N.</creator><creator>Yakimova, N. M.</creator><creator>Kuchumova, I. D.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20190701</creationdate><title>Determination of Volatile Low-Molecular-Weight Amines in Water by Capillary Electrophoresis after Headspace Microextraction</title><author>Malinina, Yu ; Kamentsev, M. Ya ; Timofeeva, I. I. ; Moskvin, L. N. ; Yakimova, N. M. ; Kuchumova, I. D.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-5baf5bf7202f6b0970e4fadfcce047293ed3e9001796011a9b2a946e8a97a1a13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Acetic acid</topic><topic>Alkylamines</topic><topic>Amines</topic><topic>Analytical Chemistry</topic><topic>Aqueous solutions</topic><topic>Capillary electrophoresis</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Drinking water</topic><topic>Electrophoresis</topic><topic>Photometry</topic><topic>Trimethylamine</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Malinina, Yu</creatorcontrib><creatorcontrib>Kamentsev, M. Ya</creatorcontrib><creatorcontrib>Timofeeva, I. I.</creatorcontrib><creatorcontrib>Moskvin, L. N.</creatorcontrib><creatorcontrib>Yakimova, N. M.</creatorcontrib><creatorcontrib>Kuchumova, I. D.</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of analytical chemistry (New York, N.Y.)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Malinina, Yu</au><au>Kamentsev, M. Ya</au><au>Timofeeva, I. I.</au><au>Moskvin, L. N.</au><au>Yakimova, N. M.</au><au>Kuchumova, I. D.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Determination of Volatile Low-Molecular-Weight Amines in Water by Capillary Electrophoresis after Headspace Microextraction</atitle><jtitle>Journal of analytical chemistry (New York, N.Y.)</jtitle><stitle>J Anal Chem</stitle><date>2019-07-01</date><risdate>2019</risdate><volume>74</volume><issue>Suppl 1</issue><spage>27</spage><epage>31</epage><pages>27-31</pages><issn>1061-9348</issn><eissn>1608-3199</eissn><abstract>A method for the simultaneous determination of ammonium and seven volatile alkylamines (methylamine, dimethylamine, trimethylamine, ethylamine,
n
-propylamine, isopropylamine, and diethylamine) in aqueous media by capillary electrophoresis after headspace microextraction into a 5-μL drop of a 0.01 M solution of H
3
PO
4
was developed. A solution containing 2 mM acridine, 20 mM acetic acid, and 0.05% Tween 20 was chosen as a background electrolyte for indirect photometric detection. Hydrodynamic sample injection was used. The method was tested using the samples of drinking water with the addition of ammonium and alkylamines. The accuracy of the results was confirmed by a standard addition method. The method developed provides an analytical range from 0.003 to 20 mg/L.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S1061934819070153</doi><tpages>5</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1061-9348 |
| ispartof | Journal of analytical chemistry (New York, N.Y.), 2019-07, Vol.74 (Suppl 1), p.27-31 |
| issn | 1061-9348 1608-3199 |
| language | eng |
| recordid | cdi_proquest_journals_2281216223 |
| source | SpringerNature Journals |
| subjects | Acetic acid Alkylamines Amines Analytical Chemistry Aqueous solutions Capillary electrophoresis Chemistry Chemistry and Materials Science Drinking water Electrophoresis Photometry Trimethylamine |
| title | Determination of Volatile Low-Molecular-Weight Amines in Water by Capillary Electrophoresis after Headspace Microextraction |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-16T02%3A54%3A01IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Determination%20of%20Volatile%20Low-Molecular-Weight%20Amines%20in%20Water%20by%20Capillary%20Electrophoresis%20after%20Headspace%20Microextraction&rft.jtitle=Journal%20of%20analytical%20chemistry%20(New%20York,%20N.Y.)&rft.au=Malinina,%20Yu&rft.date=2019-07-01&rft.volume=74&rft.issue=Suppl%201&rft.spage=27&rft.epage=31&rft.pages=27-31&rft.issn=1061-9348&rft.eissn=1608-3199&rft_id=info:doi/10.1134/S1061934819070153&rft_dat=%3Cproquest_cross%3E2281216223%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2281216223&rft_id=info:pmid/&rfr_iscdi=true |