Mechanical and Corrosion Behavior of TiN Coatings Deposited on Nitrided AISI 420 Stainless Steel
TiN coatings are widely used in different applications for extending the lifetime of components due to their high hardness and good wear resistance. However, it is not convenient to deposit them on soft stainless steels. In this work, the wear and corrosion behavior of commercial TiN coatings deposi...
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| Veröffentlicht in: | Key engineering materials 2019-07, Vol.813, p.135-140 |
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| creator | Silva, Kevin Dalibon, Eugenia Laura Moreira, Ramiro D. Cabo, Amado Halabi, Jorge Brühl, Sonia P. |
| description | TiN coatings are widely used in different applications for extending the lifetime of components due to their high hardness and good wear resistance. However, it is not convenient to deposit them on soft stainless steels. In this work, the wear and corrosion behavior of commercial TiN coatings deposited by Arc-PVD on nitrided and non-nitrided martensitic stainless steel was studied. Two different nitriding conditions were used, one at high temperature (HTN) and the other at low temperature (LTN). Nanohardness and microhardness were measured. The microstructure was characterized by OM, SEM, XRD and XPS. Pin on disk and erosion tests were carried out in order to evaluate their wear resistance. The corrosion behavior was analyzed in salt spray fog and electrochemical tests in NaCl solution and the adhesion was measured in Scratch and Rockwell C Indentation tests.The coating thickness was about 1.5 µm and its hardness of 34 GPa. The nitrided layers were 13 µm and 17 µm thick for LTN and HTN, the hardness was approximately 12 GPa for both nitrided samples. The nitrided layer improved TiN coating adhesion in the Scratch tests. The wear loss volume was similar for both duplex and only coated samples in pin on disk tests. Nevertheless, wear resistance was not good for the LTN or HTN + TiN coating system in the erosion tests. Regarding corrosion behavior, the coatings showed poor corrosion resistance and this could be related to the presence of porous defects, which allow the solution to reach and attack the substrate, thus producing coating detachment around the pits. |
| doi_str_mv | 10.4028/www.scientific.net/KEM.813.135 |
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However, it is not convenient to deposit them on soft stainless steels. In this work, the wear and corrosion behavior of commercial TiN coatings deposited by Arc-PVD on nitrided and non-nitrided martensitic stainless steel was studied. Two different nitriding conditions were used, one at high temperature (HTN) and the other at low temperature (LTN). Nanohardness and microhardness were measured. The microstructure was characterized by OM, SEM, XRD and XPS. Pin on disk and erosion tests were carried out in order to evaluate their wear resistance. The corrosion behavior was analyzed in salt spray fog and electrochemical tests in NaCl solution and the adhesion was measured in Scratch and Rockwell C Indentation tests.The coating thickness was about 1.5 µm and its hardness of 34 GPa. The nitrided layers were 13 µm and 17 µm thick for LTN and HTN, the hardness was approximately 12 GPa for both nitrided samples. The nitrided layer improved TiN coating adhesion in the Scratch tests. The wear loss volume was similar for both duplex and only coated samples in pin on disk tests. Nevertheless, wear resistance was not good for the LTN or HTN + TiN coating system in the erosion tests. Regarding corrosion behavior, the coatings showed poor corrosion resistance and this could be related to the presence of porous defects, which allow the solution to reach and attack the substrate, thus producing coating detachment around the pits.</description><identifier>ISSN: 1013-9826</identifier><identifier>ISSN: 1662-9795</identifier><identifier>EISSN: 1662-9795</identifier><identifier>DOI: 10.4028/www.scientific.net/KEM.813.135</identifier><language>eng</language><publisher>Zurich: Trans Tech Publications Ltd</publisher><subject>Adhesion tests ; Arc deposition ; Corrosion ; Corrosion resistance ; Corrosion tests ; Corrosive wear ; Duplex stainless steels ; Erosion resistance ; Hardness ; Hardness tests ; High temperature ; Indentation ; Martensitic stainless steels ; Microhardness ; Nanohardness ; Pin on disk tests ; Protective coatings ; Scratch tests ; Service life assessment ; Stainless steel ; Substrates ; Tin ; Wear resistance ; X ray photoelectron spectroscopy</subject><ispartof>Key engineering materials, 2019-07, Vol.813, p.135-140</ispartof><rights>2019 Trans Tech Publications Ltd</rights><rights>Copyright Trans Tech Publications Ltd. Jul 2019</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c2715-4393d5085de668002fdd99967a10ed8a33e9c3bc8485fa5fad08c4fe33844fc03</citedby><cites>FETCH-LOGICAL-c2715-4393d5085de668002fdd99967a10ed8a33e9c3bc8485fa5fad08c4fe33844fc03</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttps://www.scientific.net/Image/TitleCover/4885?width=600</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Silva, Kevin</creatorcontrib><creatorcontrib>Dalibon, Eugenia Laura</creatorcontrib><creatorcontrib>Moreira, Ramiro D.</creatorcontrib><creatorcontrib>Cabo, Amado</creatorcontrib><creatorcontrib>Halabi, Jorge</creatorcontrib><creatorcontrib>Brühl, Sonia P.</creatorcontrib><title>Mechanical and Corrosion Behavior of TiN Coatings Deposited on Nitrided AISI 420 Stainless Steel</title><title>Key engineering materials</title><description>TiN coatings are widely used in different applications for extending the lifetime of components due to their high hardness and good wear resistance. However, it is not convenient to deposit them on soft stainless steels. In this work, the wear and corrosion behavior of commercial TiN coatings deposited by Arc-PVD on nitrided and non-nitrided martensitic stainless steel was studied. Two different nitriding conditions were used, one at high temperature (HTN) and the other at low temperature (LTN). Nanohardness and microhardness were measured. The microstructure was characterized by OM, SEM, XRD and XPS. Pin on disk and erosion tests were carried out in order to evaluate their wear resistance. The corrosion behavior was analyzed in salt spray fog and electrochemical tests in NaCl solution and the adhesion was measured in Scratch and Rockwell C Indentation tests.The coating thickness was about 1.5 µm and its hardness of 34 GPa. The nitrided layers were 13 µm and 17 µm thick for LTN and HTN, the hardness was approximately 12 GPa for both nitrided samples. The nitrided layer improved TiN coating adhesion in the Scratch tests. The wear loss volume was similar for both duplex and only coated samples in pin on disk tests. Nevertheless, wear resistance was not good for the LTN or HTN + TiN coating system in the erosion tests. Regarding corrosion behavior, the coatings showed poor corrosion resistance and this could be related to the presence of porous defects, which allow the solution to reach and attack the substrate, thus producing coating detachment around the pits.</description><subject>Adhesion tests</subject><subject>Arc deposition</subject><subject>Corrosion</subject><subject>Corrosion resistance</subject><subject>Corrosion tests</subject><subject>Corrosive wear</subject><subject>Duplex stainless steels</subject><subject>Erosion resistance</subject><subject>Hardness</subject><subject>Hardness tests</subject><subject>High temperature</subject><subject>Indentation</subject><subject>Martensitic stainless steels</subject><subject>Microhardness</subject><subject>Nanohardness</subject><subject>Pin on disk tests</subject><subject>Protective coatings</subject><subject>Scratch tests</subject><subject>Service life assessment</subject><subject>Stainless steel</subject><subject>Substrates</subject><subject>Tin</subject><subject>Wear resistance</subject><subject>X ray photoelectron spectroscopy</subject><issn>1013-9826</issn><issn>1662-9795</issn><issn>1662-9795</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNqNkEFLAzEQhRdRsFb_Q0Dwtttkk90mF7HWqsW2HlrPMSZZm1KzNUkt_nunVPAqDDMP5vGG-bLsiuCC4ZL3drtdEbWzPrnG6cLb1HsaTQtOaEFodZR1SF2XueiL6hg0JjQXvKxPs7MYVxhTwknVyV6nVi-Vd1qtkfIGDdsQ2uhaj27tUn25NqC2QQs3g41Kzr9HdGc34EjWIHDNXArOgB6M52PESozmSTm_tjGCsnZ9np00ah3txe_sZi_3o8XwMZ88P4yHg0muyz6pckYFNRXmlbF1zTEuG2OEEHVfEWwNV5Raoemb5oxXjYIymGvWWEo5Y43GtJtdHnI3of3c2pjkqt0GDydlWdaM7ZsA1_XBpeHLGGwjN8F9qPAtCZZ7qhKoyj-qEqhKoCqBqgSqEHBzCEhB-ZgA3t-df0b8AMlNiAw</recordid><startdate>20190701</startdate><enddate>20190701</enddate><creator>Silva, Kevin</creator><creator>Dalibon, Eugenia Laura</creator><creator>Moreira, Ramiro D.</creator><creator>Cabo, Amado</creator><creator>Halabi, Jorge</creator><creator>Brühl, Sonia P.</creator><general>Trans Tech Publications Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F28</scope><scope>FR3</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope></search><sort><creationdate>20190701</creationdate><title>Mechanical and Corrosion Behavior of TiN Coatings Deposited on Nitrided AISI 420 Stainless Steel</title><author>Silva, Kevin ; 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However, it is not convenient to deposit them on soft stainless steels. In this work, the wear and corrosion behavior of commercial TiN coatings deposited by Arc-PVD on nitrided and non-nitrided martensitic stainless steel was studied. Two different nitriding conditions were used, one at high temperature (HTN) and the other at low temperature (LTN). Nanohardness and microhardness were measured. The microstructure was characterized by OM, SEM, XRD and XPS. Pin on disk and erosion tests were carried out in order to evaluate their wear resistance. The corrosion behavior was analyzed in salt spray fog and electrochemical tests in NaCl solution and the adhesion was measured in Scratch and Rockwell C Indentation tests.The coating thickness was about 1.5 µm and its hardness of 34 GPa. The nitrided layers were 13 µm and 17 µm thick for LTN and HTN, the hardness was approximately 12 GPa for both nitrided samples. The nitrided layer improved TiN coating adhesion in the Scratch tests. The wear loss volume was similar for both duplex and only coated samples in pin on disk tests. Nevertheless, wear resistance was not good for the LTN or HTN + TiN coating system in the erosion tests. Regarding corrosion behavior, the coatings showed poor corrosion resistance and this could be related to the presence of porous defects, which allow the solution to reach and attack the substrate, thus producing coating detachment around the pits.</abstract><cop>Zurich</cop><pub>Trans Tech Publications Ltd</pub><doi>10.4028/www.scientific.net/KEM.813.135</doi><tpages>6</tpages></addata></record> |
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| subjects | Adhesion tests Arc deposition Corrosion Corrosion resistance Corrosion tests Corrosive wear Duplex stainless steels Erosion resistance Hardness Hardness tests High temperature Indentation Martensitic stainless steels Microhardness Nanohardness Pin on disk tests Protective coatings Scratch tests Service life assessment Stainless steel Substrates Tin Wear resistance X ray photoelectron spectroscopy |
| title | Mechanical and Corrosion Behavior of TiN Coatings Deposited on Nitrided AISI 420 Stainless Steel |
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