Effects of microstructure on flexural strength of biomorphic C/SiC composites

Biomorphic C/SiC composites were fabricated from different kinds of wood by liquid silicon infiltration (LSI) following a two-step process. In the first-step, the wood is converted into carbon preforms by pyrolysis in a nitrogen atmosphere. The carbon preforms are then infiltrated by silicon melt at...

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Veröffentlicht in:International journal of fracture 2008-06, Vol.151 (2), p.233-245
Hauptverfasser: Park, Hee S., Jang, Jong J., Lee, Kyong H., Lim, Kwang H., Park, Sang B., Kim, Yun C., Hong, Soon H.
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container_end_page 245
container_issue 2
container_start_page 233
container_title International journal of fracture
container_volume 151
creator Park, Hee S.
Jang, Jong J.
Lee, Kyong H.
Lim, Kwang H.
Park, Sang B.
Kim, Yun C.
Hong, Soon H.
description Biomorphic C/SiC composites were fabricated from different kinds of wood by liquid silicon infiltration (LSI) following a two-step process. In the first-step, the wood is converted into carbon preforms by pyrolysis in a nitrogen atmosphere. The carbon preforms are then infiltrated by silicon melt at 1,560°C under vacuum to fabricate C/SiC composites. The mechanical properties of the C/SiC composites were characterized by flexural tests at ambient temperature, 1,000, and 1,300°C, and the relationship between mechanical properties and microstructure was analyzed. The flexural strength of the biomorphic composites was strongly dependent on the properties of the carbon preforms and the degree of silicon infiltration. The flexural strength increased with increasing SiC content and bulk density of composite, and with decreasing porosity in the C/SiC composite. An analysis of fractographs of fractured C/SiC composites showed a cleavage type fracture, indicating brittle fracture behavior.
doi_str_mv 10.1007/s10704-008-9259-6
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In the first-step, the wood is converted into carbon preforms by pyrolysis in a nitrogen atmosphere. The carbon preforms are then infiltrated by silicon melt at 1,560°C under vacuum to fabricate C/SiC composites. The mechanical properties of the C/SiC composites were characterized by flexural tests at ambient temperature, 1,000, and 1,300°C, and the relationship between mechanical properties and microstructure was analyzed. The flexural strength of the biomorphic composites was strongly dependent on the properties of the carbon preforms and the degree of silicon infiltration. The flexural strength increased with increasing SiC content and bulk density of composite, and with decreasing porosity in the C/SiC composite. An analysis of fractographs of fractured C/SiC composites showed a cleavage type fracture, indicating brittle fracture behavior.</description><identifier>ISSN: 0376-9429</identifier><identifier>EISSN: 1573-2673</identifier><identifier>DOI: 10.1007/s10704-008-9259-6</identifier><identifier>CODEN: IJFRAP</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Ambient temperature ; Applied sciences ; Automotive Engineering ; Bulk density ; Carbon ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Civil Engineering ; Classical Mechanics ; Composite materials ; Exact sciences and technology ; Flexural strength ; Fracture mechanics (crack, fatigue, damage...) ; Fundamental areas of phenomenology (including applications) ; Infiltration ; Materials Science ; Mechanical Engineering ; Mechanical properties ; Microstructure ; Original Paper ; Physics ; Polymer industry, paints, wood ; Porosity ; Preforms ; Pyrolysis ; Solid mechanics ; Structural and continuum mechanics ; Wood ; Wood. 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In the first-step, the wood is converted into carbon preforms by pyrolysis in a nitrogen atmosphere. The carbon preforms are then infiltrated by silicon melt at 1,560°C under vacuum to fabricate C/SiC composites. The mechanical properties of the C/SiC composites were characterized by flexural tests at ambient temperature, 1,000, and 1,300°C, and the relationship between mechanical properties and microstructure was analyzed. The flexural strength of the biomorphic composites was strongly dependent on the properties of the carbon preforms and the degree of silicon infiltration. The flexural strength increased with increasing SiC content and bulk density of composite, and with decreasing porosity in the C/SiC composite. An analysis of fractographs of fractured C/SiC composites showed a cleavage type fracture, indicating brittle fracture behavior.</description><subject>Ambient temperature</subject><subject>Applied sciences</subject><subject>Automotive Engineering</subject><subject>Bulk density</subject><subject>Carbon</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Civil Engineering</subject><subject>Classical Mechanics</subject><subject>Composite materials</subject><subject>Exact sciences and technology</subject><subject>Flexural strength</subject><subject>Fracture mechanics (crack, fatigue, damage...)</subject><subject>Fundamental areas of phenomenology (including applications)</subject><subject>Infiltration</subject><subject>Materials Science</subject><subject>Mechanical Engineering</subject><subject>Mechanical properties</subject><subject>Microstructure</subject><subject>Original Paper</subject><subject>Physics</subject><subject>Polymer industry, paints, wood</subject><subject>Porosity</subject><subject>Preforms</subject><subject>Pyrolysis</subject><subject>Solid mechanics</subject><subject>Structural and continuum mechanics</subject><subject>Wood</subject><subject>Wood. 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subjects Ambient temperature
Applied sciences
Automotive Engineering
Bulk density
Carbon
Characterization and Evaluation of Materials
Chemistry and Materials Science
Civil Engineering
Classical Mechanics
Composite materials
Exact sciences and technology
Flexural strength
Fracture mechanics (crack, fatigue, damage...)
Fundamental areas of phenomenology (including applications)
Infiltration
Materials Science
Mechanical Engineering
Mechanical properties
Microstructure
Original Paper
Physics
Polymer industry, paints, wood
Porosity
Preforms
Pyrolysis
Solid mechanics
Structural and continuum mechanics
Wood
Wood. Paper. Non wovens
title Effects of microstructure on flexural strength of biomorphic C/SiC composites
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