Influence of microstructure on the mechanical properties and hydrogen embrittlement characteristics of 1800 MPa grade hot-stamped 22MnB5 steel

The influence of the microstructural characteristics on the mechanical and hydrogen embrittlement properties of 1800 MPa grade hot-stamped 22MnB5 steel was experimentally investigated using samples processed under various hot-stamping conditions, i.e., different heating temperatures and strain level...

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Veröffentlicht in:Journal of materials science 2019-03, Vol.54 (6), p.5061-5073
Hauptverfasser: Okayasu, Mitsuhiro, Yang, Lele
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description The influence of the microstructural characteristics on the mechanical and hydrogen embrittlement properties of 1800 MPa grade hot-stamped 22MnB5 steel was experimentally investigated using samples processed under various hot-stamping conditions, i.e., different heating temperatures and strain levels. The tensile strength increased with increasing hot-stamping temperature up to approximately 920 °C and subsequently decreased owing to the increasing sizes of the lath martensite and prior austenite phases. Some degree of internal strain was introduced into the 22MnB5 steel specimen during hot stamping at 920 °C, which led to a slightly higher hardness although no clear microstructural change was observed. The severity of hydrogen embrittlement of the hot-stamped 22MnB5 steel samples was investigated after immersion in a NH 4 SCN solution, and the degree of hydrogen embrittlement was found to be directly associated with the amount of hydrogen that penetrated into the grain boundary and lath martensite boundary. The high-strength 22MnB5 steel with a very small lath martensite phase exhibited severe hydrogen embrittlement due to the large amount of hydrogen in the sample, and the high internal strain (or high dislocation density) could lead to accelerated hydrogen embrittlement. Severe hydrogen embrittlement occurred upon charging with more than approximately 0.8 ppm hydrogen. Based on the obtained results, models are proposed for the hydrogen embrittlement characteristics of hot-stamped 22MnB5 steel.
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The tensile strength increased with increasing hot-stamping temperature up to approximately 920 °C and subsequently decreased owing to the increasing sizes of the lath martensite and prior austenite phases. Some degree of internal strain was introduced into the 22MnB5 steel specimen during hot stamping at 920 °C, which led to a slightly higher hardness although no clear microstructural change was observed. The severity of hydrogen embrittlement of the hot-stamped 22MnB5 steel samples was investigated after immersion in a NH 4 SCN solution, and the degree of hydrogen embrittlement was found to be directly associated with the amount of hydrogen that penetrated into the grain boundary and lath martensite boundary. The high-strength 22MnB5 steel with a very small lath martensite phase exhibited severe hydrogen embrittlement due to the large amount of hydrogen in the sample, and the high internal strain (or high dislocation density) could lead to accelerated hydrogen embrittlement. Severe hydrogen embrittlement occurred upon charging with more than approximately 0.8 ppm hydrogen. Based on the obtained results, models are proposed for the hydrogen embrittlement characteristics of hot-stamped 22MnB5 steel.</description><identifier>ISSN: 0022-2461</identifier><identifier>EISSN: 1573-4803</identifier><identifier>DOI: 10.1007/s10853-018-3175-6</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Boron steels ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Classical Mechanics ; Crystallography and Scattering Methods ; Dislocation density ; Grain boundaries ; Hardness (Materials) ; Heat treating ; Hot stamping ; Hydrogen ; Hydrogen embrittlement ; Martensite ; Materials Science ; Mechanical properties ; Metals ; Microstructure ; Nickel ; Polymer Sciences ; Solid Mechanics ; Submerging</subject><ispartof>Journal of materials science, 2019-03, Vol.54 (6), p.5061-5073</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2018</rights><rights>COPYRIGHT 2019 Springer</rights><rights>Journal of Materials Science is a copyright of Springer, (2018). 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The tensile strength increased with increasing hot-stamping temperature up to approximately 920 °C and subsequently decreased owing to the increasing sizes of the lath martensite and prior austenite phases. Some degree of internal strain was introduced into the 22MnB5 steel specimen during hot stamping at 920 °C, which led to a slightly higher hardness although no clear microstructural change was observed. The severity of hydrogen embrittlement of the hot-stamped 22MnB5 steel samples was investigated after immersion in a NH 4 SCN solution, and the degree of hydrogen embrittlement was found to be directly associated with the amount of hydrogen that penetrated into the grain boundary and lath martensite boundary. The high-strength 22MnB5 steel with a very small lath martensite phase exhibited severe hydrogen embrittlement due to the large amount of hydrogen in the sample, and the high internal strain (or high dislocation density) could lead to accelerated hydrogen embrittlement. Severe hydrogen embrittlement occurred upon charging with more than approximately 0.8 ppm hydrogen. Based on the obtained results, models are proposed for the hydrogen embrittlement characteristics of hot-stamped 22MnB5 steel.</description><subject>Boron steels</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Classical Mechanics</subject><subject>Crystallography and Scattering Methods</subject><subject>Dislocation density</subject><subject>Grain boundaries</subject><subject>Hardness (Materials)</subject><subject>Heat treating</subject><subject>Hot stamping</subject><subject>Hydrogen</subject><subject>Hydrogen embrittlement</subject><subject>Martensite</subject><subject>Materials Science</subject><subject>Mechanical properties</subject><subject>Metals</subject><subject>Microstructure</subject><subject>Nickel</subject><subject>Polymer Sciences</subject><subject>Solid Mechanics</subject><subject>Submerging</subject><issn>0022-2461</issn><issn>1573-4803</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp1kc1u1TAQhS0EEpfCA7CzxIpF2rEd28myVBSu1ArEz9rydca5qRLnYjtS-xS8As_Ck-EoSKgLNAtLo-_M-Mwh5DWDcwagLxKDRooKWFMJpmWlnpAdk1pUdQPiKdkBcF7xWrHn5EVKdwAgNWc78nMf_LhgcEhnT6fBxTnluLi8xNIJNB-RTuiONgzOjvQU5xPGPGCiNnT0-NDFucdAcTrEIecRJwyZFjxalzEOKQ8urZNZA_D71-1nS_toO6THOVcp2-mEHeX8NryTNGXE8SV55u2Y8NXf94x8v37_7epjdfPpw_7q8qZyAmpVOX2QnYWm1tC1ngmvpbaIxZRwB1m7RjjXam1lLaDBFhh43mlQzErHOifFGXmzzS2OfiyYsrmblxjKSsO5bBVvVc0Ldb5RvR3RDMHPuRgr1WE51RzQD6V_KZXmWimxCt4-EhQm433u7ZKS2X_98phlG7vePEX05hSHycYHw8CsoZotVFNCNWuoRhUN3zSpsKHH-O_b_xf9AX31pP8</recordid><startdate>20190301</startdate><enddate>20190301</enddate><creator>Okayasu, Mitsuhiro</creator><creator>Yang, Lele</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><orcidid>https://orcid.org/0000-0003-3897-070X</orcidid></search><sort><creationdate>20190301</creationdate><title>Influence of microstructure on the mechanical properties and hydrogen embrittlement characteristics of 1800 MPa grade hot-stamped 22MnB5 steel</title><author>Okayasu, Mitsuhiro ; 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The tensile strength increased with increasing hot-stamping temperature up to approximately 920 °C and subsequently decreased owing to the increasing sizes of the lath martensite and prior austenite phases. Some degree of internal strain was introduced into the 22MnB5 steel specimen during hot stamping at 920 °C, which led to a slightly higher hardness although no clear microstructural change was observed. The severity of hydrogen embrittlement of the hot-stamped 22MnB5 steel samples was investigated after immersion in a NH 4 SCN solution, and the degree of hydrogen embrittlement was found to be directly associated with the amount of hydrogen that penetrated into the grain boundary and lath martensite boundary. The high-strength 22MnB5 steel with a very small lath martensite phase exhibited severe hydrogen embrittlement due to the large amount of hydrogen in the sample, and the high internal strain (or high dislocation density) could lead to accelerated hydrogen embrittlement. 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subjects Boron steels
Characterization and Evaluation of Materials
Chemistry and Materials Science
Classical Mechanics
Crystallography and Scattering Methods
Dislocation density
Grain boundaries
Hardness (Materials)
Heat treating
Hot stamping
Hydrogen
Hydrogen embrittlement
Martensite
Materials Science
Mechanical properties
Metals
Microstructure
Nickel
Polymer Sciences
Solid Mechanics
Submerging
title Influence of microstructure on the mechanical properties and hydrogen embrittlement characteristics of 1800 MPa grade hot-stamped 22MnB5 steel
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