Solvothermal synthesis of indium-doped zinc oxide TCO films
This paper outlines the preparation of indium-doped zinc oxide films via solvothermal synthesis of nanoparticles, followed by spin coating of the transparent conductive oxide (TCO) layer. The effect of stabilizer type and its concentration on the suspension stability was studied. The influence of th...
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| Veröffentlicht in: | Journal of sol-gel science and technology 2017, Vol.81 (1), p.3-10 |
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| creator | Dinner, O. Shter, G. E. Grader, G. S. |
| description | This paper outlines the preparation of indium-doped zinc oxide films via solvothermal synthesis of nanoparticles, followed by spin coating of the transparent conductive oxide (TCO) layer. The effect of stabilizer type and its concentration on the suspension stability was studied. The influence of the In/Zn molar ratio (in the 0–0.06 range) on the lattice parameters and the cell volume was determined by XRD analysis. A linear change in these parameters was found, indicating a uniform integration of the indium into the ZnO crystal. Thermal analysis using TGA/DTA pointed to the optimal thermal treatment of the TCO layers at 500 °C. In addition, the effect of the molar ratio on the optical and electrical properties was studied. A minimal sheet resistance of 85 % at In/Zn = 0.04 were achieved. The above findings indicate that the solvothermal route can be very effective in the synthesis of state-of-the-art TCO coatings.
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| doi_str_mv | 10.1007/s10971-016-4153-6 |
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Graphical Abstract</description><subject>Ceramics</subject><subject>Chemistry and Materials Science</subject><subject>Composites</subject><subject>Crystal lattices</subject><subject>Differential thermal analysis</subject><subject>Electrical properties</subject><subject>Glass</subject><subject>Heat treatment</subject><subject>Indium</subject><subject>Inorganic Chemistry</subject><subject>Lattice parameters</subject><subject>Materials Science</subject><subject>Nanoparticles</subject><subject>Nanotechnology</subject><subject>Natural Materials</subject><subject>Optical and Electronic Materials</subject><subject>Optical properties</subject><subject>Original Paper: Functional coatings</subject><subject>Oxide coatings</subject><subject>Spin coating</subject><subject>Stabilizers (agents)</subject><subject>Synthesis</subject><subject>thin films and membranes (including deposition techniques)</subject><subject>Zinc coatings</subject><subject>Zinc oxide</subject><subject>Zinc oxides</subject><issn>0928-0707</issn><issn>1573-4846</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp9kDtPwzAUhS0EEqXwA9giMRvu9TtiQhUvqVIHymyZ2IFUSVziFlF-Pa7CwALTucN3zpU-Qs4RLhFAXyWEUiMFVFSg5FQdkAlKzakwQh2SCZTMUNCgj8lJSisAkAL1hFw_xfYjbt7C0Lm2SLs-n6lJRayLpvfNtqM-roMvvpq-KuJn40OxnC2Kumm7dEqOatemcPaTU_J8d7ucPdD54v5xdjOnFRdiQ43Oz7QMoRalD1wqj9KpUBvuGQ9OVTkZIqB4kd44RBa0ckbrGox2EvmUXIy76yG-b0Pa2FXcDn1-aRmTpZRMc_iPQmNAG45YZgpHqhpiSkOo7XpoOjfsLILdm7SjSZtN2r1Jq3KHjZ2U2f41DL-W_yx9A2Wlc5Q</recordid><startdate>2017</startdate><enddate>2017</enddate><creator>Dinner, O.</creator><creator>Shter, G. 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S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c344t-8700575eef49de356d15a6ef83d23ea6c3d2211014b5d8a112e76a877f087a513</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Ceramics</topic><topic>Chemistry and Materials Science</topic><topic>Composites</topic><topic>Crystal lattices</topic><topic>Differential thermal analysis</topic><topic>Electrical properties</topic><topic>Glass</topic><topic>Heat treatment</topic><topic>Indium</topic><topic>Inorganic Chemistry</topic><topic>Lattice parameters</topic><topic>Materials Science</topic><topic>Nanoparticles</topic><topic>Nanotechnology</topic><topic>Natural Materials</topic><topic>Optical and Electronic Materials</topic><topic>Optical properties</topic><topic>Original Paper: Functional coatings</topic><topic>Oxide coatings</topic><topic>Spin coating</topic><topic>Stabilizers (agents)</topic><topic>Synthesis</topic><topic>thin films and membranes (including deposition techniques)</topic><topic>Zinc coatings</topic><topic>Zinc oxide</topic><topic>Zinc oxides</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Dinner, O.</creatorcontrib><creatorcontrib>Shter, G. 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E.</au><au>Grader, G. S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Solvothermal synthesis of indium-doped zinc oxide TCO films</atitle><jtitle>Journal of sol-gel science and technology</jtitle><stitle>J Sol-Gel Sci Technol</stitle><date>2017</date><risdate>2017</risdate><volume>81</volume><issue>1</issue><spage>3</spage><epage>10</epage><pages>3-10</pages><issn>0928-0707</issn><eissn>1573-4846</eissn><abstract>This paper outlines the preparation of indium-doped zinc oxide films via solvothermal synthesis of nanoparticles, followed by spin coating of the transparent conductive oxide (TCO) layer. The effect of stabilizer type and its concentration on the suspension stability was studied. The influence of the In/Zn molar ratio (in the 0–0.06 range) on the lattice parameters and the cell volume was determined by XRD analysis. A linear change in these parameters was found, indicating a uniform integration of the indium into the ZnO crystal. Thermal analysis using TGA/DTA pointed to the optimal thermal treatment of the TCO layers at 500 °C. In addition, the effect of the molar ratio on the optical and electrical properties was studied. A minimal sheet resistance of <46 ohm/square and optical transparency of >85 % at In/Zn = 0.04 were achieved. The above findings indicate that the solvothermal route can be very effective in the synthesis of state-of-the-art TCO coatings.
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| subjects | Ceramics Chemistry and Materials Science Composites Crystal lattices Differential thermal analysis Electrical properties Glass Heat treatment Indium Inorganic Chemistry Lattice parameters Materials Science Nanoparticles Nanotechnology Natural Materials Optical and Electronic Materials Optical properties Original Paper: Functional coatings Oxide coatings Spin coating Stabilizers (agents) Synthesis thin films and membranes (including deposition techniques) Zinc coatings Zinc oxide Zinc oxides |
| title | Solvothermal synthesis of indium-doped zinc oxide TCO films |
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