Rapid mechanochemical synthesis of nanostructured mohite Cu2SnS3 (CTS)

Rapid solvent-free mechanochemical synthesis of CTS nanocrystals from elemental precursors is reported herein. The process is completed in 15 min, proceeding through immediate formation of CuS in a self-sustaining manner and its subsequent reaction with Sn and residual sulfur. The reaction progress...

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Veröffentlicht in:	Journal of materials science 2018-10, Vol.53 (19), p.13631-13642
Hauptverfasser:	Baláž, Matej, Daneu, Nina, Rajňák, Michal, Kurimský, Juraj, Hegedüs, Michal, Dutková, Erika, Fabián, Martin, Kaňuchová, Mária, Baláž, Peter
Format:	Artikel
Sprache:	eng
Schlagworte:	Characterization and Evaluation of Materials Chemistry and Materials Science Classical Mechanics Copper sulfides Crystallites Crystallography and Scattering Methods Electrical resistivity Grain size Materials Science Mechanochemical Synthesis Nanocrystals Optical properties Photoelectrons Polymer Sciences Precursors Silicon Solid Mechanics Synthesis Transmission electron microscopy X-ray diffraction
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