Photocatalytic application of BiFeO3 synthesized via a facile microwave-assisted solution combustion method

Bismuth ferrite (BiFeO 3 ) nanopowder have been successfully synthesized for the first time via a microwave-assisted sol-gel combustion method by using citric acid as fuel. The resulting nanopowder was characterized using FT-IR, TG-DTA, XRD, EDX, VSM, SEM, and UV-Vis DRS. A ferromagnetic hysteresis...

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Veröffentlicht in:Journal of sol-gel science and technology 2018-08, Vol.87 (2), p.340-346
Hauptverfasser: Rabbani, Mahboubeh, Rahimi, Rahmatollah, Farajnejad Ghadi, Hani
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creator Rabbani, Mahboubeh
Rahimi, Rahmatollah
Farajnejad Ghadi, Hani
description Bismuth ferrite (BiFeO 3 ) nanopowder have been successfully synthesized for the first time via a microwave-assisted sol-gel combustion method by using citric acid as fuel. The resulting nanopowder was characterized using FT-IR, TG-DTA, XRD, EDX, VSM, SEM, and UV-Vis DRS. A ferromagnetic hysteresis loop with a saturation magnetization ( M S ) of 0.66 emu g −1 has been observed at room temperature in the sample. The optical properties of the nanosized BiFeO 3 showed its small band gap (=2.08 eV) indicates a possibility of utilizing much visible light for photocatalysis. Highlights BiFeO 3 nanopowder was synthesized via a microwave-assisted combustion method. Citric acid was utilized as fuel for the first time to prepare BiFeO 3 . A ferromagnetic hysteresis loop with a M S of 0.66 emu/g has been observed at RT. The small band gap of 2.08 eV make it a visible light driven photocatalyst.
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The resulting nanopowder was characterized using FT-IR, TG-DTA, XRD, EDX, VSM, SEM, and UV-Vis DRS. A ferromagnetic hysteresis loop with a saturation magnetization ( M S ) of 0.66 emu g −1 has been observed at room temperature in the sample. The optical properties of the nanosized BiFeO 3 showed its small band gap (=2.08 eV) indicates a possibility of utilizing much visible light for photocatalysis. Highlights BiFeO 3 nanopowder was synthesized via a microwave-assisted combustion method. Citric acid was utilized as fuel for the first time to prepare BiFeO 3 . A ferromagnetic hysteresis loop with a M S of 0.66 emu/g has been observed at RT. The small band gap of 2.08 eV make it a visible light driven photocatalyst.</description><identifier>ISSN: 0928-0707</identifier><identifier>EISSN: 1573-4846</identifier><identifier>DOI: 10.1007/s10971-018-4743-6</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Bismuth ferrite ; Ceramics ; Chemistry and Materials Science ; Citric acid ; colloids ; Combustion ; Composites ; Energy gap ; etc. ; Ferromagnetism ; fibers ; Fuels ; Glass ; Hysteresis loops ; Inorganic Chemistry ; Magnetic saturation ; Materials Science ; Nanotechnology ; Natural Materials ; Optical and Electronic Materials ; Optical properties ; Original Paper: Nano-structured materials (particles ; Photocatalysis ; Sol-gel processes ; Synthesis</subject><ispartof>Journal of sol-gel science and technology, 2018-08, Vol.87 (2), p.340-346</ispartof><rights>Springer Science+Business Media, LLC, part of Springer Nature 2018</rights><rights>Copyright Springer Science &amp; Business Media 2018</rights><rights>Journal of Sol-Gel Science and Technology is a copyright of Springer, (2018). 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The resulting nanopowder was characterized using FT-IR, TG-DTA, XRD, EDX, VSM, SEM, and UV-Vis DRS. A ferromagnetic hysteresis loop with a saturation magnetization ( M S ) of 0.66 emu g −1 has been observed at room temperature in the sample. The optical properties of the nanosized BiFeO 3 showed its small band gap (=2.08 eV) indicates a possibility of utilizing much visible light for photocatalysis. Highlights BiFeO 3 nanopowder was synthesized via a microwave-assisted combustion method. Citric acid was utilized as fuel for the first time to prepare BiFeO 3 . A ferromagnetic hysteresis loop with a M S of 0.66 emu/g has been observed at RT. The small band gap of 2.08 eV make it a visible light driven photocatalyst.</description><subject>Bismuth ferrite</subject><subject>Ceramics</subject><subject>Chemistry and Materials Science</subject><subject>Citric acid</subject><subject>colloids</subject><subject>Combustion</subject><subject>Composites</subject><subject>Energy gap</subject><subject>etc.</subject><subject>Ferromagnetism</subject><subject>fibers</subject><subject>Fuels</subject><subject>Glass</subject><subject>Hysteresis loops</subject><subject>Inorganic Chemistry</subject><subject>Magnetic saturation</subject><subject>Materials Science</subject><subject>Nanotechnology</subject><subject>Natural Materials</subject><subject>Optical and Electronic Materials</subject><subject>Optical properties</subject><subject>Original Paper: Nano-structured materials (particles</subject><subject>Photocatalysis</subject><subject>Sol-gel processes</subject><subject>Synthesis</subject><issn>0928-0707</issn><issn>1573-4846</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNp9kE1LAzEQhoMoWKs_wNuC5-jMJpuPoxa_oFAPeg5pNmtTt03dbJX6601bwZOeZoZ53hnel5BzhEsEkFcJQUukgIpyyRkVB2SAlWSUKy4OyQB0qShIkMfkJKU5AFQc5YC8Pc1iH53tbbvpgyvsatWGPIa4LGJT3IQ7P2FF2iz7mU_hy9fFR7CFLRrrQuuLRXBd_LQfntqUQurzPsV2vZO7uJiu065d-H4W61Ny1Ng2-bOfOiQvd7fPowc6ntw_jq7H1DGFPeVT8E4pxRtENRUlB611VWcDvGKodC1qxTW3eVTaC6elkliByCxI4Twbkov93VUX39c-9WYe190yvzRlWemqRMHwXwqUYhxLZJnCPZV9ptT5xqy6sLDdxiCYbfJmn7zJyZtt8kZkTbnXpMwuX333e_lv0TeZUoVS</recordid><startdate>20180801</startdate><enddate>20180801</enddate><creator>Rabbani, Mahboubeh</creator><creator>Rahimi, Rahmatollah</creator><creator>Farajnejad Ghadi, Hani</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope></search><sort><creationdate>20180801</creationdate><title>Photocatalytic application of BiFeO3 synthesized via a facile microwave-assisted solution combustion method</title><author>Rabbani, Mahboubeh ; 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The resulting nanopowder was characterized using FT-IR, TG-DTA, XRD, EDX, VSM, SEM, and UV-Vis DRS. A ferromagnetic hysteresis loop with a saturation magnetization ( M S ) of 0.66 emu g −1 has been observed at room temperature in the sample. The optical properties of the nanosized BiFeO 3 showed its small band gap (=2.08 eV) indicates a possibility of utilizing much visible light for photocatalysis. Highlights BiFeO 3 nanopowder was synthesized via a microwave-assisted combustion method. Citric acid was utilized as fuel for the first time to prepare BiFeO 3 . A ferromagnetic hysteresis loop with a M S of 0.66 emu/g has been observed at RT. The small band gap of 2.08 eV make it a visible light driven photocatalyst.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10971-018-4743-6</doi><tpages>7</tpages></addata></record>
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subjects Bismuth ferrite
Ceramics
Chemistry and Materials Science
Citric acid
colloids
Combustion
Composites
Energy gap
etc.
Ferromagnetism
fibers
Fuels
Glass
Hysteresis loops
Inorganic Chemistry
Magnetic saturation
Materials Science
Nanotechnology
Natural Materials
Optical and Electronic Materials
Optical properties
Original Paper: Nano-structured materials (particles
Photocatalysis
Sol-gel processes
Synthesis
title Photocatalytic application of BiFeO3 synthesized via a facile microwave-assisted solution combustion method
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