[Formula Omitted]-Band Complex Permittivity Measurements at High Temperature Using Free-Space Methods

Free-space measurement techniques can be contactless and are able to accommodate large, flat sheets of dielectric material, making them useful for characterization of high-temperature, millimeter-wave, window and radome candidate materials. As part of the present work, a high-temperature, W-band (75...

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Veröffentlicht in:IEEE transactions on components, packaging, and manufacturing technology (2011) packaging, and manufacturing technology (2011), 2019-01, Vol.9 (6), p.1011
Hauptverfasser: Hilario, Martin S, Hoff, Brad W, Benmaan Jawdat, Lanagan, Michael T, Cohick, Zane W, Dynys, Frederick W, Mackey, Jonathan A, Gaone, Joseph M
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container_title IEEE transactions on components, packaging, and manufacturing technology (2011)
container_volume 9
creator Hilario, Martin S
Hoff, Brad W
Benmaan Jawdat
Lanagan, Michael T
Cohick, Zane W
Dynys, Frederick W
Mackey, Jonathan A
Gaone, Joseph M
description Free-space measurement techniques can be contactless and are able to accommodate large, flat sheets of dielectric material, making them useful for characterization of high-temperature, millimeter-wave, window and radome candidate materials. As part of the present work, a high-temperature, W-band (75–110 GHz), free-space measurement system was developed and used to characterize complex dielectric properties of bulk material samples at temperatures ranging from 25 °C to 600 °C. Two test cases, polyvinyl chloride (PVC) and CoorsTek 92% alumina, were measured at 25 °C and found to have [Formula Omitted] values of 2.731 ± 0.005 and 8.061 ± 0.027 at 95 GHz, respectively. The 25 °C PVC sample was measured to have a [Formula Omitted] value of 0.032 ± 0.007. At 25 °C, the [Formula Omitted] value of the 92% alumina sample was below the uncertainty threshold achievable with the present free-space measurement apparatus and could only be bounded to
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As part of the present work, a high-temperature, W-band (75–110 GHz), free-space measurement system was developed and used to characterize complex dielectric properties of bulk material samples at temperatures ranging from 25 °C to 600 °C. Two test cases, polyvinyl chloride (PVC) and CoorsTek 92% alumina, were measured at 25 °C and found to have [Formula Omitted] values of 2.731 ± 0.005 and 8.061 ± 0.027 at 95 GHz, respectively. The 25 °C PVC sample was measured to have a [Formula Omitted] value of 0.032 ± 0.007. At 25 °C, the [Formula Omitted] value of the 92% alumina sample was below the uncertainty threshold achievable with the present free-space measurement apparatus and could only be bounded to &lt;0.009. As the alumina sample was heated to 600 °C, [Formula Omitted] and [Formula Omitted] values increased to 8.501 ± 0.028 and 0.035 ± 0.008, respectively. The high-temperature behavior of the authors’ 92% alumina ceramic was found to be similar to that previously documented for Sumitomo AKP-50 alumina over the 25 °C–600 °C temperature range. In addition to the 92% alumina sample, three commercially available ceramic substrates (zirconium oxide, boron nitride, and silicon nitride) were also characterized at temperatures ranging from 25 °C to 600 °C.</description><identifier>ISSN: 2156-3950</identifier><identifier>EISSN: 2156-3985</identifier><identifier>DOI: 10.1109/TCPMT.2019.2912837</identifier><language>eng</language><publisher>Piscataway: The Institute of Electrical and Electronics Engineers, Inc. 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As part of the present work, a high-temperature, W-band (75–110 GHz), free-space measurement system was developed and used to characterize complex dielectric properties of bulk material samples at temperatures ranging from 25 °C to 600 °C. Two test cases, polyvinyl chloride (PVC) and CoorsTek 92% alumina, were measured at 25 °C and found to have [Formula Omitted] values of 2.731 ± 0.005 and 8.061 ± 0.027 at 95 GHz, respectively. The 25 °C PVC sample was measured to have a [Formula Omitted] value of 0.032 ± 0.007. At 25 °C, the [Formula Omitted] value of the 92% alumina sample was below the uncertainty threshold achievable with the present free-space measurement apparatus and could only be bounded to &lt;0.009. As the alumina sample was heated to 600 °C, [Formula Omitted] and [Formula Omitted] values increased to 8.501 ± 0.028 and 0.035 ± 0.008, respectively. The high-temperature behavior of the authors’ 92% alumina ceramic was found to be similar to that previously documented for Sumitomo AKP-50 alumina over the 25 °C–600 °C temperature range. 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The high-temperature behavior of the authors’ 92% alumina ceramic was found to be similar to that previously documented for Sumitomo AKP-50 alumina over the 25 °C–600 °C temperature range. In addition to the 92% alumina sample, three commercially available ceramic substrates (zirconium oxide, boron nitride, and silicon nitride) were also characterized at temperatures ranging from 25 °C to 600 °C.</abstract><cop>Piscataway</cop><pub>The Institute of Electrical and Electronics Engineers, Inc. (IEEE)</pub><doi>10.1109/TCPMT.2019.2912837</doi></addata></record>
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subjects Alumina
Aluminum oxide
Boron nitride
Complex permittivity
Dielectric properties
High temperature
Materials selection
Measurement methods
Measurement techniques
Millimeter waves
Polyvinyl chloride
Radomes
Silicon nitride
Silicon substrates
Zirconium oxides
title [Formula Omitted]-Band Complex Permittivity Measurements at High Temperature Using Free-Space Methods
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