Synthesis and high-temperature creep behavior of a SiLuOC-based glass-ceramic
In this work, a lutetium-modified silicon oxycarbide (SiOC) glass ceramic was prepared from a single-source precursor via pyrolysis and subsequent hot pressing. It is shown that the main crystalline phase in the hot-pressed SiLuOC is Lu2Si2O7. The high-temperature (HT) creep behavior of SiLuOC was a...
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| Veröffentlicht in: | Journal of the Ceramic Society of Japan 2016/10/01, Vol.124(10), pp.1006-1012 |
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| container_title | Journal of the Ceramic Society of Japan |
| container_volume | 124 |
| creator | STABLER, Christina SEEMÜLLER, Christoph CHOUDHARY, Ahmad HEILMAIER, Martin LAUTERBACH, Stefan KLEEBE, Hans-Joachim IONESCU, Emanuel |
| description | In this work, a lutetium-modified silicon oxycarbide (SiOC) glass ceramic was prepared from a single-source precursor via pyrolysis and subsequent hot pressing. It is shown that the main crystalline phase in the hot-pressed SiLuOC is Lu2Si2O7. The high-temperature (HT) creep behavior of SiLuOC was assessed by compression creep experiments performed between 1100 and 1300°C at constant true stresses between 25 and 75 MPa. The calculated viscosity values of SiLuOC were found to be significantly higher as compared to those of SiRE(Al,Mg)ON glasses (RE = rare earth elements). Thus, the presented SiLuOC-based glasses might be used as alternative sintering aids for the liquid-phase sintering of HT creep resistant Si3N4 monolithic samples. |
| doi_str_mv | 10.2109/jcersj2.16101 |
| format | Article |
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It is shown that the main crystalline phase in the hot-pressed SiLuOC is Lu2Si2O7. The high-temperature (HT) creep behavior of SiLuOC was assessed by compression creep experiments performed between 1100 and 1300°C at constant true stresses between 25 and 75 MPa. The calculated viscosity values of SiLuOC were found to be significantly higher as compared to those of SiRE(Al,Mg)ON glasses (RE = rare earth elements). Thus, the presented SiLuOC-based glasses might be used as alternative sintering aids for the liquid-phase sintering of HT creep resistant Si3N4 monolithic samples.</description><identifier>ISSN: 1882-0743</identifier><identifier>EISSN: 1348-6535</identifier><identifier>DOI: 10.2109/jcersj2.16101</identifier><language>eng ; jpn</language><publisher>Tokyo: The Ceramic Society of Japan</publisher><subject>Aluminum ; Compression tests ; Creep strength ; Glass ceramics ; High temperature ; High-temperature creep behavior ; Hot pressing ; Liquid phase sintering ; Liquid phases ; Lutetium ; Magnesium ; Polymer-derived ceramics ; Pyrolysis ; Rare earth elements ; Silicon oxycarbides ; SiLuOC glass ceramics ; Sintering aids</subject><ispartof>Journal of the Ceramic Society of Japan, 2016/10/01, Vol.124(10), pp.1006-1012</ispartof><rights>2016 The Ceramic Society of Japan</rights><rights>Copyright Japan Science and Technology Agency 2016</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c534t-e700845958b727fa426aace8e3d6e064033c017f2fe53a0511e1dc6c1024eebf3</citedby><cites>FETCH-LOGICAL-c534t-e700845958b727fa426aace8e3d6e064033c017f2fe53a0511e1dc6c1024eebf3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,1883,27924,27925</link.rule.ids></links><search><creatorcontrib>STABLER, Christina</creatorcontrib><creatorcontrib>SEEMÜLLER, Christoph</creatorcontrib><creatorcontrib>CHOUDHARY, Ahmad</creatorcontrib><creatorcontrib>HEILMAIER, Martin</creatorcontrib><creatorcontrib>LAUTERBACH, Stefan</creatorcontrib><creatorcontrib>KLEEBE, Hans-Joachim</creatorcontrib><creatorcontrib>IONESCU, Emanuel</creatorcontrib><title>Synthesis and high-temperature creep behavior of a SiLuOC-based glass-ceramic</title><title>Journal of the Ceramic Society of Japan</title><addtitle>J. Ceram. Soc. Japan</addtitle><description>In this work, a lutetium-modified silicon oxycarbide (SiOC) glass ceramic was prepared from a single-source precursor via pyrolysis and subsequent hot pressing. It is shown that the main crystalline phase in the hot-pressed SiLuOC is Lu2Si2O7. The high-temperature (HT) creep behavior of SiLuOC was assessed by compression creep experiments performed between 1100 and 1300°C at constant true stresses between 25 and 75 MPa. The calculated viscosity values of SiLuOC were found to be significantly higher as compared to those of SiRE(Al,Mg)ON glasses (RE = rare earth elements). Thus, the presented SiLuOC-based glasses might be used as alternative sintering aids for the liquid-phase sintering of HT creep resistant Si3N4 monolithic samples.</description><subject>Aluminum</subject><subject>Compression tests</subject><subject>Creep strength</subject><subject>Glass ceramics</subject><subject>High temperature</subject><subject>High-temperature creep behavior</subject><subject>Hot pressing</subject><subject>Liquid phase sintering</subject><subject>Liquid phases</subject><subject>Lutetium</subject><subject>Magnesium</subject><subject>Polymer-derived ceramics</subject><subject>Pyrolysis</subject><subject>Rare earth elements</subject><subject>Silicon oxycarbides</subject><subject>SiLuOC glass ceramics</subject><subject>Sintering aids</subject><issn>1882-0743</issn><issn>1348-6535</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNpFkDtPwzAUhS0EElXpyG6J2cXPxBlRRQGpqENhthznpnHUJsFOkPrvSR8q07nDd8-RPoQeGZ1zRrPn2kGINZ-zhFF2gyZMSE0SJdTteGvNCU2luEezGH1OuUpkxpmeoM_NoekriD5i2xS48tuK9LDvINh-CIBdAOhwDpX99W3AbYkt3vjVsF6Q3EYo8HZnYyTjuN1794DuSruLMLvkFH0vX78W72S1fvtYvKyIU0L2BFJKtVSZ0nnK09JKnljrQIMoEqCJpEI4ytKSl6CEpYoxYIVLHKNcAuSlmKKnc28X2p8BYm_qdgjNOGk4F1xlqdRipMiZcqGNMUBpuuD3NhwMo-YozVykmZO0kV-e-Tr2dgtX2obeux3801weG05xfLwCrrLBQCP-ACLueLk</recordid><startdate>20160101</startdate><enddate>20160101</enddate><creator>STABLER, Christina</creator><creator>SEEMÜLLER, Christoph</creator><creator>CHOUDHARY, Ahmad</creator><creator>HEILMAIER, Martin</creator><creator>LAUTERBACH, Stefan</creator><creator>KLEEBE, Hans-Joachim</creator><creator>IONESCU, Emanuel</creator><general>The Ceramic Society of Japan</general><general>Japan Science and Technology Agency</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20160101</creationdate><title>Synthesis and high-temperature creep behavior of a SiLuOC-based glass-ceramic</title><author>STABLER, Christina ; SEEMÜLLER, Christoph ; CHOUDHARY, Ahmad ; HEILMAIER, Martin ; LAUTERBACH, Stefan ; KLEEBE, Hans-Joachim ; IONESCU, Emanuel</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c534t-e700845958b727fa426aace8e3d6e064033c017f2fe53a0511e1dc6c1024eebf3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng ; jpn</language><creationdate>2016</creationdate><topic>Aluminum</topic><topic>Compression tests</topic><topic>Creep strength</topic><topic>Glass ceramics</topic><topic>High temperature</topic><topic>High-temperature creep behavior</topic><topic>Hot pressing</topic><topic>Liquid phase sintering</topic><topic>Liquid phases</topic><topic>Lutetium</topic><topic>Magnesium</topic><topic>Polymer-derived ceramics</topic><topic>Pyrolysis</topic><topic>Rare earth elements</topic><topic>Silicon oxycarbides</topic><topic>SiLuOC glass ceramics</topic><topic>Sintering aids</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>STABLER, Christina</creatorcontrib><creatorcontrib>SEEMÜLLER, Christoph</creatorcontrib><creatorcontrib>CHOUDHARY, Ahmad</creatorcontrib><creatorcontrib>HEILMAIER, Martin</creatorcontrib><creatorcontrib>LAUTERBACH, Stefan</creatorcontrib><creatorcontrib>KLEEBE, Hans-Joachim</creatorcontrib><creatorcontrib>IONESCU, Emanuel</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of the Ceramic Society of Japan</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>STABLER, Christina</au><au>SEEMÜLLER, Christoph</au><au>CHOUDHARY, Ahmad</au><au>HEILMAIER, Martin</au><au>LAUTERBACH, Stefan</au><au>KLEEBE, Hans-Joachim</au><au>IONESCU, Emanuel</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and high-temperature creep behavior of a SiLuOC-based glass-ceramic</atitle><jtitle>Journal of the Ceramic Society of Japan</jtitle><addtitle>J. Ceram. Soc. Japan</addtitle><date>2016-01-01</date><risdate>2016</risdate><volume>124</volume><issue>10</issue><spage>1006</spage><epage>1012</epage><pages>1006-1012</pages><issn>1882-0743</issn><eissn>1348-6535</eissn><abstract>In this work, a lutetium-modified silicon oxycarbide (SiOC) glass ceramic was prepared from a single-source precursor via pyrolysis and subsequent hot pressing. It is shown that the main crystalline phase in the hot-pressed SiLuOC is Lu2Si2O7. The high-temperature (HT) creep behavior of SiLuOC was assessed by compression creep experiments performed between 1100 and 1300°C at constant true stresses between 25 and 75 MPa. The calculated viscosity values of SiLuOC were found to be significantly higher as compared to those of SiRE(Al,Mg)ON glasses (RE = rare earth elements). Thus, the presented SiLuOC-based glasses might be used as alternative sintering aids for the liquid-phase sintering of HT creep resistant Si3N4 monolithic samples.</abstract><cop>Tokyo</cop><pub>The Ceramic Society of Japan</pub><doi>10.2109/jcersj2.16101</doi><tpages>7</tpages><oa>free_for_read</oa></addata></record> |
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| issn | 1882-0743 1348-6535 |
| language | eng ; jpn |
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| source | J-STAGE Free |
| subjects | Aluminum Compression tests Creep strength Glass ceramics High temperature High-temperature creep behavior Hot pressing Liquid phase sintering Liquid phases Lutetium Magnesium Polymer-derived ceramics Pyrolysis Rare earth elements Silicon oxycarbides SiLuOC glass ceramics Sintering aids |
| title | Synthesis and high-temperature creep behavior of a SiLuOC-based glass-ceramic |
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