Optimization of Microwave-Assisted Extraction of Essential Oil from Vietnamese Basil (Ocimum basilicum L.) Using Response Surface Methodology
Basil plant is a common source for linalool and estragole. However, it has been showed that the chemical composition of basil varies considerably depending on many factors including method of extraction, cultivar of the plant or geographical location. In this study, we attempted to extract essential...
Gespeichert in:
| Veröffentlicht in: | Processes 2018-11, Vol.6 (11), p.206 |
|---|---|
| Hauptverfasser: | , , , , , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | |
|---|---|
| container_issue | 11 |
| container_start_page | 206 |
| container_title | Processes |
| container_volume | 6 |
| creator | Tran, Thien Hien Nguyen, Huynh Huu Hao Nguyen, Duy Chinh Nguyen, Thanh Quang Tan, Huynh Nhan, Le Thi Hong Nguyen, Dai Hai Tran, Lam Dai Do, Sy Trung Nguyen, Trinh Duy |
| description | Basil plant is a common source for linalool and estragole. However, it has been showed that the chemical composition of basil varies considerably depending on many factors including method of extraction, cultivar of the plant or geographical location. In this study, we attempted to extract essential oil from Vietnamese basil and analyze the chemical composition of the obtained oil using gas chromatography–mass spectrometry (GC-MS). The extraction method of choice was microwave-assisted hydro-distillation (MAHD) and the process was optimized with Response Surface Methodology (RSM) with regard to four experimental parameters including raw material size, raw material to water ratio, extraction time and microwave power. The results showed that ground basil leaves, when extracted with optimal conditions of water-to-material ratio of 3.2:1, extraction time of 97 (min) and microwave power of 430 (W), gave the actual essential oil yield of 0.6%. Regarding ANOVA results of the quadratic model, high determination coefficient (R2 = 0.9077), significant F-value of 10.92 and the p-value of less than 0.05 indicate that this model is significant between experimental and predicted variables, and should be fixed. In addition, GC-MS analysis revealed that major components of Vietnamese Basil were Estragole (87.869%), α-Bergamotene (2.922%), τ-Cadinol (2.770%), and Linalool (1.347%). |
| doi_str_mv | 10.3390/pr6110206 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2228746201</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2228746201</sourcerecordid><originalsourceid>FETCH-LOGICAL-c292t-2b946fdc81b9fb3a91d29eec9a9b45ce3441e1443044a43ca21407d19fe4e2043</originalsourceid><addsrcrecordid>eNpNkE1Lw0AQhoMoWGoP_oMFL_aQul9Nusda6ge0BNR6DZvNbN3SZOPuRq3_wf9sSlWcy7wzPMzAE0XnBI8YE_iqcQkhmOLkKOpRStNYpCQ9_pdPo4H3G9yVIGwyTnrRV9YEU5lPGYytkdVoaZSz7_IN4qn3xgco0fwjOKl-gbn3UAcjtygzW6SdrdCzgVDLCjyga-m77WWmTNVWqNhPRnVpMRqilTf1Gj2Ab2zdoY-t01IBWkJ4saXd2vXuLDrRcuth8NP70epm_jS7ixfZ7f1suogVFTTEtBA80aWakELogklBSioAlJCi4GMFjHMChHOGOZecKUkJx2lJhAYOFHPWjy4OdxtnX1vwId_Y1tXdy7xzNUl5QjHpqOGB6ox470DnjTOVdLuc4HwvPP8Tzr4BHud0Og</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2228746201</pqid></control><display><type>article</type><title>Optimization of Microwave-Assisted Extraction of Essential Oil from Vietnamese Basil (Ocimum basilicum L.) Using Response Surface Methodology</title><source>MDPI - Multidisciplinary Digital Publishing Institute</source><source>EZB-FREE-00999 freely available EZB journals</source><creator>Tran, Thien Hien ; Nguyen, Huynh Huu Hao ; Nguyen, Duy Chinh ; Nguyen, Thanh Quang ; Tan, Huynh ; Nhan, Le Thi Hong ; Nguyen, Dai Hai ; Tran, Lam Dai ; Do, Sy Trung ; Nguyen, Trinh Duy</creator><creatorcontrib>Tran, Thien Hien ; Nguyen, Huynh Huu Hao ; Nguyen, Duy Chinh ; Nguyen, Thanh Quang ; Tan, Huynh ; Nhan, Le Thi Hong ; Nguyen, Dai Hai ; Tran, Lam Dai ; Do, Sy Trung ; Nguyen, Trinh Duy</creatorcontrib><description>Basil plant is a common source for linalool and estragole. However, it has been showed that the chemical composition of basil varies considerably depending on many factors including method of extraction, cultivar of the plant or geographical location. In this study, we attempted to extract essential oil from Vietnamese basil and analyze the chemical composition of the obtained oil using gas chromatography–mass spectrometry (GC-MS). The extraction method of choice was microwave-assisted hydro-distillation (MAHD) and the process was optimized with Response Surface Methodology (RSM) with regard to four experimental parameters including raw material size, raw material to water ratio, extraction time and microwave power. The results showed that ground basil leaves, when extracted with optimal conditions of water-to-material ratio of 3.2:1, extraction time of 97 (min) and microwave power of 430 (W), gave the actual essential oil yield of 0.6%. Regarding ANOVA results of the quadratic model, high determination coefficient (R2 = 0.9077), significant F-value of 10.92 and the p-value of less than 0.05 indicate that this model is significant between experimental and predicted variables, and should be fixed. In addition, GC-MS analysis revealed that major components of Vietnamese Basil were Estragole (87.869%), α-Bergamotene (2.922%), τ-Cadinol (2.770%), and Linalool (1.347%).</description><identifier>ISSN: 2227-9717</identifier><identifier>EISSN: 2227-9717</identifier><identifier>DOI: 10.3390/pr6110206</identifier><language>eng</language><publisher>Basel: MDPI AG</publisher><subject>Activated carbon ; Cadinol ; Chemical composition ; Chemistry ; Cultivars ; Distillation ; Essential oils ; Food ; Gas chromatography ; Geographical distribution ; Geographical locations ; Leaves ; Linalool ; Mass spectrometry ; Mass spectroscopy ; Methods ; Microwaves ; Ocimum basilicum ; Oils & fats ; Optimization ; Organic chemistry ; Plant extracts ; Response surface methodology ; Science ; Studies ; Sugarcane</subject><ispartof>Processes, 2018-11, Vol.6 (11), p.206</ispartof><rights>2018. This work is licensed under https://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c292t-2b946fdc81b9fb3a91d29eec9a9b45ce3441e1443044a43ca21407d19fe4e2043</citedby><cites>FETCH-LOGICAL-c292t-2b946fdc81b9fb3a91d29eec9a9b45ce3441e1443044a43ca21407d19fe4e2043</cites><orcidid>0000-0003-3501-7390 ; 0000-0002-9157-9358 ; 0000-0002-9353-6132 ; 0000-0002-7241-1488 ; 0000-0003-1364-8001</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27903,27904</link.rule.ids></links><search><creatorcontrib>Tran, Thien Hien</creatorcontrib><creatorcontrib>Nguyen, Huynh Huu Hao</creatorcontrib><creatorcontrib>Nguyen, Duy Chinh</creatorcontrib><creatorcontrib>Nguyen, Thanh Quang</creatorcontrib><creatorcontrib>Tan, Huynh</creatorcontrib><creatorcontrib>Nhan, Le Thi Hong</creatorcontrib><creatorcontrib>Nguyen, Dai Hai</creatorcontrib><creatorcontrib>Tran, Lam Dai</creatorcontrib><creatorcontrib>Do, Sy Trung</creatorcontrib><creatorcontrib>Nguyen, Trinh Duy</creatorcontrib><title>Optimization of Microwave-Assisted Extraction of Essential Oil from Vietnamese Basil (Ocimum basilicum L.) Using Response Surface Methodology</title><title>Processes</title><description>Basil plant is a common source for linalool and estragole. However, it has been showed that the chemical composition of basil varies considerably depending on many factors including method of extraction, cultivar of the plant or geographical location. In this study, we attempted to extract essential oil from Vietnamese basil and analyze the chemical composition of the obtained oil using gas chromatography–mass spectrometry (GC-MS). The extraction method of choice was microwave-assisted hydro-distillation (MAHD) and the process was optimized with Response Surface Methodology (RSM) with regard to four experimental parameters including raw material size, raw material to water ratio, extraction time and microwave power. The results showed that ground basil leaves, when extracted with optimal conditions of water-to-material ratio of 3.2:1, extraction time of 97 (min) and microwave power of 430 (W), gave the actual essential oil yield of 0.6%. Regarding ANOVA results of the quadratic model, high determination coefficient (R2 = 0.9077), significant F-value of 10.92 and the p-value of less than 0.05 indicate that this model is significant between experimental and predicted variables, and should be fixed. In addition, GC-MS analysis revealed that major components of Vietnamese Basil were Estragole (87.869%), α-Bergamotene (2.922%), τ-Cadinol (2.770%), and Linalool (1.347%).</description><subject>Activated carbon</subject><subject>Cadinol</subject><subject>Chemical composition</subject><subject>Chemistry</subject><subject>Cultivars</subject><subject>Distillation</subject><subject>Essential oils</subject><subject>Food</subject><subject>Gas chromatography</subject><subject>Geographical distribution</subject><subject>Geographical locations</subject><subject>Leaves</subject><subject>Linalool</subject><subject>Mass spectrometry</subject><subject>Mass spectroscopy</subject><subject>Methods</subject><subject>Microwaves</subject><subject>Ocimum basilicum</subject><subject>Oils & fats</subject><subject>Optimization</subject><subject>Organic chemistry</subject><subject>Plant extracts</subject><subject>Response surface methodology</subject><subject>Science</subject><subject>Studies</subject><subject>Sugarcane</subject><issn>2227-9717</issn><issn>2227-9717</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNpNkE1Lw0AQhoMoWGoP_oMFL_aQul9Nusda6ge0BNR6DZvNbN3SZOPuRq3_wf9sSlWcy7wzPMzAE0XnBI8YE_iqcQkhmOLkKOpRStNYpCQ9_pdPo4H3G9yVIGwyTnrRV9YEU5lPGYytkdVoaZSz7_IN4qn3xgco0fwjOKl-gbn3UAcjtygzW6SdrdCzgVDLCjyga-m77WWmTNVWqNhPRnVpMRqilTf1Gj2Ab2zdoY-t01IBWkJ4saXd2vXuLDrRcuth8NP70epm_jS7ixfZ7f1suogVFTTEtBA80aWakELogklBSioAlJCi4GMFjHMChHOGOZecKUkJx2lJhAYOFHPWjy4OdxtnX1vwId_Y1tXdy7xzNUl5QjHpqOGB6ox470DnjTOVdLuc4HwvPP8Tzr4BHud0Og</recordid><startdate>20181101</startdate><enddate>20181101</enddate><creator>Tran, Thien Hien</creator><creator>Nguyen, Huynh Huu Hao</creator><creator>Nguyen, Duy Chinh</creator><creator>Nguyen, Thanh Quang</creator><creator>Tan, Huynh</creator><creator>Nhan, Le Thi Hong</creator><creator>Nguyen, Dai Hai</creator><creator>Tran, Lam Dai</creator><creator>Do, Sy Trung</creator><creator>Nguyen, Trinh Duy</creator><general>MDPI AG</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FH</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BBNVY</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>LK8</scope><scope>M7P</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><orcidid>https://orcid.org/0000-0003-3501-7390</orcidid><orcidid>https://orcid.org/0000-0002-9157-9358</orcidid><orcidid>https://orcid.org/0000-0002-9353-6132</orcidid><orcidid>https://orcid.org/0000-0002-7241-1488</orcidid><orcidid>https://orcid.org/0000-0003-1364-8001</orcidid></search><sort><creationdate>20181101</creationdate><title>Optimization of Microwave-Assisted Extraction of Essential Oil from Vietnamese Basil (Ocimum basilicum L.) Using Response Surface Methodology</title><author>Tran, Thien Hien ; Nguyen, Huynh Huu Hao ; Nguyen, Duy Chinh ; Nguyen, Thanh Quang ; Tan, Huynh ; Nhan, Le Thi Hong ; Nguyen, Dai Hai ; Tran, Lam Dai ; Do, Sy Trung ; Nguyen, Trinh Duy</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c292t-2b946fdc81b9fb3a91d29eec9a9b45ce3441e1443044a43ca21407d19fe4e2043</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Activated carbon</topic><topic>Cadinol</topic><topic>Chemical composition</topic><topic>Chemistry</topic><topic>Cultivars</topic><topic>Distillation</topic><topic>Essential oils</topic><topic>Food</topic><topic>Gas chromatography</topic><topic>Geographical distribution</topic><topic>Geographical locations</topic><topic>Leaves</topic><topic>Linalool</topic><topic>Mass spectrometry</topic><topic>Mass spectroscopy</topic><topic>Methods</topic><topic>Microwaves</topic><topic>Ocimum basilicum</topic><topic>Oils & fats</topic><topic>Optimization</topic><topic>Organic chemistry</topic><topic>Plant extracts</topic><topic>Response surface methodology</topic><topic>Science</topic><topic>Studies</topic><topic>Sugarcane</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Tran, Thien Hien</creatorcontrib><creatorcontrib>Nguyen, Huynh Huu Hao</creatorcontrib><creatorcontrib>Nguyen, Duy Chinh</creatorcontrib><creatorcontrib>Nguyen, Thanh Quang</creatorcontrib><creatorcontrib>Tan, Huynh</creatorcontrib><creatorcontrib>Nhan, Le Thi Hong</creatorcontrib><creatorcontrib>Nguyen, Dai Hai</creatorcontrib><creatorcontrib>Tran, Lam Dai</creatorcontrib><creatorcontrib>Do, Sy Trung</creatorcontrib><creatorcontrib>Nguyen, Trinh Duy</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Natural Science Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>Biological Science Collection</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection (ProQuest)</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>ProQuest Biological Science Collection</collection><collection>Biological Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><jtitle>Processes</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Tran, Thien Hien</au><au>Nguyen, Huynh Huu Hao</au><au>Nguyen, Duy Chinh</au><au>Nguyen, Thanh Quang</au><au>Tan, Huynh</au><au>Nhan, Le Thi Hong</au><au>Nguyen, Dai Hai</au><au>Tran, Lam Dai</au><au>Do, Sy Trung</au><au>Nguyen, Trinh Duy</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Optimization of Microwave-Assisted Extraction of Essential Oil from Vietnamese Basil (Ocimum basilicum L.) Using Response Surface Methodology</atitle><jtitle>Processes</jtitle><date>2018-11-01</date><risdate>2018</risdate><volume>6</volume><issue>11</issue><spage>206</spage><pages>206-</pages><issn>2227-9717</issn><eissn>2227-9717</eissn><abstract>Basil plant is a common source for linalool and estragole. However, it has been showed that the chemical composition of basil varies considerably depending on many factors including method of extraction, cultivar of the plant or geographical location. In this study, we attempted to extract essential oil from Vietnamese basil and analyze the chemical composition of the obtained oil using gas chromatography–mass spectrometry (GC-MS). The extraction method of choice was microwave-assisted hydro-distillation (MAHD) and the process was optimized with Response Surface Methodology (RSM) with regard to four experimental parameters including raw material size, raw material to water ratio, extraction time and microwave power. The results showed that ground basil leaves, when extracted with optimal conditions of water-to-material ratio of 3.2:1, extraction time of 97 (min) and microwave power of 430 (W), gave the actual essential oil yield of 0.6%. Regarding ANOVA results of the quadratic model, high determination coefficient (R2 = 0.9077), significant F-value of 10.92 and the p-value of less than 0.05 indicate that this model is significant between experimental and predicted variables, and should be fixed. In addition, GC-MS analysis revealed that major components of Vietnamese Basil were Estragole (87.869%), α-Bergamotene (2.922%), τ-Cadinol (2.770%), and Linalool (1.347%).</abstract><cop>Basel</cop><pub>MDPI AG</pub><doi>10.3390/pr6110206</doi><orcidid>https://orcid.org/0000-0003-3501-7390</orcidid><orcidid>https://orcid.org/0000-0002-9157-9358</orcidid><orcidid>https://orcid.org/0000-0002-9353-6132</orcidid><orcidid>https://orcid.org/0000-0002-7241-1488</orcidid><orcidid>https://orcid.org/0000-0003-1364-8001</orcidid><oa>free_for_read</oa></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 2227-9717 |
| ispartof | Processes, 2018-11, Vol.6 (11), p.206 |
| issn | 2227-9717 2227-9717 |
| language | eng |
| recordid | cdi_proquest_journals_2228746201 |
| source | MDPI - Multidisciplinary Digital Publishing Institute; EZB-FREE-00999 freely available EZB journals |
| subjects | Activated carbon Cadinol Chemical composition Chemistry Cultivars Distillation Essential oils Food Gas chromatography Geographical distribution Geographical locations Leaves Linalool Mass spectrometry Mass spectroscopy Methods Microwaves Ocimum basilicum Oils & fats Optimization Organic chemistry Plant extracts Response surface methodology Science Studies Sugarcane |
| title | Optimization of Microwave-Assisted Extraction of Essential Oil from Vietnamese Basil (Ocimum basilicum L.) Using Response Surface Methodology |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-24T14%3A22%3A12IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Optimization%20of%20Microwave-Assisted%20Extraction%20of%20Essential%20Oil%20from%20Vietnamese%20Basil%20(Ocimum%20basilicum%20L.)%20Using%20Response%20Surface%20Methodology&rft.jtitle=Processes&rft.au=Tran,%20Thien%20Hien&rft.date=2018-11-01&rft.volume=6&rft.issue=11&rft.spage=206&rft.pages=206-&rft.issn=2227-9717&rft.eissn=2227-9717&rft_id=info:doi/10.3390/pr6110206&rft_dat=%3Cproquest_cross%3E2228746201%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2228746201&rft_id=info:pmid/&rfr_iscdi=true |