Synthesis and Properties of [4-(Diethylamino)phenyl]dichlorophosphine

[4-(Diethylamino)phenyl]dichlorophosphine synthesized for the first time has reacted with trialkyl orthoformate and ethylene oxide in the presence of ethyl chloroacetate with the formation of phosphorylated formals and ethyl [4-(diethylamino)phenyl](2-chloroethoxy)phosphonyl acetate, a precursor of...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Russian journal of general chemistry 2019, Vol.89 (1), p.63-66
Hauptverfasser: Gazizov, M. B., Ibragimov, Sh. N., Khairullina, O. D., Ivanova, S. Yu, Gazizova, K. S., Khairullin, R. A., Kirillina, Yu. S., Pistsova, A. L.
Format: Artikel
Sprache:eng
Schlagworte:
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page 66
container_issue 1
container_start_page 63
container_title Russian journal of general chemistry
container_volume 89
creator Gazizov, M. B.
Ibragimov, Sh. N.
Khairullina, O. D.
Ivanova, S. Yu
Gazizova, K. S.
Khairullin, R. A.
Kirillina, Yu. S.
Pistsova, A. L.
description [4-(Diethylamino)phenyl]dichlorophosphine synthesized for the first time has reacted with trialkyl orthoformate and ethylene oxide in the presence of ethyl chloroacetate with the formation of phosphorylated formals and ethyl [4-(diethylamino)phenyl](2-chloroethoxy)phosphonyl acetate, a precursor of a new analog of nootropic drug KAPAKh.
doi_str_mv 10.1134/S1070363219010110
format Article
fullrecord <record><control><sourceid>gale_proqu</sourceid><recordid>TN_cdi_proquest_journals_2202474879</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><galeid>A727024813</galeid><sourcerecordid>A727024813</sourcerecordid><originalsourceid>FETCH-LOGICAL-c307t-79716ebc9f373d0894361e518fb12f82c44dd3882f9216fea5f5d6e6471c3efe3</originalsourceid><addsrcrecordid>eNp1kM9LwzAUx4soOKd_gLeCFz105iVtkh7HnD9AUJieRErXvqwZXVKT7tD_3owKHkRyeCHfz-fl8aLoEsgMgKW3KyCCMM4o5AQIADmKJsCJTBjLyHG4hzg55KfRmfdbEiDC6SRargbTN-i1j0tTx6_Oduh6jT62Kv5Ik-s7jX0ztOVOG3vTNWiG9rPWVdPagDbWd402eB6dqLL1ePFTp9H7_fJt8Zg8vzw8LebPScWI6BORC-C4rnLFBKuJzFPGATOQag1USVqlaV0zKanKKXCFZaaymiNPBVQMFbJpdDX27Zz92qPvi63dOxO-LCglNBWpFHmgZiO1KVsstFG2d2UVTo07XVmDSof3uaAiKBJYEGAUKme9d6iKzuld6YYCSHFYb_FnvcGho-MDazbofkf5X_oGDkx67Q</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2202474879</pqid></control><display><type>article</type><title>Synthesis and Properties of [4-(Diethylamino)phenyl]dichlorophosphine</title><source>SpringerLink Journals - AutoHoldings</source><creator>Gazizov, M. B. ; Ibragimov, Sh. N. ; Khairullina, O. D. ; Ivanova, S. Yu ; Gazizova, K. S. ; Khairullin, R. A. ; Kirillina, Yu. S. ; Pistsova, A. L.</creator><creatorcontrib>Gazizov, M. B. ; Ibragimov, Sh. N. ; Khairullina, O. D. ; Ivanova, S. Yu ; Gazizova, K. S. ; Khairullin, R. A. ; Kirillina, Yu. S. ; Pistsova, A. L.</creatorcontrib><description>[4-(Diethylamino)phenyl]dichlorophosphine synthesized for the first time has reacted with trialkyl orthoformate and ethylene oxide in the presence of ethyl chloroacetate with the formation of phosphorylated formals and ethyl [4-(diethylamino)phenyl](2-chloroethoxy)phosphonyl acetate, a precursor of a new analog of nootropic drug KAPAKh.</description><identifier>ISSN: 1070-3632</identifier><identifier>EISSN: 1608-3350</identifier><identifier>DOI: 10.1134/S1070363219010110</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Chemistry ; Chemistry and Materials Science ; Chemistry/Food Science ; Ethylene oxide ; Nuclear magnetic resonance spectroscopy</subject><ispartof>Russian journal of general chemistry, 2019, Vol.89 (1), p.63-66</ispartof><rights>Pleiades Publishing, Ltd. 2019</rights><rights>COPYRIGHT 2019 Springer</rights><rights>Copyright Springer Nature B.V. 2019</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c307t-79716ebc9f373d0894361e518fb12f82c44dd3882f9216fea5f5d6e6471c3efe3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S1070363219010110$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S1070363219010110$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Gazizov, M. B.</creatorcontrib><creatorcontrib>Ibragimov, Sh. N.</creatorcontrib><creatorcontrib>Khairullina, O. D.</creatorcontrib><creatorcontrib>Ivanova, S. Yu</creatorcontrib><creatorcontrib>Gazizova, K. S.</creatorcontrib><creatorcontrib>Khairullin, R. A.</creatorcontrib><creatorcontrib>Kirillina, Yu. S.</creatorcontrib><creatorcontrib>Pistsova, A. L.</creatorcontrib><title>Synthesis and Properties of [4-(Diethylamino)phenyl]dichlorophosphine</title><title>Russian journal of general chemistry</title><addtitle>Russ J Gen Chem</addtitle><description>[4-(Diethylamino)phenyl]dichlorophosphine synthesized for the first time has reacted with trialkyl orthoformate and ethylene oxide in the presence of ethyl chloroacetate with the formation of phosphorylated formals and ethyl [4-(diethylamino)phenyl](2-chloroethoxy)phosphonyl acetate, a precursor of a new analog of nootropic drug KAPAKh.</description><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry/Food Science</subject><subject>Ethylene oxide</subject><subject>Nuclear magnetic resonance spectroscopy</subject><issn>1070-3632</issn><issn>1608-3350</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2019</creationdate><recordtype>article</recordtype><recordid>eNp1kM9LwzAUx4soOKd_gLeCFz105iVtkh7HnD9AUJieRErXvqwZXVKT7tD_3owKHkRyeCHfz-fl8aLoEsgMgKW3KyCCMM4o5AQIADmKJsCJTBjLyHG4hzg55KfRmfdbEiDC6SRargbTN-i1j0tTx6_Oduh6jT62Kv5Ik-s7jX0ztOVOG3vTNWiG9rPWVdPagDbWd402eB6dqLL1ePFTp9H7_fJt8Zg8vzw8LebPScWI6BORC-C4rnLFBKuJzFPGATOQag1USVqlaV0zKanKKXCFZaaymiNPBVQMFbJpdDX27Zz92qPvi63dOxO-LCglNBWpFHmgZiO1KVsstFG2d2UVTo07XVmDSof3uaAiKBJYEGAUKme9d6iKzuld6YYCSHFYb_FnvcGho-MDazbofkf5X_oGDkx67Q</recordid><startdate>2019</startdate><enddate>2019</enddate><creator>Gazizov, M. B.</creator><creator>Ibragimov, Sh. N.</creator><creator>Khairullina, O. D.</creator><creator>Ivanova, S. Yu</creator><creator>Gazizova, K. S.</creator><creator>Khairullin, R. A.</creator><creator>Kirillina, Yu. S.</creator><creator>Pistsova, A. L.</creator><general>Pleiades Publishing</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>2019</creationdate><title>Synthesis and Properties of [4-(Diethylamino)phenyl]dichlorophosphine</title><author>Gazizov, M. B. ; Ibragimov, Sh. N. ; Khairullina, O. D. ; Ivanova, S. Yu ; Gazizova, K. S. ; Khairullin, R. A. ; Kirillina, Yu. S. ; Pistsova, A. L.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c307t-79716ebc9f373d0894361e518fb12f82c44dd3882f9216fea5f5d6e6471c3efe3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2019</creationdate><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chemistry/Food Science</topic><topic>Ethylene oxide</topic><topic>Nuclear magnetic resonance spectroscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Gazizov, M. B.</creatorcontrib><creatorcontrib>Ibragimov, Sh. N.</creatorcontrib><creatorcontrib>Khairullina, O. D.</creatorcontrib><creatorcontrib>Ivanova, S. Yu</creatorcontrib><creatorcontrib>Gazizova, K. S.</creatorcontrib><creatorcontrib>Khairullin, R. A.</creatorcontrib><creatorcontrib>Kirillina, Yu. S.</creatorcontrib><creatorcontrib>Pistsova, A. L.</creatorcontrib><collection>CrossRef</collection><jtitle>Russian journal of general chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Gazizov, M. B.</au><au>Ibragimov, Sh. N.</au><au>Khairullina, O. D.</au><au>Ivanova, S. Yu</au><au>Gazizova, K. S.</au><au>Khairullin, R. A.</au><au>Kirillina, Yu. S.</au><au>Pistsova, A. L.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and Properties of [4-(Diethylamino)phenyl]dichlorophosphine</atitle><jtitle>Russian journal of general chemistry</jtitle><stitle>Russ J Gen Chem</stitle><date>2019</date><risdate>2019</risdate><volume>89</volume><issue>1</issue><spage>63</spage><epage>66</epage><pages>63-66</pages><issn>1070-3632</issn><eissn>1608-3350</eissn><abstract>[4-(Diethylamino)phenyl]dichlorophosphine synthesized for the first time has reacted with trialkyl orthoformate and ethylene oxide in the presence of ethyl chloroacetate with the formation of phosphorylated formals and ethyl [4-(diethylamino)phenyl](2-chloroethoxy)phosphonyl acetate, a precursor of a new analog of nootropic drug KAPAKh.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S1070363219010110</doi><tpages>4</tpages></addata></record>
fulltext fulltext
identifier ISSN: 1070-3632
ispartof Russian journal of general chemistry, 2019, Vol.89 (1), p.63-66
issn 1070-3632
1608-3350
language eng
recordid cdi_proquest_journals_2202474879
source SpringerLink Journals - AutoHoldings
subjects Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Ethylene oxide
Nuclear magnetic resonance spectroscopy
title Synthesis and Properties of [4-(Diethylamino)phenyl]dichlorophosphine
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-08T02%3A33%3A28IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-gale_proqu&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Synthesis%20and%20Properties%20of%20%5B4-(Diethylamino)phenyl%5Ddichlorophosphine&rft.jtitle=Russian%20journal%20of%20general%20chemistry&rft.au=Gazizov,%20M.%20B.&rft.date=2019&rft.volume=89&rft.issue=1&rft.spage=63&rft.epage=66&rft.pages=63-66&rft.issn=1070-3632&rft.eissn=1608-3350&rft_id=info:doi/10.1134/S1070363219010110&rft_dat=%3Cgale_proqu%3EA727024813%3C/gale_proqu%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2202474879&rft_id=info:pmid/&rft_galeid=A727024813&rfr_iscdi=true