Spark plasma sintering of zirconia/nano-nickel composites
This work describes a whole processing route for obtaining dense and nanostructured zirconia-nickel composites with low contents of metallic phase (1–3.5 vol%). For the processing route, a combination of spray-freezing and lyophilization has been proposed. After the calcination and reduction of the...
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| Veröffentlicht in: | Mechanics & industry : an international journal on mechanical sciences and engineering applications 2015, Vol.16 (Supplement), p.703 |
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| container_title | Mechanics & industry : an international journal on mechanical sciences and engineering applications |
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| creator | Gutierrez-Gonzalez, Carlos F. Solis Pinargote, Nestor W. Agouram, Said Peretyagin, Pavel Y. Lopez-Esteban, Sonia Torrecillas, Ramon |
| description | This work describes a whole processing route for obtaining dense and nanostructured zirconia-nickel composites with low contents of metallic phase (1–3.5 vol%). For the processing route, a combination of spray-freezing and lyophilization has been proposed. After the calcination and reduction of the resulting powders an X-ray and HRTEM characterization has been performed. This showed the formation of pure zirconia and nickel, well dispersed and homogeneously distributed, nanostructured phases. The obtained powders were subsequently sintered by Spark Plasma Sintering (SPS). As a result, dense ZrO2-Ni composites were obtained, revealing that the sizes of the metal particles were kept in the nanometer range and appear homogeneously and well dispersed into the ceramic matrix. The mechanical behavior of these materials was evaluated by means of the Vickers hardness, showing and increment of about 25% with respect to pure zirconia with only a Ni concentration of 1 vol%. |
| doi_str_mv | 10.1051/meca/2015090 |
| format | Article |
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For the processing route, a combination of spray-freezing and lyophilization has been proposed. After the calcination and reduction of the resulting powders an X-ray and HRTEM characterization has been performed. This showed the formation of pure zirconia and nickel, well dispersed and homogeneously distributed, nanostructured phases. The obtained powders were subsequently sintered by Spark Plasma Sintering (SPS). As a result, dense ZrO2-Ni composites were obtained, revealing that the sizes of the metal particles were kept in the nanometer range and appear homogeneously and well dispersed into the ceramic matrix. 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The mechanical behavior of these materials was evaluated by means of the Vickers hardness, showing and increment of about 25% with respect to pure zirconia with only a Ni concentration of 1 vol%.</description><subject>Composite materials</subject><subject>Diamond pyramid hardness</subject><subject>Freezing</subject><subject>Mechanical properties</subject><subject>Metal particles</subject><subject>nanoceramics</subject><subject>nanocomposites</subject><subject>nanomaterials</subject><subject>Nanostructure</subject><subject>Nickel</subject><subject>Plasma sintering</subject><subject>powder materials</subject><subject>Spark plasma sintering</subject><subject>zirconia-nickel composites</subject><subject>Zirconium dioxide</subject><issn>2257-7777</issn><issn>2257-7750</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2015</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNo9kEFLwzAYhoMoOOZu_oCCV-u-JE2THGWoEwceVBQv4VuaSra1qUkH6q-3Y2On9z08vC88hFxSuKEg6LRxFqcMqAANJ2TEmJC5lAJOj13KczJJaQUAtNS6KMoR0S8dxnXWbTA1mCXf9i769isLdfbnow2tx2mLbchbb9duk9nQdCH53qULclbjJrnJIcfk7f7udTbPF88Pj7PbRW45131eK7esNaiyUsxV2vJlBRXWSlC0qqoYoELJEW0hlRoqWA5lseQIArBgyMfkar_bxfC9dak3q7CN7XBpGNWaScXLYqCu95SNIaXoatNF32D8NRTMzo_Z-TEHPwOe73GfevdzZAcVppRcCqPg3TzpD1F-SmoY_weZFmdM</recordid><startdate>2015</startdate><enddate>2015</enddate><creator>Gutierrez-Gonzalez, Carlos F.</creator><creator>Solis Pinargote, Nestor W.</creator><creator>Agouram, Said</creator><creator>Peretyagin, Pavel Y.</creator><creator>Lopez-Esteban, Sonia</creator><creator>Torrecillas, Ramon</creator><general>EDP Sciences</general><scope>BSCLL</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7TB</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>FR3</scope><scope>HCIFZ</scope><scope>L6V</scope><scope>M7S</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><scope>S0W</scope></search><sort><creationdate>2015</creationdate><title>Spark plasma sintering of zirconia/nano-nickel composites</title><author>Gutierrez-Gonzalez, Carlos F. ; 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| ispartof | Mechanics & industry : an international journal on mechanical sciences and engineering applications, 2015, Vol.16 (Supplement), p.703 |
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| subjects | Composite materials Diamond pyramid hardness Freezing Mechanical properties Metal particles nanoceramics nanocomposites nanomaterials Nanostructure Nickel Plasma sintering powder materials Spark plasma sintering zirconia-nickel composites Zirconium dioxide |
| title | Spark plasma sintering of zirconia/nano-nickel composites |
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