Studies on the Structure and Catalytic Properties for Heck Reaction of Troxerutin Supported Palladium Catalyst
Troxerutin supported palladium (TXT-Pd) catalyst was prepared readily by using one-step synthetic method. As-fabricated TXT-Pd catalyst was evaluated by means of fourier transform infrared spectrometer (FTIR), atomic absorption spectroscope instrument (AAS), and X-ray photoelectron spectrum (XPS). A...
Gespeichert in:
| Veröffentlicht in: | Theoretical foundations of chemical engineering 2018-11, Vol.52 (6), p.1039-1044 |
|---|---|
| Hauptverfasser: | , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 1044 |
|---|---|
| container_issue | 6 |
| container_start_page | 1039 |
| container_title | Theoretical foundations of chemical engineering |
| container_volume | 52 |
| creator | Xu, Q. J. Zuo, C. S. Liu, D. Y. Shi, W. Z. |
| description | Troxerutin supported palladium (TXT-Pd) catalyst was prepared readily by using one-step synthetic method. As-fabricated TXT-Pd catalyst was evaluated by means of fourier transform infrared spectrometer (FTIR), atomic absorption spectroscope instrument (AAS), and X-ray photoelectron spectrum (XPS). As-prepared catalyst possessed perfect catalytic properties to the Heck reaction of aryl halide with vinyl compounds in N
2
atmosphere and the yields were up to above 95%. Particularly, the TXT-Pd catalyst could catalyze the Heck reaction of bromobenzene with low reaction activity and acrylic acid even at a low temperature 80°C even with a little amount of the catalyst. The remarkable interest was reusing properties, with which the yield was up to 36.7% after 7 times of the reusable catalyst. Moreover, TXT-Pd catalyst also showed high catalytic activity to the Heck reaction of substituted aryl halides with acrylic acid or styrene. |
| doi_str_mv | 10.1134/S0040579518060155 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2169320976</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2169320976</sourcerecordid><originalsourceid>FETCH-LOGICAL-c353t-e720e8ab246604c072111962fdb1eff493ed6cab8aea03a558f4db5594e948183</originalsourceid><addsrcrecordid>eNp1kM9LwzAYhoMoOKd_gLeA52rS_GhzlKFOGDjsPJc0_aKdXVOTFNx_b8sGHsTTd3if5_3gReiakltKGb8rCOFEZErQnEhChThBMypJnjDO6CmaTXEy5efoIoQtIURJqWaoK-JQNxCw63D8AFxEP5g4eMC6q_FCR93uY2Pw2rsefJxI6zxegvnEr6BNbEbRWbzx7hv8EJsOF0PfOx-hxmvdtrpuht2xKMRLdGZ1G-DqeOfo7fFhs1gmq5en58X9KjFMsJhAlhLIdZVyKQk3JEsppUqmtq4oWMsVg1oaXeUaNGFaiNzyuhJCcVA8pzmbo5tDb-_d1wAhlls3-G58WaZUKpYSlcmRogfKeBeCB1v2vtlpvy8pKadZyz-zjk56cMLIdu_gf5v_l34APu16dQ</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2169320976</pqid></control><display><type>article</type><title>Studies on the Structure and Catalytic Properties for Heck Reaction of Troxerutin Supported Palladium Catalyst</title><source>SpringerLink Journals - AutoHoldings</source><creator>Xu, Q. J. ; Zuo, C. S. ; Liu, D. Y. ; Shi, W. Z.</creator><creatorcontrib>Xu, Q. J. ; Zuo, C. S. ; Liu, D. Y. ; Shi, W. Z.</creatorcontrib><description>Troxerutin supported palladium (TXT-Pd) catalyst was prepared readily by using one-step synthetic method. As-fabricated TXT-Pd catalyst was evaluated by means of fourier transform infrared spectrometer (FTIR), atomic absorption spectroscope instrument (AAS), and X-ray photoelectron spectrum (XPS). As-prepared catalyst possessed perfect catalytic properties to the Heck reaction of aryl halide with vinyl compounds in N
2
atmosphere and the yields were up to above 95%. Particularly, the TXT-Pd catalyst could catalyze the Heck reaction of bromobenzene with low reaction activity and acrylic acid even at a low temperature 80°C even with a little amount of the catalyst. The remarkable interest was reusing properties, with which the yield was up to 36.7% after 7 times of the reusable catalyst. Moreover, TXT-Pd catalyst also showed high catalytic activity to the Heck reaction of substituted aryl halides with acrylic acid or styrene.</description><identifier>ISSN: 0040-5795</identifier><identifier>EISSN: 1608-3431</identifier><identifier>DOI: 10.1134/S0040579518060155</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Acrylic acid ; Acrylics ; Aromatic compounds ; Atomic absorption analysis ; Catalysis ; Catalysts ; Catalytic activity ; Chemistry ; Chemistry and Materials Science ; Fourier transforms ; FTIR spectrometers ; Halides ; Industrial Chemistry/Chemical Engineering ; Palladium ; Photoelectrons ; Properties (attributes) ; X ray photoelectron spectroscopy</subject><ispartof>Theoretical foundations of chemical engineering, 2018-11, Vol.52 (6), p.1039-1044</ispartof><rights>Pleiades Publishing, Ltd. 2018</rights><rights>Copyright Springer Science & Business Media 2018</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c353t-e720e8ab246604c072111962fdb1eff493ed6cab8aea03a558f4db5594e948183</citedby><cites>FETCH-LOGICAL-c353t-e720e8ab246604c072111962fdb1eff493ed6cab8aea03a558f4db5594e948183</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S0040579518060155$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S0040579518060155$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27903,27904,41467,42536,51297</link.rule.ids></links><search><creatorcontrib>Xu, Q. J.</creatorcontrib><creatorcontrib>Zuo, C. S.</creatorcontrib><creatorcontrib>Liu, D. Y.</creatorcontrib><creatorcontrib>Shi, W. Z.</creatorcontrib><title>Studies on the Structure and Catalytic Properties for Heck Reaction of Troxerutin Supported Palladium Catalyst</title><title>Theoretical foundations of chemical engineering</title><addtitle>Theor Found Chem Eng</addtitle><description>Troxerutin supported palladium (TXT-Pd) catalyst was prepared readily by using one-step synthetic method. As-fabricated TXT-Pd catalyst was evaluated by means of fourier transform infrared spectrometer (FTIR), atomic absorption spectroscope instrument (AAS), and X-ray photoelectron spectrum (XPS). As-prepared catalyst possessed perfect catalytic properties to the Heck reaction of aryl halide with vinyl compounds in N
2
atmosphere and the yields were up to above 95%. Particularly, the TXT-Pd catalyst could catalyze the Heck reaction of bromobenzene with low reaction activity and acrylic acid even at a low temperature 80°C even with a little amount of the catalyst. The remarkable interest was reusing properties, with which the yield was up to 36.7% after 7 times of the reusable catalyst. Moreover, TXT-Pd catalyst also showed high catalytic activity to the Heck reaction of substituted aryl halides with acrylic acid or styrene.</description><subject>Acrylic acid</subject><subject>Acrylics</subject><subject>Aromatic compounds</subject><subject>Atomic absorption analysis</subject><subject>Catalysis</subject><subject>Catalysts</subject><subject>Catalytic activity</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Fourier transforms</subject><subject>FTIR spectrometers</subject><subject>Halides</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Palladium</subject><subject>Photoelectrons</subject><subject>Properties (attributes)</subject><subject>X ray photoelectron spectroscopy</subject><issn>0040-5795</issn><issn>1608-3431</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNp1kM9LwzAYhoMoOKd_gLeA52rS_GhzlKFOGDjsPJc0_aKdXVOTFNx_b8sGHsTTd3if5_3gReiakltKGb8rCOFEZErQnEhChThBMypJnjDO6CmaTXEy5efoIoQtIURJqWaoK-JQNxCw63D8AFxEP5g4eMC6q_FCR93uY2Pw2rsefJxI6zxegvnEr6BNbEbRWbzx7hv8EJsOF0PfOx-hxmvdtrpuht2xKMRLdGZ1G-DqeOfo7fFhs1gmq5en58X9KjFMsJhAlhLIdZVyKQk3JEsppUqmtq4oWMsVg1oaXeUaNGFaiNzyuhJCcVA8pzmbo5tDb-_d1wAhlls3-G58WaZUKpYSlcmRogfKeBeCB1v2vtlpvy8pKadZyz-zjk56cMLIdu_gf5v_l34APu16dQ</recordid><startdate>20181101</startdate><enddate>20181101</enddate><creator>Xu, Q. J.</creator><creator>Zuo, C. S.</creator><creator>Liu, D. Y.</creator><creator>Shi, W. Z.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20181101</creationdate><title>Studies on the Structure and Catalytic Properties for Heck Reaction of Troxerutin Supported Palladium Catalyst</title><author>Xu, Q. J. ; Zuo, C. S. ; Liu, D. Y. ; Shi, W. Z.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c353t-e720e8ab246604c072111962fdb1eff493ed6cab8aea03a558f4db5594e948183</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Acrylic acid</topic><topic>Acrylics</topic><topic>Aromatic compounds</topic><topic>Atomic absorption analysis</topic><topic>Catalysis</topic><topic>Catalysts</topic><topic>Catalytic activity</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Fourier transforms</topic><topic>FTIR spectrometers</topic><topic>Halides</topic><topic>Industrial Chemistry/Chemical Engineering</topic><topic>Palladium</topic><topic>Photoelectrons</topic><topic>Properties (attributes)</topic><topic>X ray photoelectron spectroscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Xu, Q. J.</creatorcontrib><creatorcontrib>Zuo, C. S.</creatorcontrib><creatorcontrib>Liu, D. Y.</creatorcontrib><creatorcontrib>Shi, W. Z.</creatorcontrib><collection>CrossRef</collection><jtitle>Theoretical foundations of chemical engineering</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Xu, Q. J.</au><au>Zuo, C. S.</au><au>Liu, D. Y.</au><au>Shi, W. Z.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Studies on the Structure and Catalytic Properties for Heck Reaction of Troxerutin Supported Palladium Catalyst</atitle><jtitle>Theoretical foundations of chemical engineering</jtitle><stitle>Theor Found Chem Eng</stitle><date>2018-11-01</date><risdate>2018</risdate><volume>52</volume><issue>6</issue><spage>1039</spage><epage>1044</epage><pages>1039-1044</pages><issn>0040-5795</issn><eissn>1608-3431</eissn><abstract>Troxerutin supported palladium (TXT-Pd) catalyst was prepared readily by using one-step synthetic method. As-fabricated TXT-Pd catalyst was evaluated by means of fourier transform infrared spectrometer (FTIR), atomic absorption spectroscope instrument (AAS), and X-ray photoelectron spectrum (XPS). As-prepared catalyst possessed perfect catalytic properties to the Heck reaction of aryl halide with vinyl compounds in N
2
atmosphere and the yields were up to above 95%. Particularly, the TXT-Pd catalyst could catalyze the Heck reaction of bromobenzene with low reaction activity and acrylic acid even at a low temperature 80°C even with a little amount of the catalyst. The remarkable interest was reusing properties, with which the yield was up to 36.7% after 7 times of the reusable catalyst. Moreover, TXT-Pd catalyst also showed high catalytic activity to the Heck reaction of substituted aryl halides with acrylic acid or styrene.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S0040579518060155</doi><tpages>6</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0040-5795 |
| ispartof | Theoretical foundations of chemical engineering, 2018-11, Vol.52 (6), p.1039-1044 |
| issn | 0040-5795 1608-3431 |
| language | eng |
| recordid | cdi_proquest_journals_2169320976 |
| source | SpringerLink Journals - AutoHoldings |
| subjects | Acrylic acid Acrylics Aromatic compounds Atomic absorption analysis Catalysis Catalysts Catalytic activity Chemistry Chemistry and Materials Science Fourier transforms FTIR spectrometers Halides Industrial Chemistry/Chemical Engineering Palladium Photoelectrons Properties (attributes) X ray photoelectron spectroscopy |
| title | Studies on the Structure and Catalytic Properties for Heck Reaction of Troxerutin Supported Palladium Catalyst |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-28T01%3A12%3A24IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Studies%20on%20the%20Structure%20and%20Catalytic%20Properties%20for%20Heck%20Reaction%20of%20Troxerutin%20Supported%20Palladium%20Catalyst&rft.jtitle=Theoretical%20foundations%20of%20chemical%20engineering&rft.au=Xu,%20Q.%20J.&rft.date=2018-11-01&rft.volume=52&rft.issue=6&rft.spage=1039&rft.epage=1044&rft.pages=1039-1044&rft.issn=0040-5795&rft.eissn=1608-3431&rft_id=info:doi/10.1134/S0040579518060155&rft_dat=%3Cproquest_cross%3E2169320976%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2169320976&rft_id=info:pmid/&rfr_iscdi=true |