ICP-AES Analysis of Secondary Tungsten-Containing Raw Materials for Production of Hard Alloys
A method for ICP-AES determination of Ti, V, Cr, Fe, Co, Ni, Cu, Zn, and Ta in recycled cemented tungsten carbide is developed including preliminary microwave sample decomposition in a steam pressure vessel (autoclave). We have specified the composition of the reaction mixture for sample dissolution...
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| Veröffentlicht in: | Inorganic materials 2018-12, Vol.54 (14), p.1430-1434 |
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| container_issue | 14 |
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| container_title | Inorganic materials |
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| creator | Vyacheslavov, A. V. Bichaev, V. B. Titova, A. D. Rybin, D. S. Ermolaeva, T. N. |
| description | A method for ICP-AES determination of Ti, V, Cr, Fe, Co, Ni, Cu, Zn, and Ta in recycled cemented tungsten carbide is developed including preliminary microwave sample decomposition in a steam pressure vessel (autoclave). We have specified the composition of the reaction mixture for sample dissolution and optimized the parameters of microwave heating in the autoclave. Correctness of the results is proved by the method of sample weight variation and spike tests. The results of analysis are compared with the data obtained by standardless method of X-ray fluorescence spectrometry. The technique is characterized by good reproducibility and allows significant reduction of the analysis time owing to the combination of the multielement method of ICP-AES and microwave sample preparation. |
| doi_str_mv | 10.1134/S0020168518140169 |
| format | Article |
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The technique is characterized by good reproducibility and allows significant reduction of the analysis time owing to the combination of the multielement method of ICP-AES and microwave sample preparation.</description><subject>Alloys</subject><subject>Analysis of Substances</subject><subject>Atomic emission spectroscopy</subject><subject>Autoclaving</subject><subject>Cemented carbides</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chromium</subject><subject>Copper</subject><subject>Emission analysis</subject><subject>Inductively coupled plasma</subject><subject>Industrial Chemistry/Chemical Engineering</subject><subject>Inorganic Chemistry</subject><subject>Materials Science</subject><subject>Nickel</subject><subject>Pressure vessels</subject><subject>Raw materials</subject><subject>Reproducibility</subject><subject>Tungsten carbide</subject><subject>Weight</subject><subject>X ray fluorescence analysis</subject><issn>0020-1685</issn><issn>1608-3172</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNp1kFFLwzAUhYMoOKc_wLeAz9XcJF3Tx1KmG0wcbj5KydJkdNRkJi3Sf2_KBB_Ep3vhfOfAOQjdArkHYPxhQwglMBMpCODxyc_QBGZEJAwyeo4mo5yM-iW6CuFACOGpyCfofVmuk2K-wYWV7RCagJ3BG62craUf8La3-9Bpm5TOdrKxjd3jV_mFn2WnfSPbgI3zeO1d3auucXZ0L6SvcdG2bgjX6MJESN_83Cl6e5xvy0WyenlalsUqUSxlXcLNDPKd0kbVSua1kVSSlHKS0zRjO5bvakEpp9xQDZDrjDCVqZRlogYCigs2RXen3KN3n70OXXVwvY-NQkVjaUoZT3mk4EQp70Lw2lRH33zEmhWQalyx-rNi9NCTJ0TW7rX_Tf7f9A35xnJd</recordid><startdate>20181201</startdate><enddate>20181201</enddate><creator>Vyacheslavov, A. 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V.</creatorcontrib><creatorcontrib>Bichaev, V. B.</creatorcontrib><creatorcontrib>Titova, A. D.</creatorcontrib><creatorcontrib>Rybin, D. S.</creatorcontrib><creatorcontrib>Ermolaeva, T. N.</creatorcontrib><collection>CrossRef</collection><jtitle>Inorganic materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Vyacheslavov, A. V.</au><au>Bichaev, V. B.</au><au>Titova, A. D.</au><au>Rybin, D. S.</au><au>Ermolaeva, T. 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| subjects | Alloys Analysis of Substances Atomic emission spectroscopy Autoclaving Cemented carbides Chemistry Chemistry and Materials Science Chromium Copper Emission analysis Inductively coupled plasma Industrial Chemistry/Chemical Engineering Inorganic Chemistry Materials Science Nickel Pressure vessels Raw materials Reproducibility Tungsten carbide Weight X ray fluorescence analysis |
| title | ICP-AES Analysis of Secondary Tungsten-Containing Raw Materials for Production of Hard Alloys |
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