Reaction of sodium 4-acetyl-1-phenyl-1H-1,2,3-triazol-5-olate with 1,2,3-thiadiazole-4-carboxylic acid hydrazide

Reaction of sodium 4-acetyl-1-phenyl-1H-1,2,3-triazol-5-olate with 1,2,3-thiadiazole-4-carboxylic acid hydrazide

The present work describes a method for the synthesis a new N-1,2,3-triazol-1-yl-1,2,3-thiadiazol-4-carboxamide via condensation of open-chain form of 4-acetyl-1,2,3-triazolium-5-olate with 1,2,3-thiadiazole-4-carboxylic acid hydrazide, followed by formation new 1,2,3-triazole cycle. The structure o...

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Hauptverfasser: Tokareva, M. A., Obydennov, K. L., Slepukhin, P. A., Vysokova, O. A., Glukhareva, T. V.
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Sprache:eng
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Mass spectrometry
NMR
Nuclear magnetic resonance
X-ray diffraction
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creator Tokareva, M. A.
Obydennov, K. L.
Slepukhin, P. A.
Vysokova, O. A.
Glukhareva, T. V.
description The present work describes a method for the synthesis a new N-1,2,3-triazol-1-yl-1,2,3-thiadiazol-4-carboxamide via condensation of open-chain form of 4-acetyl-1,2,3-triazolium-5-olate with 1,2,3-thiadiazole-4-carboxylic acid hydrazide, followed by formation new 1,2,3-triazole cycle. The structure of synthesized compound was characterized by spectroscopic methods such as 1H NMR, 13C NMR, IR, mass spectrometry and X-ray diffraction.
doi_str_mv 10.1063/1.5087392
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subjects Mass spectrometry
NMR
Nuclear magnetic resonance
X-ray diffraction
title Reaction of sodium 4-acetyl-1-phenyl-1H-1,2,3-triazol-5-olate with 1,2,3-thiadiazole-4-carboxylic acid hydrazide
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