Synthesis and characterization of rhombic dodecahedral YAG microcrystals with good dispersity, high crystallinity and controllable crystal size
By exploring the optimal reaction temperature and the ratio of Na 2 SO 4 to the precursor, highly symmetrical rhombic dodecahedral yttrium aluminum garnet (Y 3 Al 5 O 12 , YAG) microcrystals with a good dispersity were successfully prepared using improved hydrothermal methods. YAG microcrystals exhi...
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| Veröffentlicht in: | CrystEngComm 2018, Vol.2 (48), p.7773-7781 |
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| creator | Yuan, Rui Xie, Xi-Xi Zheng, Li-Xian Yu, Li-Li Hu, Jian-Feng Qin, Hai-Ming Zhang, Zhi-Jun Zhao, Jing-Tai |
| description | By exploring the optimal reaction temperature and the ratio of Na
2
SO
4
to the precursor, highly symmetrical rhombic dodecahedral yttrium aluminum garnet (Y
3
Al
5
O
12
, YAG) microcrystals with a good dispersity were successfully prepared using improved hydrothermal methods. YAG microcrystals exhibit well-developed crystal faces, high crystallinity and a controllable crystal size, from hundreds of nanometers to approximately 4 μm. The morphology and crystal size of the YAG microcrystals can be controlled by changing the reaction temperature and the ratio of Na
2
SO
4
to the precursor. After analysis using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and energy dispersive spectrometry (EDS), the growth mechanism of the YAG crystals was studied in detail. Cerium doped YAG (YAG:Ce
3+
) microcrystals exhibit an intense broad band emission at approximately 523 nm. Considering the high crystallinity, controllable size and strong emission of YAG microcrystals, one has reason to assume that they could have wide applications in many areas.
Symmetrical rhombic dodecahedral YAG microcrystals were successfully prepared using improved hydrothermal methods. |
| doi_str_mv | 10.1039/c8ce01688g |
| format | Article |
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2
SO
4
to the precursor, highly symmetrical rhombic dodecahedral yttrium aluminum garnet (Y
3
Al
5
O
12
, YAG) microcrystals with a good dispersity were successfully prepared using improved hydrothermal methods. YAG microcrystals exhibit well-developed crystal faces, high crystallinity and a controllable crystal size, from hundreds of nanometers to approximately 4 μm. The morphology and crystal size of the YAG microcrystals can be controlled by changing the reaction temperature and the ratio of Na
2
SO
4
to the precursor. After analysis using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and energy dispersive spectrometry (EDS), the growth mechanism of the YAG crystals was studied in detail. Cerium doped YAG (YAG:Ce
3+
) microcrystals exhibit an intense broad band emission at approximately 523 nm. Considering the high crystallinity, controllable size and strong emission of YAG microcrystals, one has reason to assume that they could have wide applications in many areas.
Symmetrical rhombic dodecahedral YAG microcrystals were successfully prepared using improved hydrothermal methods.</description><identifier>ISSN: 1466-8033</identifier><identifier>EISSN: 1466-8033</identifier><identifier>DOI: 10.1039/c8ce01688g</identifier><language>eng</language><publisher>Cambridge: Royal Society of Chemistry</publisher><subject>Aluminum ; Cerium ; Crystal structure ; Crystallinity ; Crystals ; Fourier transforms ; Infrared analysis ; Infrared spectroscopy ; Microcrystals ; Morphology ; Particle size ; Particle size distribution ; Precursors ; Scanning electron microscopy ; Sodium sulfate ; Stability ; X ray spectra ; X-ray diffraction ; Yttrium ; Yttrium-aluminum garnet</subject><ispartof>CrystEngComm, 2018, Vol.2 (48), p.7773-7781</ispartof><rights>Copyright Royal Society of Chemistry 2018</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c318t-47b2d96e21fd3a7f5a4132853bcab5d186b8529601a044ee77456cca75e415a23</citedby><cites>FETCH-LOGICAL-c318t-47b2d96e21fd3a7f5a4132853bcab5d186b8529601a044ee77456cca75e415a23</cites><orcidid>0000-0003-2841-5462 ; 0000-0003-4740-526X ; 0000-0002-0593-2048</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,4024,27923,27924,27925</link.rule.ids></links><search><creatorcontrib>Yuan, Rui</creatorcontrib><creatorcontrib>Xie, Xi-Xi</creatorcontrib><creatorcontrib>Zheng, Li-Xian</creatorcontrib><creatorcontrib>Yu, Li-Li</creatorcontrib><creatorcontrib>Hu, Jian-Feng</creatorcontrib><creatorcontrib>Qin, Hai-Ming</creatorcontrib><creatorcontrib>Zhang, Zhi-Jun</creatorcontrib><creatorcontrib>Zhao, Jing-Tai</creatorcontrib><title>Synthesis and characterization of rhombic dodecahedral YAG microcrystals with good dispersity, high crystallinity and controllable crystal size</title><title>CrystEngComm</title><description>By exploring the optimal reaction temperature and the ratio of Na
2
SO
4
to the precursor, highly symmetrical rhombic dodecahedral yttrium aluminum garnet (Y
3
Al
5
O
12
, YAG) microcrystals with a good dispersity were successfully prepared using improved hydrothermal methods. YAG microcrystals exhibit well-developed crystal faces, high crystallinity and a controllable crystal size, from hundreds of nanometers to approximately 4 μm. The morphology and crystal size of the YAG microcrystals can be controlled by changing the reaction temperature and the ratio of Na
2
SO
4
to the precursor. After analysis using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and energy dispersive spectrometry (EDS), the growth mechanism of the YAG crystals was studied in detail. Cerium doped YAG (YAG:Ce
3+
) microcrystals exhibit an intense broad band emission at approximately 523 nm. Considering the high crystallinity, controllable size and strong emission of YAG microcrystals, one has reason to assume that they could have wide applications in many areas.
Symmetrical rhombic dodecahedral YAG microcrystals were successfully prepared using improved hydrothermal methods.</description><subject>Aluminum</subject><subject>Cerium</subject><subject>Crystal structure</subject><subject>Crystallinity</subject><subject>Crystals</subject><subject>Fourier transforms</subject><subject>Infrared analysis</subject><subject>Infrared spectroscopy</subject><subject>Microcrystals</subject><subject>Morphology</subject><subject>Particle size</subject><subject>Particle size distribution</subject><subject>Precursors</subject><subject>Scanning electron microscopy</subject><subject>Sodium sulfate</subject><subject>Stability</subject><subject>X ray spectra</subject><subject>X-ray diffraction</subject><subject>Yttrium</subject><subject>Yttrium-aluminum garnet</subject><issn>1466-8033</issn><issn>1466-8033</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNpNkU1LAzEQhoMoWKsX70LAm7iabD42PZalVqHgQT14WrJJtpuy3dQkRbZ_wr_s6taP0wwzD-_LvAPAOUY3GJHJrRLKIMyFWB6AEaacJwIRcvivPwYnIawQwhRjNAIfT10baxNsgLLVUNXSSxWNtzsZrWuhq6Cv3bq0CmqnjZK10V428HU6h2urvFO-C1E2Ab7bWMOlcxpqGzbGBxu7a1jbZQ33TGPbfjb4uDZ61zSybMzPGga7M6fgqOrVzNm-jsHL3ew5v08Wj_OHfLpIFMEiJjQrUz3hJsWVJjKrmKSYpIKRUsmSaSx4KVg64QhLRKkxWUYZV0pmzFDMZErG4HLQ3Xj3tjUhFiu39W1vWaSYEU4oz7Keuhqo_tAQvKmKjbdr6bsCo-Ir8CIX-ew78HkPXwywD-qX-3sI-QRdxIBJ</recordid><startdate>2018</startdate><enddate>2018</enddate><creator>Yuan, Rui</creator><creator>Xie, Xi-Xi</creator><creator>Zheng, Li-Xian</creator><creator>Yu, Li-Li</creator><creator>Hu, Jian-Feng</creator><creator>Qin, Hai-Ming</creator><creator>Zhang, Zhi-Jun</creator><creator>Zhao, Jing-Tai</creator><general>Royal Society of Chemistry</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope><orcidid>https://orcid.org/0000-0003-2841-5462</orcidid><orcidid>https://orcid.org/0000-0003-4740-526X</orcidid><orcidid>https://orcid.org/0000-0002-0593-2048</orcidid></search><sort><creationdate>2018</creationdate><title>Synthesis and characterization of rhombic dodecahedral YAG microcrystals with good dispersity, high crystallinity and controllable crystal size</title><author>Yuan, Rui ; Xie, Xi-Xi ; Zheng, Li-Xian ; Yu, Li-Li ; Hu, Jian-Feng ; Qin, Hai-Ming ; Zhang, Zhi-Jun ; Zhao, Jing-Tai</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c318t-47b2d96e21fd3a7f5a4132853bcab5d186b8529601a044ee77456cca75e415a23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Aluminum</topic><topic>Cerium</topic><topic>Crystal structure</topic><topic>Crystallinity</topic><topic>Crystals</topic><topic>Fourier transforms</topic><topic>Infrared analysis</topic><topic>Infrared spectroscopy</topic><topic>Microcrystals</topic><topic>Morphology</topic><topic>Particle size</topic><topic>Particle size distribution</topic><topic>Precursors</topic><topic>Scanning electron microscopy</topic><topic>Sodium sulfate</topic><topic>Stability</topic><topic>X ray spectra</topic><topic>X-ray diffraction</topic><topic>Yttrium</topic><topic>Yttrium-aluminum garnet</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yuan, Rui</creatorcontrib><creatorcontrib>Xie, Xi-Xi</creatorcontrib><creatorcontrib>Zheng, Li-Xian</creatorcontrib><creatorcontrib>Yu, Li-Li</creatorcontrib><creatorcontrib>Hu, Jian-Feng</creatorcontrib><creatorcontrib>Qin, Hai-Ming</creatorcontrib><creatorcontrib>Zhang, Zhi-Jun</creatorcontrib><creatorcontrib>Zhao, Jing-Tai</creatorcontrib><collection>CrossRef</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>CrystEngComm</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yuan, Rui</au><au>Xie, Xi-Xi</au><au>Zheng, Li-Xian</au><au>Yu, Li-Li</au><au>Hu, Jian-Feng</au><au>Qin, Hai-Ming</au><au>Zhang, Zhi-Jun</au><au>Zhao, Jing-Tai</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and characterization of rhombic dodecahedral YAG microcrystals with good dispersity, high crystallinity and controllable crystal size</atitle><jtitle>CrystEngComm</jtitle><date>2018</date><risdate>2018</risdate><volume>2</volume><issue>48</issue><spage>7773</spage><epage>7781</epage><pages>7773-7781</pages><issn>1466-8033</issn><eissn>1466-8033</eissn><abstract>By exploring the optimal reaction temperature and the ratio of Na
2
SO
4
to the precursor, highly symmetrical rhombic dodecahedral yttrium aluminum garnet (Y
3
Al
5
O
12
, YAG) microcrystals with a good dispersity were successfully prepared using improved hydrothermal methods. YAG microcrystals exhibit well-developed crystal faces, high crystallinity and a controllable crystal size, from hundreds of nanometers to approximately 4 μm. The morphology and crystal size of the YAG microcrystals can be controlled by changing the reaction temperature and the ratio of Na
2
SO
4
to the precursor. After analysis using X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FT-IR), and energy dispersive spectrometry (EDS), the growth mechanism of the YAG crystals was studied in detail. Cerium doped YAG (YAG:Ce
3+
) microcrystals exhibit an intense broad band emission at approximately 523 nm. Considering the high crystallinity, controllable size and strong emission of YAG microcrystals, one has reason to assume that they could have wide applications in many areas.
Symmetrical rhombic dodecahedral YAG microcrystals were successfully prepared using improved hydrothermal methods.</abstract><cop>Cambridge</cop><pub>Royal Society of Chemistry</pub><doi>10.1039/c8ce01688g</doi><tpages>9</tpages><orcidid>https://orcid.org/0000-0003-2841-5462</orcidid><orcidid>https://orcid.org/0000-0003-4740-526X</orcidid><orcidid>https://orcid.org/0000-0002-0593-2048</orcidid></addata></record> |
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| ispartof | CrystEngComm, 2018, Vol.2 (48), p.7773-7781 |
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| language | eng |
| recordid | cdi_proquest_journals_2153634677 |
| source | Royal Society Of Chemistry Journals; Alma/SFX Local Collection |
| subjects | Aluminum Cerium Crystal structure Crystallinity Crystals Fourier transforms Infrared analysis Infrared spectroscopy Microcrystals Morphology Particle size Particle size distribution Precursors Scanning electron microscopy Sodium sulfate Stability X ray spectra X-ray diffraction Yttrium Yttrium-aluminum garnet |
| title | Synthesis and characterization of rhombic dodecahedral YAG microcrystals with good dispersity, high crystallinity and controllable crystal size |
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