Photo-catalyst and magnetic nanocomposites: hydrothermal preparation of core–shell Fe3O4@PbS for photo-degradation of toxic dyes
In this work, at the first stage Fe 3 O 4 and mono-disperse lead sulfide (PbS) nanostructures were synthesized via a simple hydrothermal method at water as a green solvent. Then Fe 3 O 4 @PbS nanocomposites were prepared by facile chemical procedure. The effect of concentration, temperature, precipi...
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| Veröffentlicht in: | Journal of materials science. Materials in electronics 2017, Vol.28 (2), p.1577-1589 |
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| container_title | Journal of materials science. Materials in electronics |
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| creator | Hedayati, Kambiz Kord, Mohsen Goodarzi, Mojtaba Ghanbari, Davood Gharigh, Simin |
| description | In this work, at the first stage Fe
3
O
4
and mono-disperse lead sulfide (PbS) nanostructures were synthesized via a simple hydrothermal method at water as a green solvent. Then Fe
3
O
4
@PbS nanocomposites were prepared by facile chemical procedure. The effect of concentration, temperature, precipitating agent, capping agent on the morphology and particle size of the products was investigated. Glucose was used as green, safe, cost-effective and bio-compatible capping agent. The prepared products were characterized by X-ray diffraction, scanning electron microscopy, electron microscopy transmission and Fourier transform infrared spectroscopy. Vibration sample magnetometer approves the super paramagnetic property of the magnetite and nanocomposites. The photo-catalytic behaviour of nanocomposites was evaluated using the degradation of four azo dyes (acid black, acid brown, acid violet and acid blue) under ultraviolet light irradiation. The results introduce a nanocomposite with applicable magnetic and photocatalytic performance. |
| doi_str_mv | 10.1007/s10854-016-5698-4 |
| format | Article |
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3
O
4
and mono-disperse lead sulfide (PbS) nanostructures were synthesized via a simple hydrothermal method at water as a green solvent. Then Fe
3
O
4
@PbS nanocomposites were prepared by facile chemical procedure. The effect of concentration, temperature, precipitating agent, capping agent on the morphology and particle size of the products was investigated. Glucose was used as green, safe, cost-effective and bio-compatible capping agent. The prepared products were characterized by X-ray diffraction, scanning electron microscopy, electron microscopy transmission and Fourier transform infrared spectroscopy. Vibration sample magnetometer approves the super paramagnetic property of the magnetite and nanocomposites. The photo-catalytic behaviour of nanocomposites was evaluated using the degradation of four azo dyes (acid black, acid brown, acid violet and acid blue) under ultraviolet light irradiation. The results introduce a nanocomposite with applicable magnetic and photocatalytic performance.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-016-5698-4</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Acids ; Biocompatibility ; Capping ; Catalysis ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Dyes ; Fourier transforms ; Iron oxides ; Lead sulfides ; Light irradiation ; Magnetic properties ; Materials Science ; Microscopy ; Morphology ; Nanocomposites ; Optical and Electronic Materials ; Organic chemistry ; Photodegradation ; Scanning electron microscopy ; Ultraviolet radiation ; X ray spectra ; X-ray diffraction</subject><ispartof>Journal of materials science. Materials in electronics, 2017, Vol.28 (2), p.1577-1589</ispartof><rights>Springer Science+Business Media New York 2016</rights><rights>Journal of Materials Science: Materials in Electronics is a copyright of Springer, (2016). All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c353t-b642c0ae751510580277bec735d7d7cf9a1ba059200df46717663f061a9dfba13</citedby><cites>FETCH-LOGICAL-c353t-b642c0ae751510580277bec735d7d7cf9a1ba059200df46717663f061a9dfba13</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10854-016-5698-4$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10854-016-5698-4$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27903,27904,41467,42536,51297</link.rule.ids></links><search><creatorcontrib>Hedayati, Kambiz</creatorcontrib><creatorcontrib>Kord, Mohsen</creatorcontrib><creatorcontrib>Goodarzi, Mojtaba</creatorcontrib><creatorcontrib>Ghanbari, Davood</creatorcontrib><creatorcontrib>Gharigh, Simin</creatorcontrib><title>Photo-catalyst and magnetic nanocomposites: hydrothermal preparation of core–shell Fe3O4@PbS for photo-degradation of toxic dyes</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>In this work, at the first stage Fe
3
O
4
and mono-disperse lead sulfide (PbS) nanostructures were synthesized via a simple hydrothermal method at water as a green solvent. Then Fe
3
O
4
@PbS nanocomposites were prepared by facile chemical procedure. The effect of concentration, temperature, precipitating agent, capping agent on the morphology and particle size of the products was investigated. Glucose was used as green, safe, cost-effective and bio-compatible capping agent. The prepared products were characterized by X-ray diffraction, scanning electron microscopy, electron microscopy transmission and Fourier transform infrared spectroscopy. Vibration sample magnetometer approves the super paramagnetic property of the magnetite and nanocomposites. The photo-catalytic behaviour of nanocomposites was evaluated using the degradation of four azo dyes (acid black, acid brown, acid violet and acid blue) under ultraviolet light irradiation. The results introduce a nanocomposite with applicable magnetic and photocatalytic performance.</description><subject>Acids</subject><subject>Biocompatibility</subject><subject>Capping</subject><subject>Catalysis</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Dyes</subject><subject>Fourier transforms</subject><subject>Iron oxides</subject><subject>Lead sulfides</subject><subject>Light irradiation</subject><subject>Magnetic properties</subject><subject>Materials Science</subject><subject>Microscopy</subject><subject>Morphology</subject><subject>Nanocomposites</subject><subject>Optical and Electronic Materials</subject><subject>Organic chemistry</subject><subject>Photodegradation</subject><subject>Scanning electron microscopy</subject><subject>Ultraviolet radiation</subject><subject>X ray spectra</subject><subject>X-ray diffraction</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp1kMtKxDAYhYMoOF4ewF3AdfRPc2tdKeINBAdUcBfSJJ0LnaYmEZyd-Aq-oU9ixxFduTqb75wDH0IHFI4ogDpOFErBCVBJhKxKwjfQiArFCC-Lp000gkoowkVRbKOdlOYAIDkrR-h9PA05EGuyaZcpY9M5vDCTzueZxZ3pgg2LPqRZ9ukET5cuhjz1cWFa3Effm2jyLHQ4NNiG6D_fPtLUty2-9OyOn47re9yEiPvvC-cn0bhfPofX4cEtfdpDW41pk9__yV30eHnxcH5Nbu-ubs7PbollgmVSS15YMF4JKiiIEgqlam8VE045ZZvK0NqAqAoA13CpqJKSNSCpqVxTG8p20eF6t4_h-cWnrOfhJXbDpS4oEwqYkiuKrikbQ0rRN7qPs4WJS01Br1TrtWo9qNYr1ZoPnWLdSQPbTXz8W_6_9AWOE4QA</recordid><startdate>2017</startdate><enddate>2017</enddate><creator>Hedayati, Kambiz</creator><creator>Kord, Mohsen</creator><creator>Goodarzi, Mojtaba</creator><creator>Ghanbari, Davood</creator><creator>Gharigh, Simin</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F28</scope><scope>FR3</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L7M</scope><scope>P5Z</scope><scope>P62</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>S0W</scope></search><sort><creationdate>2017</creationdate><title>Photo-catalyst and magnetic nanocomposites: hydrothermal preparation of core–shell Fe3O4@PbS for photo-degradation of toxic dyes</title><author>Hedayati, Kambiz ; Kord, Mohsen ; Goodarzi, Mojtaba ; Ghanbari, Davood ; Gharigh, Simin</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c353t-b642c0ae751510580277bec735d7d7cf9a1ba059200df46717663f061a9dfba13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Acids</topic><topic>Biocompatibility</topic><topic>Capping</topic><topic>Catalysis</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Dyes</topic><topic>Fourier transforms</topic><topic>Iron oxides</topic><topic>Lead sulfides</topic><topic>Light irradiation</topic><topic>Magnetic properties</topic><topic>Materials Science</topic><topic>Microscopy</topic><topic>Morphology</topic><topic>Nanocomposites</topic><topic>Optical and Electronic Materials</topic><topic>Organic chemistry</topic><topic>Photodegradation</topic><topic>Scanning electron microscopy</topic><topic>Ultraviolet radiation</topic><topic>X ray spectra</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hedayati, Kambiz</creatorcontrib><creatorcontrib>Kord, Mohsen</creatorcontrib><creatorcontrib>Goodarzi, Mojtaba</creatorcontrib><creatorcontrib>Ghanbari, Davood</creatorcontrib><creatorcontrib>Gharigh, Simin</creatorcontrib><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>Advanced Technologies & Aerospace Database (1962 - current)</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>ProQuest advanced technologies & aerospace journals</collection><collection>test</collection><collection>Materials science collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DELNET Engineering & Technology Collection</collection><jtitle>Journal of materials science. Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Hedayati, Kambiz</au><au>Kord, Mohsen</au><au>Goodarzi, Mojtaba</au><au>Ghanbari, Davood</au><au>Gharigh, Simin</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Photo-catalyst and magnetic nanocomposites: hydrothermal preparation of core–shell Fe3O4@PbS for photo-degradation of toxic dyes</atitle><jtitle>Journal of materials science. Materials in electronics</jtitle><stitle>J Mater Sci: Mater Electron</stitle><date>2017</date><risdate>2017</risdate><volume>28</volume><issue>2</issue><spage>1577</spage><epage>1589</epage><pages>1577-1589</pages><issn>0957-4522</issn><eissn>1573-482X</eissn><abstract>In this work, at the first stage Fe
3
O
4
and mono-disperse lead sulfide (PbS) nanostructures were synthesized via a simple hydrothermal method at water as a green solvent. Then Fe
3
O
4
@PbS nanocomposites were prepared by facile chemical procedure. The effect of concentration, temperature, precipitating agent, capping agent on the morphology and particle size of the products was investigated. Glucose was used as green, safe, cost-effective and bio-compatible capping agent. The prepared products were characterized by X-ray diffraction, scanning electron microscopy, electron microscopy transmission and Fourier transform infrared spectroscopy. Vibration sample magnetometer approves the super paramagnetic property of the magnetite and nanocomposites. The photo-catalytic behaviour of nanocomposites was evaluated using the degradation of four azo dyes (acid black, acid brown, acid violet and acid blue) under ultraviolet light irradiation. The results introduce a nanocomposite with applicable magnetic and photocatalytic performance.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-016-5698-4</doi><tpages>13</tpages></addata></record> |
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| subjects | Acids Biocompatibility Capping Catalysis Characterization and Evaluation of Materials Chemistry and Materials Science Dyes Fourier transforms Iron oxides Lead sulfides Light irradiation Magnetic properties Materials Science Microscopy Morphology Nanocomposites Optical and Electronic Materials Organic chemistry Photodegradation Scanning electron microscopy Ultraviolet radiation X ray spectra X-ray diffraction |
| title | Photo-catalyst and magnetic nanocomposites: hydrothermal preparation of core–shell Fe3O4@PbS for photo-degradation of toxic dyes |
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