An Environmentally Significant Experiment Using GC/MS and GC Retention Indices in an Undergraduate Analytical Laboratory
An undergraduate laboratory experiment has been developed in which the students extract and analyze the additives from plastic food wrap, Tygon tubing and plastic soda bottles that have been crushed in a bottle return machine. The modifiers are extracted from the plastics using methylene chloride an...
Gespeichert in:
Veröffentlicht in: | Journal of chemical education 1996-12, Vol.73 (12), p.1176 |
---|---|
Hauptverfasser: | , , , , , |
Format: | Artikel |
Sprache: | eng |
Schlagworte: | |
Online-Zugang: | Volltext |
Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
container_end_page | |
---|---|
container_issue | 12 |
container_start_page | 1176 |
container_title | Journal of chemical education |
container_volume | 73 |
creator | Guisto-Norkus, Rebecca Gounili, Giv Wisniecki, Peter Hubball, John A Smith, S. Ruven Stuart, James D |
description | An undergraduate laboratory experiment has been developed in which the students extract and analyze the additives from plastic food wrap, Tygon tubing and plastic soda bottles that have been crushed in a bottle return machine. The modifiers are extracted from the plastics using methylene chloride and/or methanol as solvents and the extracts are analyzed by GC/MS. Identifications are carried out by a combination of automated computer and manual library searches and chromatographic retention indices. |
doi_str_mv | 10.1021/ed073p1176 |
format | Article |
fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_211920657</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1096721281</sourcerecordid><originalsourceid>FETCH-LOGICAL-a287t-df0a82f435dbd154a985ee64e9456ee161bf50603149e789c9fc5200693d3a023</originalsourceid><addsrcrecordid>eNptkE1LAzEQhoMoWKsXf0Hw4EFYm4_NbnIspdZCRbD2vKSb2ZKyZmuSSvffm1KhF08z8Dy8zLwI3VPyTAmjIzCk5DtKy-ICDajiMqOcyUs0IIlmSsj8Gt2EsCWEMqHkAB3GDk_dj_Wd-wIXddv2eGk3zja21i7i6WEH3h4RXgXrNng2Gb0tsXYmbfgDYiK2c3jujK0hYOsSwytnwG-8NnsdAY-dbvuY8lq80OvO69j5_hZdNboNcPc3h2j1Mv2cvGaL99l8Ml5kmskyZqYhWrIm58KsDRW5VlIAFDmoXBQAtKDrRpCCcJorKKWqVVMLRkihuOGaMD5ED6fcne--9xBite32Pl0UKkapYqQQZZKeTlLtuxA8NNUuPa19X1FSHYutzsUm-fEk6zqcw_4RfwGO8HdT</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>211920657</pqid></control><display><type>article</type><title>An Environmentally Significant Experiment Using GC/MS and GC Retention Indices in an Undergraduate Analytical Laboratory</title><source>American Chemical Society Journals</source><creator>Guisto-Norkus, Rebecca ; Gounili, Giv ; Wisniecki, Peter ; Hubball, John A ; Smith, S. Ruven ; Stuart, James D</creator><creatorcontrib>Guisto-Norkus, Rebecca ; Gounili, Giv ; Wisniecki, Peter ; Hubball, John A ; Smith, S. Ruven ; Stuart, James D</creatorcontrib><description>An undergraduate laboratory experiment has been developed in which the students extract and analyze the additives from plastic food wrap, Tygon tubing and plastic soda bottles that have been crushed in a bottle return machine. The modifiers are extracted from the plastics using methylene chloride and/or methanol as solvents and the extracts are analyzed by GC/MS. Identifications are carried out by a combination of automated computer and manual library searches and chromatographic retention indices.</description><identifier>ISSN: 0021-9584</identifier><identifier>EISSN: 1938-1328</identifier><identifier>DOI: 10.1021/ed073p1176</identifier><identifier>CODEN: JCEDA8</identifier><language>eng</language><publisher>Easton: Division of Chemical Education</publisher><subject>Adjuncts ; Chloride ; Chromatography ; Climate ; Computers ; Dichloromethane ; Drinking water ; Environmental impact ; Environmental monitoring ; Environmental protection ; Esters ; Experiments ; Food ; Gas chromatography ; Identification ; Identification (Psychology) ; Inhalants ; Instrumentation ; Laboratories ; Laboratory Experiments ; Libraries ; Mass spectra ; Mass spectrometry ; Nitrogen ; Organic compounds ; Plasticizers ; Plastics ; Retention ; Scientific Concepts ; Scientific imaging ; Solvents ; Spectroscopy ; Temperature</subject><ispartof>Journal of chemical education, 1996-12, Vol.73 (12), p.1176</ispartof><rights>Copyright American Chemical Society Dec 1996</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-a287t-df0a82f435dbd154a985ee64e9456ee161bf50603149e789c9fc5200693d3a023</citedby></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://pubs.acs.org/doi/pdf/10.1021/ed073p1176$$EPDF$$P50$$Gacs$$H</linktopdf><linktohtml>$$Uhttps://pubs.acs.org/doi/10.1021/ed073p1176$$EHTML$$P50$$Gacs$$H</linktohtml><link.rule.ids>314,780,784,2765,27076,27924,27925,56738,56788</link.rule.ids></links><search><creatorcontrib>Guisto-Norkus, Rebecca</creatorcontrib><creatorcontrib>Gounili, Giv</creatorcontrib><creatorcontrib>Wisniecki, Peter</creatorcontrib><creatorcontrib>Hubball, John A</creatorcontrib><creatorcontrib>Smith, S. Ruven</creatorcontrib><creatorcontrib>Stuart, James D</creatorcontrib><title>An Environmentally Significant Experiment Using GC/MS and GC Retention Indices in an Undergraduate Analytical Laboratory</title><title>Journal of chemical education</title><addtitle>J. Chem. Educ</addtitle><description>An undergraduate laboratory experiment has been developed in which the students extract and analyze the additives from plastic food wrap, Tygon tubing and plastic soda bottles that have been crushed in a bottle return machine. The modifiers are extracted from the plastics using methylene chloride and/or methanol as solvents and the extracts are analyzed by GC/MS. Identifications are carried out by a combination of automated computer and manual library searches and chromatographic retention indices.</description><subject>Adjuncts</subject><subject>Chloride</subject><subject>Chromatography</subject><subject>Climate</subject><subject>Computers</subject><subject>Dichloromethane</subject><subject>Drinking water</subject><subject>Environmental impact</subject><subject>Environmental monitoring</subject><subject>Environmental protection</subject><subject>Esters</subject><subject>Experiments</subject><subject>Food</subject><subject>Gas chromatography</subject><subject>Identification</subject><subject>Identification (Psychology)</subject><subject>Inhalants</subject><subject>Instrumentation</subject><subject>Laboratories</subject><subject>Laboratory Experiments</subject><subject>Libraries</subject><subject>Mass spectra</subject><subject>Mass spectrometry</subject><subject>Nitrogen</subject><subject>Organic compounds</subject><subject>Plasticizers</subject><subject>Plastics</subject><subject>Retention</subject><subject>Scientific Concepts</subject><subject>Scientific imaging</subject><subject>Solvents</subject><subject>Spectroscopy</subject><subject>Temperature</subject><issn>0021-9584</issn><issn>1938-1328</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1996</creationdate><recordtype>article</recordtype><sourceid>8G5</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AIMQZ</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><sourceid>GUQSH</sourceid><sourceid>M2O</sourceid><recordid>eNptkE1LAzEQhoMoWKsXf0Hw4EFYm4_NbnIspdZCRbD2vKSb2ZKyZmuSSvffm1KhF08z8Dy8zLwI3VPyTAmjIzCk5DtKy-ICDajiMqOcyUs0IIlmSsj8Gt2EsCWEMqHkAB3GDk_dj_Wd-wIXddv2eGk3zja21i7i6WEH3h4RXgXrNng2Gb0tsXYmbfgDYiK2c3jujK0hYOsSwytnwG-8NnsdAY-dbvuY8lq80OvO69j5_hZdNboNcPc3h2j1Mv2cvGaL99l8Ml5kmskyZqYhWrIm58KsDRW5VlIAFDmoXBQAtKDrRpCCcJorKKWqVVMLRkihuOGaMD5ED6fcne--9xBite32Pl0UKkapYqQQZZKeTlLtuxA8NNUuPa19X1FSHYutzsUm-fEk6zqcw_4RfwGO8HdT</recordid><startdate>19961201</startdate><enddate>19961201</enddate><creator>Guisto-Norkus, Rebecca</creator><creator>Gounili, Giv</creator><creator>Wisniecki, Peter</creator><creator>Hubball, John A</creator><creator>Smith, S. Ruven</creator><creator>Stuart, James D</creator><general>Division of Chemical Education</general><general>American Chemical Society</general><scope>AAYXX</scope><scope>CITATION</scope><scope>0-V</scope><scope>3V.</scope><scope>7X7</scope><scope>7XB</scope><scope>88B</scope><scope>88E</scope><scope>88I</scope><scope>8A4</scope><scope>8FE</scope><scope>8FG</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>8G5</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AIMQZ</scope><scope>ALSLI</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>BKSAR</scope><scope>CCPQU</scope><scope>CJNVE</scope><scope>D1I</scope><scope>DWQXO</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>GUQSH</scope><scope>HCIFZ</scope><scope>K9.</scope><scope>KB.</scope><scope>LIQON</scope><scope>M0P</scope><scope>M0S</scope><scope>M1P</scope><scope>M2O</scope><scope>M2P</scope><scope>MBDVC</scope><scope>PADUT</scope><scope>PCBAR</scope><scope>PDBOC</scope><scope>PQEDU</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>Q9U</scope></search><sort><creationdate>19961201</creationdate><title>An Environmentally Significant Experiment Using GC/MS and GC Retention Indices in an Undergraduate Analytical Laboratory</title><author>Guisto-Norkus, Rebecca ; Gounili, Giv ; Wisniecki, Peter ; Hubball, John A ; Smith, S. Ruven ; Stuart, James D</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-a287t-df0a82f435dbd154a985ee64e9456ee161bf50603149e789c9fc5200693d3a023</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1996</creationdate><topic>Adjuncts</topic><topic>Chloride</topic><topic>Chromatography</topic><topic>Climate</topic><topic>Computers</topic><topic>Dichloromethane</topic><topic>Drinking water</topic><topic>Environmental impact</topic><topic>Environmental monitoring</topic><topic>Environmental protection</topic><topic>Esters</topic><topic>Experiments</topic><topic>Food</topic><topic>Gas chromatography</topic><topic>Identification</topic><topic>Identification (Psychology)</topic><topic>Inhalants</topic><topic>Instrumentation</topic><topic>Laboratories</topic><topic>Laboratory Experiments</topic><topic>Libraries</topic><topic>Mass spectra</topic><topic>Mass spectrometry</topic><topic>Nitrogen</topic><topic>Organic compounds</topic><topic>Plasticizers</topic><topic>Plastics</topic><topic>Retention</topic><topic>Scientific Concepts</topic><topic>Scientific imaging</topic><topic>Solvents</topic><topic>Spectroscopy</topic><topic>Temperature</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Guisto-Norkus, Rebecca</creatorcontrib><creatorcontrib>Gounili, Giv</creatorcontrib><creatorcontrib>Wisniecki, Peter</creatorcontrib><creatorcontrib>Hubball, John A</creatorcontrib><creatorcontrib>Smith, S. Ruven</creatorcontrib><creatorcontrib>Stuart, James D</creatorcontrib><collection>CrossRef</collection><collection>ProQuest Social Sciences Premium Collection</collection><collection>ProQuest Central (Corporate)</collection><collection>Health & Medical Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Education Database (Alumni Edition)</collection><collection>Medical Database (Alumni Edition)</collection><collection>Science Database (Alumni Edition)</collection><collection>Education Periodicals</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Hospital Premium Collection</collection><collection>Hospital Premium Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Research Library (Alumni Edition)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest One Literature</collection><collection>Social Science Premium Collection</collection><collection>ProQuest Central Essentials</collection><collection>Proquest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>Earth, Atmospheric & Aquatic Science Collection</collection><collection>ProQuest One Community College</collection><collection>Education Collection</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>Health Research Premium Collection</collection><collection>Health Research Premium Collection (Alumni)</collection><collection>ProQuest Central Student</collection><collection>Research Library Prep</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Health & Medical Complete (Alumni)</collection><collection>Materials Science Database</collection><collection>ProQuest One Literature - U.S. Customers Only</collection><collection>Education Database</collection><collection>Health & Medical Collection (Alumni Edition)</collection><collection>Medical Database</collection><collection>Research Library</collection><collection>Science Database</collection><collection>Research Library (Corporate)</collection><collection>Research Library China</collection><collection>Earth, Atmospheric & Aquatic Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Education</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>ProQuest Central Basic</collection><jtitle>Journal of chemical education</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Guisto-Norkus, Rebecca</au><au>Gounili, Giv</au><au>Wisniecki, Peter</au><au>Hubball, John A</au><au>Smith, S. Ruven</au><au>Stuart, James D</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>An Environmentally Significant Experiment Using GC/MS and GC Retention Indices in an Undergraduate Analytical Laboratory</atitle><jtitle>Journal of chemical education</jtitle><addtitle>J. Chem. Educ</addtitle><date>1996-12-01</date><risdate>1996</risdate><volume>73</volume><issue>12</issue><spage>1176</spage><pages>1176-</pages><issn>0021-9584</issn><eissn>1938-1328</eissn><coden>JCEDA8</coden><abstract>An undergraduate laboratory experiment has been developed in which the students extract and analyze the additives from plastic food wrap, Tygon tubing and plastic soda bottles that have been crushed in a bottle return machine. The modifiers are extracted from the plastics using methylene chloride and/or methanol as solvents and the extracts are analyzed by GC/MS. Identifications are carried out by a combination of automated computer and manual library searches and chromatographic retention indices.</abstract><cop>Easton</cop><pub>Division of Chemical Education</pub><doi>10.1021/ed073p1176</doi></addata></record> |
fulltext | fulltext |
identifier | ISSN: 0021-9584 |
ispartof | Journal of chemical education, 1996-12, Vol.73 (12), p.1176 |
issn | 0021-9584 1938-1328 |
language | eng |
recordid | cdi_proquest_journals_211920657 |
source | American Chemical Society Journals |
subjects | Adjuncts Chloride Chromatography Climate Computers Dichloromethane Drinking water Environmental impact Environmental monitoring Environmental protection Esters Experiments Food Gas chromatography Identification Identification (Psychology) Inhalants Instrumentation Laboratories Laboratory Experiments Libraries Mass spectra Mass spectrometry Nitrogen Organic compounds Plasticizers Plastics Retention Scientific Concepts Scientific imaging Solvents Spectroscopy Temperature |
title | An Environmentally Significant Experiment Using GC/MS and GC Retention Indices in an Undergraduate Analytical Laboratory |
url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-22T14%3A50%3A23IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=An%20Environmentally%20Significant%20Experiment%20Using%20GC/MS%20and%20GC%20Retention%20Indices%20in%20an%20Undergraduate%20Analytical%20Laboratory&rft.jtitle=Journal%20of%20chemical%20education&rft.au=Guisto-Norkus,%20Rebecca&rft.date=1996-12-01&rft.volume=73&rft.issue=12&rft.spage=1176&rft.pages=1176-&rft.issn=0021-9584&rft.eissn=1938-1328&rft.coden=JCEDA8&rft_id=info:doi/10.1021/ed073p1176&rft_dat=%3Cproquest_cross%3E1096721281%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=211920657&rft_id=info:pmid/&rfr_iscdi=true |