Synthesis and Characterization of Functionalized Se-MCM-41 a New Drug Carrier Mesopore Composite
Various nanocomposite materials play a number of important roles in modern science and technology including pharmaceutical science. Among these materials, mesoporous materials cover a large number of applications in drug delivery system. The quantitative incorporation and high dispersion of selenium...
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| Veröffentlicht in: | Oriental journal of chemistry 2017-01, Vol.33 (2), p.611-621 |
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| container_title | Oriental journal of chemistry |
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| creator | M. Rahman, M. A.B.M. Aznan, M. M.Yusof, A. Ansary R, H. J. Siddiqi, M. Yusan, S. |
| description | Various nanocomposite materials play a number of important roles in modern science and technology including pharmaceutical science. Among these materials, mesoporous materials cover a large number of applications in drug delivery system. The quantitative incorporation and high dispersion of selenium nanoparticles into MCM-41 have been made possible by the coordination between Se(IV) ion and aminopropyltriethoxysilane (APTES)-anchored MCM-41. The samples were characterized by X-ray powder diffraction, Fourier-transformed infrared spectroscopy (FTIR), scanning electron microscopy (SEM), nitrogen adsorption–desorption via multi-point Brunauer, Emmett and Teller (BET) analysis, Raman spectroscopy and UV-Vis diffusion reflection spectroscopy (UV-vis/DRS). The increase in cell parameter and the decrease in surface area observed by N2 adsorption-desorption technique were taken as evidence of selenium introduction inside the MCM-41 framework. The behaviour of drug release in these nanocomposites is probably due to hydrogen bonding interactions between drug and the hydroxyl group on the composite framework. |
| doi_str_mv | 10.13005/ojc/330208 |
| format | Article |
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Rahman, M. ; A.B.M. Aznan, M. ; M.Yusof, A. ; Ansary R, H. ; J. Siddiqi, M. ; Yusan, S.</creator><creatorcontrib>M. Rahman, M. ; A.B.M. Aznan, M. ; M.Yusof, A. ; Ansary R, H. ; J. Siddiqi, M. ; Yusan, S.</creatorcontrib><description>Various nanocomposite materials play a number of important roles in modern science and technology including pharmaceutical science. Among these materials, mesoporous materials cover a large number of applications in drug delivery system. The quantitative incorporation and high dispersion of selenium nanoparticles into MCM-41 have been made possible by the coordination between Se(IV) ion and aminopropyltriethoxysilane (APTES)-anchored MCM-41. The samples were characterized by X-ray powder diffraction, Fourier-transformed infrared spectroscopy (FTIR), scanning electron microscopy (SEM), nitrogen adsorption–desorption via multi-point Brunauer, Emmett and Teller (BET) analysis, Raman spectroscopy and UV-Vis diffusion reflection spectroscopy (UV-vis/DRS). The increase in cell parameter and the decrease in surface area observed by N2 adsorption-desorption technique were taken as evidence of selenium introduction inside the MCM-41 framework. 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Siddiqi, M.</creatorcontrib><creatorcontrib>Yusan, S.</creatorcontrib><title>Synthesis and Characterization of Functionalized Se-MCM-41 a New Drug Carrier Mesopore Composite</title><title>Oriental journal of chemistry</title><description>Various nanocomposite materials play a number of important roles in modern science and technology including pharmaceutical science. Among these materials, mesoporous materials cover a large number of applications in drug delivery system. The quantitative incorporation and high dispersion of selenium nanoparticles into MCM-41 have been made possible by the coordination between Se(IV) ion and aminopropyltriethoxysilane (APTES)-anchored MCM-41. The samples were characterized by X-ray powder diffraction, Fourier-transformed infrared spectroscopy (FTIR), scanning electron microscopy (SEM), nitrogen adsorption–desorption via multi-point Brunauer, Emmett and Teller (BET) analysis, Raman spectroscopy and UV-Vis diffusion reflection spectroscopy (UV-vis/DRS). The increase in cell parameter and the decrease in surface area observed by N2 adsorption-desorption technique were taken as evidence of selenium introduction inside the MCM-41 framework. 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| subjects | Acids Adsorption Aminopropyltriethoxysilane Atoms & subatomic particles Desorption Drug carriers Drug delivery systems Fourier transforms Hydrogen bonding Hydroxyl groups Nanocomposites Nanoparticles Polymers Raman spectroscopy Scanning electron microscopy Selenium X ray powder diffraction Zeolites |
| title | Synthesis and Characterization of Functionalized Se-MCM-41 a New Drug Carrier Mesopore Composite |
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