X-ray peak profile analysis of zinc oxide nanoparticles formed by simple precipitation method
Zinc oxide (ZnO) nanoparticles were successfully synthesized by a simple precipitation method using zinc acetate and tetramethylammonium hydroxide. The synthesized ZnO nanoparticles were characterized by X-ray Diffraction analysis (XRD) and Transmission Electron Microscopy (TEM). The XRD result reve...
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| creator | Pelicano, Christian Mark Rapadas, Nick Joaquin Magdaluyo, Eduardo |
| description | Zinc oxide (ZnO) nanoparticles were successfully synthesized by a simple precipitation method using zinc acetate and tetramethylammonium hydroxide. The synthesized ZnO nanoparticles were characterized by X-ray Diffraction analysis (XRD) and Transmission Electron Microscopy (TEM). The XRD result revealed a hexagonal wurtzite structure for the ZnO nanoparticles. The TEM image showed spherical nanoparticles with an average crystallite size of 6.70 nm. For x-ray peak analysis, Williamson-Hall (W-H) and Size-Strain Plot (SSP) methods were applied to examine the effects of crystallite size and lattice strain on the peak broadening of the ZnO nanoparticles. Based on the calculations, the estimated crystallite sizes and lattice strains obtained are in good agreement with each other. |
| doi_str_mv | 10.1063/1.5010453 |
| format | Conference Proceeding |
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The synthesized ZnO nanoparticles were characterized by X-ray Diffraction analysis (XRD) and Transmission Electron Microscopy (TEM). The XRD result revealed a hexagonal wurtzite structure for the ZnO nanoparticles. The TEM image showed spherical nanoparticles with an average crystallite size of 6.70 nm. For x-ray peak analysis, Williamson-Hall (W-H) and Size-Strain Plot (SSP) methods were applied to examine the effects of crystallite size and lattice strain on the peak broadening of the ZnO nanoparticles. Based on the calculations, the estimated crystallite sizes and lattice strains obtained are in good agreement with each other.</description><identifier>ISSN: 0094-243X</identifier><identifier>EISSN: 1551-7616</identifier><identifier>DOI: 10.1063/1.5010453</identifier><identifier>CODEN: APCPCS</identifier><language>eng</language><publisher>Melville: American Institute of Physics</publisher><subject>Diffraction ; Lattice strain ; Nanoparticles ; Synthesis ; Transmission electron microscopy ; Wurtzite ; X-ray diffraction ; Zinc acetate ; Zinc oxide ; Zinc oxides</subject><ispartof>AIP Conference Proceedings, 2017, Vol.1901 (1)</ispartof><rights>Author(s)</rights><rights>2017 Author(s). 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The synthesized ZnO nanoparticles were characterized by X-ray Diffraction analysis (XRD) and Transmission Electron Microscopy (TEM). The XRD result revealed a hexagonal wurtzite structure for the ZnO nanoparticles. The TEM image showed spherical nanoparticles with an average crystallite size of 6.70 nm. For x-ray peak analysis, Williamson-Hall (W-H) and Size-Strain Plot (SSP) methods were applied to examine the effects of crystallite size and lattice strain on the peak broadening of the ZnO nanoparticles. Based on the calculations, the estimated crystallite sizes and lattice strains obtained are in good agreement with each other.</description><subject>Diffraction</subject><subject>Lattice strain</subject><subject>Nanoparticles</subject><subject>Synthesis</subject><subject>Transmission electron microscopy</subject><subject>Wurtzite</subject><subject>X-ray diffraction</subject><subject>Zinc acetate</subject><subject>Zinc oxide</subject><subject>Zinc oxides</subject><issn>0094-243X</issn><issn>1551-7616</issn><fulltext>true</fulltext><rsrctype>conference_proceeding</rsrctype><creationdate>2017</creationdate><recordtype>conference_proceeding</recordtype><recordid>eNp90MFKxDAQBuAgCq6rB98g4E3ommnatDnKoquw4EVhLxLSdoJZ2yYmXbE-vZVd8OZpLt8M8_-EXAJbABP8BhY5A5bl_IjMIM8hKQSIYzJjTGZJmvHNKTmLcctYKouinJHXTRL0SD3qd-qDM7ZFqnvdjtFG6gz9tn1N3ZdtkPa6d16HwdYtRmpc6LCh1Uij7fy05QPW1ttBD9b1tMPhzTXn5MToNuLFYc7Jy_3d8_IhWT-tHpe366ROJR-SKqsrLoAZLCU2UgqsAJoSM24AU51LIZHlFRaiznjBoeCTMKaRE-cMCz4nV_u7U4SPHcZBbd0uTDGiSgHEFL4s80ld71WsD28qH2ynw6iAqd_6FKhDff_hTxf-oPKN4T81lnGL</recordid><startdate>20171204</startdate><enddate>20171204</enddate><creator>Pelicano, Christian Mark</creator><creator>Rapadas, Nick Joaquin</creator><creator>Magdaluyo, Eduardo</creator><general>American Institute of Physics</general><scope>8FD</scope><scope>H8D</scope><scope>L7M</scope></search><sort><creationdate>20171204</creationdate><title>X-ray peak profile analysis of zinc oxide nanoparticles formed by simple precipitation method</title><author>Pelicano, Christian Mark ; Rapadas, Nick Joaquin ; Magdaluyo, Eduardo</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c293t-b4cb3610fe89ed996eb11d8e43f1e2a5969e05be76c43731736ebffd989e30e73</frbrgroupid><rsrctype>conference_proceedings</rsrctype><prefilter>conference_proceedings</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Diffraction</topic><topic>Lattice strain</topic><topic>Nanoparticles</topic><topic>Synthesis</topic><topic>Transmission electron microscopy</topic><topic>Wurtzite</topic><topic>X-ray diffraction</topic><topic>Zinc acetate</topic><topic>Zinc oxide</topic><topic>Zinc oxides</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Pelicano, Christian Mark</creatorcontrib><creatorcontrib>Rapadas, Nick Joaquin</creatorcontrib><creatorcontrib>Magdaluyo, Eduardo</creatorcontrib><collection>Technology Research Database</collection><collection>Aerospace Database</collection><collection>Advanced Technologies Database with Aerospace</collection></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Pelicano, Christian Mark</au><au>Rapadas, Nick Joaquin</au><au>Magdaluyo, Eduardo</au><au>Noorsal, Kartini</au><au>Ibrahim, Suhaina Mohd</au><format>book</format><genre>proceeding</genre><ristype>CONF</ristype><atitle>X-ray peak profile analysis of zinc oxide nanoparticles formed by simple precipitation method</atitle><btitle>AIP Conference Proceedings</btitle><date>2017-12-04</date><risdate>2017</risdate><volume>1901</volume><issue>1</issue><issn>0094-243X</issn><eissn>1551-7616</eissn><coden>APCPCS</coden><abstract>Zinc oxide (ZnO) nanoparticles were successfully synthesized by a simple precipitation method using zinc acetate and tetramethylammonium hydroxide. The synthesized ZnO nanoparticles were characterized by X-ray Diffraction analysis (XRD) and Transmission Electron Microscopy (TEM). The XRD result revealed a hexagonal wurtzite structure for the ZnO nanoparticles. The TEM image showed spherical nanoparticles with an average crystallite size of 6.70 nm. For x-ray peak analysis, Williamson-Hall (W-H) and Size-Strain Plot (SSP) methods were applied to examine the effects of crystallite size and lattice strain on the peak broadening of the ZnO nanoparticles. Based on the calculations, the estimated crystallite sizes and lattice strains obtained are in good agreement with each other.</abstract><cop>Melville</cop><pub>American Institute of Physics</pub><doi>10.1063/1.5010453</doi><tpages>6</tpages></addata></record> |
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| issn | 0094-243X 1551-7616 |
| language | eng |
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| source | AIP Journals Complete |
| subjects | Diffraction Lattice strain Nanoparticles Synthesis Transmission electron microscopy Wurtzite X-ray diffraction Zinc acetate Zinc oxide Zinc oxides |
| title | X-ray peak profile analysis of zinc oxide nanoparticles formed by simple precipitation method |
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