Role of In situ thermal‐reduced graphene oxide on the morphology and properties of biodegradable poly(Lactic acid)/poly(butylene succinate) blends
In this article, poly(lactic acid)/poly(butylene succinate)/reduced graphene oxide (PLA/PBS/RGO) nanocomposites were first prepared by the in situ thermal reduction of graphene oxide (GO) during the processing, and the influence of RGO on the morphology, thermal, and mechanical properties of biodegr...
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| Veröffentlicht in: | Polymer composites 2018-09, Vol.39 (9), p.3057-3065 |
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| creator | Wang, Dazhong Lu, Xiang Qu, Jinping |
| description | In this article, poly(lactic acid)/poly(butylene succinate)/reduced graphene oxide (PLA/PBS/RGO) nanocomposites were first prepared by the in situ thermal reduction of graphene oxide (GO) during the processing, and the influence of RGO on the morphology, thermal, and mechanical properties of biodegradable PLA/PBS blends were investigated. X‐ray photoelectron spectroscopy (XPS), Raman spectroscopy, and thermogravimetric analysis (TGA) showed that the GO was successfully in situ thermal reduced to RGO. Scanning electronic microscope (SEM) and dynamic mechanical properties (DMA) revealed that the adding of RGO enhanced the compatibility of PLA and PBS. DMA also indicated that higher storage modulus values were observed for PLA/PBS/RGO composites. The tensile strength and impact strength of the PLA/PBS/RGO composites increased with RGO content. POLYM. COMPOS., 39:3057–3065, 2018. © 2017 Society of Plastics Engineers |
| doi_str_mv | 10.1002/pc.24310 |
| format | Article |
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X‐ray photoelectron spectroscopy (XPS), Raman spectroscopy, and thermogravimetric analysis (TGA) showed that the GO was successfully in situ thermal reduced to RGO. Scanning electronic microscope (SEM) and dynamic mechanical properties (DMA) revealed that the adding of RGO enhanced the compatibility of PLA and PBS. DMA also indicated that higher storage modulus values were observed for PLA/PBS/RGO composites. The tensile strength and impact strength of the PLA/PBS/RGO composites increased with RGO content. POLYM. 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X‐ray photoelectron spectroscopy (XPS), Raman spectroscopy, and thermogravimetric analysis (TGA) showed that the GO was successfully in situ thermal reduced to RGO. Scanning electronic microscope (SEM) and dynamic mechanical properties (DMA) revealed that the adding of RGO enhanced the compatibility of PLA and PBS. DMA also indicated that higher storage modulus values were observed for PLA/PBS/RGO composites. The tensile strength and impact strength of the PLA/PBS/RGO composites increased with RGO content. POLYM. COMPOS., 39:3057–3065, 2018. © 2017 Society of Plastics Engineers</description><subject>Biodegradability</subject><subject>Dynamic mechanical properties</subject><subject>Graphene</subject><subject>Impact strength</subject><subject>Mechanical properties</subject><subject>Mixtures</subject><subject>Morphology</subject><subject>Nanocomposites</subject><subject>Polylactic acid</subject><subject>Polymers</subject><subject>Raman spectroscopy</subject><subject>Spectrum analysis</subject><subject>Storage modulus</subject><subject>Thermal reduction</subject><subject>Thermogravimetric analysis</subject><subject>X ray photoelectron spectroscopy</subject><issn>0272-8397</issn><issn>1548-0569</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNp10MtKAzEUBuAgCtYq-AgBN3UxbS5z6SyleCkUFNF1yOTSpkwnMZlBZ-cjuPAJfRIzrVs3CeR8-ZNzALjEaIoRIjMnpiSlGB2BEc7SeYKyvDwGI0QKksxpWZyCsxC2UeI8pyPw_WxrBa2GywYG03aw3Si_4_XP55dXshNKwrXnbqOaqD6MjGszGLiz3m1sbdc95I2EzlunfGtUGMIqY6WK9ySvYrqzdT9ZcdEaAbkw8nq2P6m6tq-H3NAJYRreqmsYeSPDOTjRvA7q4m8fg9e725fFQ7J6vF8ublaJoBShJM0wzaXkQpclRhxxTKSaC5VxnSFZUpXhKosVwouqFFgXXKexb6wrlFeEEjoGV4fc-Pu3ToWWbW3nm_gki4ykOS4xjWpyUMLbELzSzHmz475nGLFh5swJtp95pMmBvpta9f869rQ4-F_NgoTP</recordid><startdate>201809</startdate><enddate>201809</enddate><creator>Wang, Dazhong</creator><creator>Lu, Xiang</creator><creator>Qu, Jinping</creator><general>Blackwell Publishing Ltd</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>201809</creationdate><title>Role of In situ thermal‐reduced graphene oxide on the morphology and properties of biodegradable poly(Lactic acid)/poly(butylene succinate) blends</title><author>Wang, Dazhong ; Lu, Xiang ; Qu, Jinping</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3300-45136ddacf9910a0a12de8ce5af50d93e51b59102a7b9c1f7af40211fb06b2323</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Biodegradability</topic><topic>Dynamic mechanical properties</topic><topic>Graphene</topic><topic>Impact strength</topic><topic>Mechanical properties</topic><topic>Mixtures</topic><topic>Morphology</topic><topic>Nanocomposites</topic><topic>Polylactic acid</topic><topic>Polymers</topic><topic>Raman spectroscopy</topic><topic>Spectrum analysis</topic><topic>Storage modulus</topic><topic>Thermal reduction</topic><topic>Thermogravimetric analysis</topic><topic>X ray photoelectron spectroscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wang, Dazhong</creatorcontrib><creatorcontrib>Lu, Xiang</creatorcontrib><creatorcontrib>Qu, Jinping</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Polymer composites</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wang, Dazhong</au><au>Lu, Xiang</au><au>Qu, Jinping</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Role of In situ thermal‐reduced graphene oxide on the morphology and properties of biodegradable poly(Lactic acid)/poly(butylene succinate) blends</atitle><jtitle>Polymer composites</jtitle><date>2018-09</date><risdate>2018</risdate><volume>39</volume><issue>9</issue><spage>3057</spage><epage>3065</epage><pages>3057-3065</pages><issn>0272-8397</issn><eissn>1548-0569</eissn><abstract>In this article, poly(lactic acid)/poly(butylene succinate)/reduced graphene oxide (PLA/PBS/RGO) nanocomposites were first prepared by the in situ thermal reduction of graphene oxide (GO) during the processing, and the influence of RGO on the morphology, thermal, and mechanical properties of biodegradable PLA/PBS blends were investigated. X‐ray photoelectron spectroscopy (XPS), Raman spectroscopy, and thermogravimetric analysis (TGA) showed that the GO was successfully in situ thermal reduced to RGO. Scanning electronic microscope (SEM) and dynamic mechanical properties (DMA) revealed that the adding of RGO enhanced the compatibility of PLA and PBS. DMA also indicated that higher storage modulus values were observed for PLA/PBS/RGO composites. The tensile strength and impact strength of the PLA/PBS/RGO composites increased with RGO content. POLYM. COMPOS., 39:3057–3065, 2018. © 2017 Society of Plastics Engineers</abstract><cop>Newtown</cop><pub>Blackwell Publishing Ltd</pub><doi>10.1002/pc.24310</doi><tpages>9</tpages></addata></record> |
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| source | Wiley Online Library Journals Frontfile Complete |
| subjects | Biodegradability Dynamic mechanical properties Graphene Impact strength Mechanical properties Mixtures Morphology Nanocomposites Polylactic acid Polymers Raman spectroscopy Spectrum analysis Storage modulus Thermal reduction Thermogravimetric analysis X ray photoelectron spectroscopy |
| title | Role of In situ thermal‐reduced graphene oxide on the morphology and properties of biodegradable poly(Lactic acid)/poly(butylene succinate) blends |
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