Fast scanning voltammetric detector for high performance liquid chromatography
This article describes the application of fast scan differential pulse voltammetry on a glassy carbon electrode as a working electrode in a wall-jet arrangement in combination with a high performance liquid chromatography. During the characterization of electrochemical detection, the separability, t...
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| Veröffentlicht in: | Electrochimica acta 2018-08, Vol.281, p.534-539 |
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| container_title | Electrochimica acta |
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| creator | Bavol, Dmytro Scampicchio, Matteo Zima, Jiri Barek, Jiri Dejmkova, Hana |
| description | This article describes the application of fast scan differential pulse voltammetry on a glassy carbon electrode as a working electrode in a wall-jet arrangement in combination with a high performance liquid chromatography. During the characterization of electrochemical detection, the separability, the repeatability, and the concentration characteristics for determination of common antioxidants in standard solutions were found. Finally, as an application of the technique, the optimized procedure has been used for the first time to determine antioxidants contained in tea samples by applying a simple extraction procedure.
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•The possibilities of the technique in combination with HPLC were successfully tested.•The main weaknesses of the FSDPV technique were discussed.•Successful determination of antioxidants in tea samples was carried out. |
| doi_str_mv | 10.1016/j.electacta.2018.05.199 |
| format | Article |
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[Display omitted]
•The possibilities of the technique in combination with HPLC were successfully tested.•The main weaknesses of the FSDPV technique were discussed.•Successful determination of antioxidants in tea samples was carried out.</description><identifier>ISSN: 0013-4686</identifier><identifier>EISSN: 1873-3859</identifier><identifier>DOI: 10.1016/j.electacta.2018.05.199</identifier><language>eng</language><publisher>Oxford: Elsevier Ltd</publisher><subject>Antioxidants ; Chromatography ; Electrochemical analysis ; Electrodes ; Fast scan differential pulse voltammetry ; Glassy carbon ; Glassy carbon electrode ; High performance liquid chromatography ; Voltammetry</subject><ispartof>Electrochimica acta, 2018-08, Vol.281, p.534-539</ispartof><rights>2018 Elsevier Ltd</rights><rights>Copyright Elsevier BV Aug 10, 2018</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c446t-5fc39440bdedd1254456bc58755a04577b8bd6b178e11b7fadd2d1bb5c77860a3</citedby><cites>FETCH-LOGICAL-c446t-5fc39440bdedd1254456bc58755a04577b8bd6b178e11b7fadd2d1bb5c77860a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0013468618312660$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65534</link.rule.ids></links><search><creatorcontrib>Bavol, Dmytro</creatorcontrib><creatorcontrib>Scampicchio, Matteo</creatorcontrib><creatorcontrib>Zima, Jiri</creatorcontrib><creatorcontrib>Barek, Jiri</creatorcontrib><creatorcontrib>Dejmkova, Hana</creatorcontrib><title>Fast scanning voltammetric detector for high performance liquid chromatography</title><title>Electrochimica acta</title><description>This article describes the application of fast scan differential pulse voltammetry on a glassy carbon electrode as a working electrode in a wall-jet arrangement in combination with a high performance liquid chromatography. During the characterization of electrochemical detection, the separability, the repeatability, and the concentration characteristics for determination of common antioxidants in standard solutions were found. Finally, as an application of the technique, the optimized procedure has been used for the first time to determine antioxidants contained in tea samples by applying a simple extraction procedure.
[Display omitted]
•The possibilities of the technique in combination with HPLC were successfully tested.•The main weaknesses of the FSDPV technique were discussed.•Successful determination of antioxidants in tea samples was carried out.</description><subject>Antioxidants</subject><subject>Chromatography</subject><subject>Electrochemical analysis</subject><subject>Electrodes</subject><subject>Fast scan differential pulse voltammetry</subject><subject>Glassy carbon</subject><subject>Glassy carbon electrode</subject><subject>High performance liquid chromatography</subject><subject>Voltammetry</subject><issn>0013-4686</issn><issn>1873-3859</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNqFkFtLAzEQhYMoWKu_wQWfd012c9vHUqwKRV_0OeS23Sx7a5IW-u9NqfgqzDDzcOYM5wPgEcECQUSfu8L2VkeZqigh4gUkBarrK7BAnFV5xUl9DRYQoirHlNNbcBdCByFklMEF-NjIELOg5Ti6cZcdpz7KYbDRO50ZG5Px5LMmdet2bTZbn_ZBjtpmvdsfnMl066dBxmnn5dye7sFNI_tgH37nEnxvXr7Wb_n28_V9vdrmGmMac9LoqsYYKmONQSXBmFClCWeESIgJY4orQxVi3CKkWCONKQ1SimjGOIWyWoKni-_sp_3Bhii66eDH9FKUCCFGKgppUrGLSvspBG8bMXs3SH8SCIozPNGJP3jiDE9AIhK8dLm6XNoU4uisF0E7m2Ib55NemMn96_EDNVB9uw</recordid><startdate>20180810</startdate><enddate>20180810</enddate><creator>Bavol, Dmytro</creator><creator>Scampicchio, Matteo</creator><creator>Zima, Jiri</creator><creator>Barek, Jiri</creator><creator>Dejmkova, Hana</creator><general>Elsevier Ltd</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20180810</creationdate><title>Fast scanning voltammetric detector for high performance liquid chromatography</title><author>Bavol, Dmytro ; Scampicchio, Matteo ; Zima, Jiri ; Barek, Jiri ; Dejmkova, Hana</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c446t-5fc39440bdedd1254456bc58755a04577b8bd6b178e11b7fadd2d1bb5c77860a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Antioxidants</topic><topic>Chromatography</topic><topic>Electrochemical analysis</topic><topic>Electrodes</topic><topic>Fast scan differential pulse voltammetry</topic><topic>Glassy carbon</topic><topic>Glassy carbon electrode</topic><topic>High performance liquid chromatography</topic><topic>Voltammetry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bavol, Dmytro</creatorcontrib><creatorcontrib>Scampicchio, Matteo</creatorcontrib><creatorcontrib>Zima, Jiri</creatorcontrib><creatorcontrib>Barek, Jiri</creatorcontrib><creatorcontrib>Dejmkova, Hana</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Electrochimica acta</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bavol, Dmytro</au><au>Scampicchio, Matteo</au><au>Zima, Jiri</au><au>Barek, Jiri</au><au>Dejmkova, Hana</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Fast scanning voltammetric detector for high performance liquid chromatography</atitle><jtitle>Electrochimica acta</jtitle><date>2018-08-10</date><risdate>2018</risdate><volume>281</volume><spage>534</spage><epage>539</epage><pages>534-539</pages><issn>0013-4686</issn><eissn>1873-3859</eissn><abstract>This article describes the application of fast scan differential pulse voltammetry on a glassy carbon electrode as a working electrode in a wall-jet arrangement in combination with a high performance liquid chromatography. During the characterization of electrochemical detection, the separability, the repeatability, and the concentration characteristics for determination of common antioxidants in standard solutions were found. Finally, as an application of the technique, the optimized procedure has been used for the first time to determine antioxidants contained in tea samples by applying a simple extraction procedure.
[Display omitted]
•The possibilities of the technique in combination with HPLC were successfully tested.•The main weaknesses of the FSDPV technique were discussed.•Successful determination of antioxidants in tea samples was carried out.</abstract><cop>Oxford</cop><pub>Elsevier Ltd</pub><doi>10.1016/j.electacta.2018.05.199</doi><tpages>6</tpages></addata></record> |
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| ispartof | Electrochimica acta, 2018-08, Vol.281, p.534-539 |
| issn | 0013-4686 1873-3859 |
| language | eng |
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| source | Elsevier ScienceDirect Journals Complete |
| subjects | Antioxidants Chromatography Electrochemical analysis Electrodes Fast scan differential pulse voltammetry Glassy carbon Glassy carbon electrode High performance liquid chromatography Voltammetry |
| title | Fast scanning voltammetric detector for high performance liquid chromatography |
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