Fabrication, structural and electrical properties of Sr(V,Nb)O^sub 3-d^ perovskite materials
The SrV1-xNbxO3-δ materials with different niobium content in perovskite B-sublattice were prepared by a solid-state reaction process. The microstructure and phase compositions of obtained samples were analyzed by the X-ray diffraction technique (XRD) and scanning electron microscopy (SEM). The elec...
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| Veröffentlicht in: | Materials chemistry and physics 2018-06, Vol.212, p.446 |
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| creator | Miruszewski, T Kamecki, B Lapinski, M Karczewski, J |
| description | The SrV1-xNbxO3-δ materials with different niobium content in perovskite B-sublattice were prepared by a solid-state reaction process. The microstructure and phase compositions of obtained samples were analyzed by the X-ray diffraction technique (XRD) and scanning electron microscopy (SEM). The electrical conductivity of samples was measured by a DC 4-wire method in range of 100–600 °C in different gas conditions. The oxidation state of the niobium and vanadium cations in the structure was determined by the X-ray photoelectron spectroscopy (XPS). The obtained results were discussed and analyzed in comparison to the previous literature reports and defect chemistry models. |
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The microstructure and phase compositions of obtained samples were analyzed by the X-ray diffraction technique (XRD) and scanning electron microscopy (SEM). The electrical conductivity of samples was measured by a DC 4-wire method in range of 100–600 °C in different gas conditions. The oxidation state of the niobium and vanadium cations in the structure was determined by the X-ray photoelectron spectroscopy (XPS). 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The microstructure and phase compositions of obtained samples were analyzed by the X-ray diffraction technique (XRD) and scanning electron microscopy (SEM). The electrical conductivity of samples was measured by a DC 4-wire method in range of 100–600 °C in different gas conditions. The oxidation state of the niobium and vanadium cations in the structure was determined by the X-ray photoelectron spectroscopy (XPS). The obtained results were discussed and analyzed in comparison to the previous literature reports and defect chemistry models.</abstract><cop>Lausanne</cop><pub>Elsevier BV</pub></addata></record> |
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| language | eng |
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| source | Elsevier ScienceDirect Journals |
| subjects | Electric properties Electric wire Electrical properties Electrical resistivity Microstructure Niobium Organic chemistry Oxidation Perovskite Perovskites Scanning electron microscopy Valence X ray photoelectron spectroscopy X-ray diffraction |
| title | Fabrication, structural and electrical properties of Sr(V,Nb)O^sub 3-d^ perovskite materials |
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