Preparation of polystyrene-b-poly(ethylene/propylene)-b-polystyrene grafted glycidyl methacrylate and its compatibility with recycled polypropylene/recycled high impact polystyrene blends
In this study, polystyrene-b-poly (ethylene/propylene)-b-polystyrene grafted glycidyl methacrylate (SEPS-g-GMA) copolymer was prepared by melt grafting in the mixer. The successful grafting of GMA on the SEPS molecular chain was analyzed by Fourier transform infrared spectroscopy (FT-IR). The grafti...
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| Veröffentlicht in: | Polymer (Guilford) 2018-06, Vol.145, p.232-241 |
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| creator | Kong, Yufei Li, Yingchun Hu, Guosheng Lin, Jing Pan, Duo Dong, Dongyao Wujick, Evan Shao, Qian Wu, Minjian Zhao, Jizhang Guo, Zhanhu |
| description | In this study, polystyrene-b-poly (ethylene/propylene)-b-polystyrene grafted glycidyl methacrylate (SEPS-g-GMA) copolymer was prepared by melt grafting in the mixer. The successful grafting of GMA on the SEPS molecular chain was analyzed by Fourier transform infrared spectroscopy (FT-IR). The grafting ratio of SEPS-g-GMA was measured by acid-base titration, which showed that N-vinylpyrrolidone (NVP) had a positive effect on the increased grafting ratio of SEPS-g-GMA. The recycled polypropylene (R-PP)/recycled high impact polystyrene (R-HIPS) blends were prepared by a melt extrusion, and the effect of SEPS-g-GMA copolymer with different ratios on the compatibility of blends was studied. The epoxy groups in SEPS-g-GMA copolymer were found to have a chemical reaction with the carboxyl groups in the waste materials. When the grafting ratio of SEPS-g-GMA was 2.44%, the notched impact strength and the elongation at break of the R-PP/R-HIPS blends with 10 phr SEPS-g-GMA reached 7.06 kJ/m2 and 34.25%, which were significantly increased by 186.99% and 68.30% compared with that of pure blends, respectively. Moreover, the observed decreased particle size and increased dispersion uniformity improved the compatibility using SEPS-g-GMA. The increased complex viscosity, storage modulus and loss modulus indicated that the chemical reaction between SEPS-g-GMA and R-PP/R-HIPS blends improved the component compatibility among the blends, resulting in the chain entanglement prominently. The presence of SEPS-g-GMA inhibited the degradation and increased the thermal stability of R-PP/R-HIPS blends.
[Display omitted]
•SEPS-g-GMA was successfully prepared and the effect of NVP content on the grafting ratio of SEPS-g-GMA was tested.•The notch impact strength of R-PP/R-HIPS blends was improved by 186.99% when the SEPS-g-GMA (G = 2.44%) content was 10 phr.•The compatibilization mechanism of SEPS-g-GMA to R-PP/R-HIPS blends was explained.•The SEPS-g-GMA compatibilization effect on R-PP/R-HIPS blends was interpreted. |
| doi_str_mv | 10.1016/j.polymer.2018.05.017 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2082632960</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S0032386118304117</els_id><sourcerecordid>2082632960</sourcerecordid><originalsourceid>FETCH-LOGICAL-c374t-7087592501570250830717739a23203ee8d0f545b460083766a3b94eb74cf9a23</originalsourceid><addsrcrecordid>eNqFUc1u1DAQtlCR2BYeAckSFzgkO7bjODkhVAGtVAkOcLYcZ7LrVTYJtkvlZ-PlcLqrqree7PH3MzP-CHnPoGTA6u2hXOYxHdGXHFhTgiyBqVdkwxolCs5bdkE2AIIXoqnZG3IZwgEAuOTVhvz76XEx3kQ3T3Qe6OoUYvI4YdEVa_UR4z6Nud4ufl4eb5_O0JlId94MEXu6G5N1fRrpMWuM9Wk0EamZeupioHY-LrlP50YXE31wcU892mTHrFzdnuy3T897t9tTl2U2Pp-MdpnWh7fk9WDGgO_O5xX5_e3rr-ub4u7H99vrL3eFFaqKhYJGyZZLYFLlraERoJhSojVccBCITQ-DrGRX1ZBBVddGdG2FnarssJKuyIeTb57wzz2GqA_zvZ9yS82h4bXgbQ2ZJU8s6-cQPA568e5ofNIM9JqTPuhzTnrNSYPUOaes-3zSYV7hr8tosA4ni73L_xB1P7sXHP4Dy36kMw</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2082632960</pqid></control><display><type>article</type><title>Preparation of polystyrene-b-poly(ethylene/propylene)-b-polystyrene grafted glycidyl methacrylate and its compatibility with recycled polypropylene/recycled high impact polystyrene blends</title><source>Elsevier ScienceDirect Journals Complete</source><creator>Kong, Yufei ; Li, Yingchun ; Hu, Guosheng ; Lin, Jing ; Pan, Duo ; Dong, Dongyao ; Wujick, Evan ; Shao, Qian ; Wu, Minjian ; Zhao, Jizhang ; Guo, Zhanhu</creator><creatorcontrib>Kong, Yufei ; Li, Yingchun ; Hu, Guosheng ; Lin, Jing ; Pan, Duo ; Dong, Dongyao ; Wujick, Evan ; Shao, Qian ; Wu, Minjian ; Zhao, Jizhang ; Guo, Zhanhu</creatorcontrib><description>In this study, polystyrene-b-poly (ethylene/propylene)-b-polystyrene grafted glycidyl methacrylate (SEPS-g-GMA) copolymer was prepared by melt grafting in the mixer. The successful grafting of GMA on the SEPS molecular chain was analyzed by Fourier transform infrared spectroscopy (FT-IR). The grafting ratio of SEPS-g-GMA was measured by acid-base titration, which showed that N-vinylpyrrolidone (NVP) had a positive effect on the increased grafting ratio of SEPS-g-GMA. The recycled polypropylene (R-PP)/recycled high impact polystyrene (R-HIPS) blends were prepared by a melt extrusion, and the effect of SEPS-g-GMA copolymer with different ratios on the compatibility of blends was studied. The epoxy groups in SEPS-g-GMA copolymer were found to have a chemical reaction with the carboxyl groups in the waste materials. When the grafting ratio of SEPS-g-GMA was 2.44%, the notched impact strength and the elongation at break of the R-PP/R-HIPS blends with 10 phr SEPS-g-GMA reached 7.06 kJ/m2 and 34.25%, which were significantly increased by 186.99% and 68.30% compared with that of pure blends, respectively. Moreover, the observed decreased particle size and increased dispersion uniformity improved the compatibility using SEPS-g-GMA. The increased complex viscosity, storage modulus and loss modulus indicated that the chemical reaction between SEPS-g-GMA and R-PP/R-HIPS blends improved the component compatibility among the blends, resulting in the chain entanglement prominently. The presence of SEPS-g-GMA inhibited the degradation and increased the thermal stability of R-PP/R-HIPS blends.
[Display omitted]
•SEPS-g-GMA was successfully prepared and the effect of NVP content on the grafting ratio of SEPS-g-GMA was tested.•The notch impact strength of R-PP/R-HIPS blends was improved by 186.99% when the SEPS-g-GMA (G = 2.44%) content was 10 phr.•The compatibilization mechanism of SEPS-g-GMA to R-PP/R-HIPS blends was explained.•The SEPS-g-GMA compatibilization effect on R-PP/R-HIPS blends was interpreted.</description><identifier>ISSN: 0032-3861</identifier><identifier>EISSN: 1873-2291</identifier><identifier>DOI: 10.1016/j.polymer.2018.05.017</identifier><language>eng</language><publisher>Kidlington: Elsevier Ltd</publisher><subject>Biocompatibility ; Chain entanglement ; Chemical reactions ; Compatibility ; Compatibilization ; Copolymers ; Elongation ; Entanglement ; Ethylene ; Extrusion ; Fourier transforms ; Graft copolymers ; Hip ; Impact strength ; Infrared analysis ; Infrared spectroscopy ; Loss modulus ; Molecular chains ; Organic chemistry ; Polymer blends ; Polymers ; Polymethyl methacrylate ; Polypropylene ; Polystyrene ; Polystyrene resins ; Propylene ; Recycled high impact polystyrene ; Recycled polypropylene ; Storage modulus ; Thermal stability ; Titration ; Vinylpyrrolidone ; Viscosity ; Waste materials</subject><ispartof>Polymer (Guilford), 2018-06, Vol.145, p.232-241</ispartof><rights>2018 Elsevier Ltd</rights><rights>Copyright Elsevier BV Jun 6, 2018</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c374t-7087592501570250830717739a23203ee8d0f545b460083766a3b94eb74cf9a23</citedby><cites>FETCH-LOGICAL-c374t-7087592501570250830717739a23203ee8d0f545b460083766a3b94eb74cf9a23</cites><orcidid>0000-0003-0134-0210 ; 0000-0002-4966-863X</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.polymer.2018.05.017$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,780,784,3548,27922,27923,45993</link.rule.ids></links><search><creatorcontrib>Kong, Yufei</creatorcontrib><creatorcontrib>Li, Yingchun</creatorcontrib><creatorcontrib>Hu, Guosheng</creatorcontrib><creatorcontrib>Lin, Jing</creatorcontrib><creatorcontrib>Pan, Duo</creatorcontrib><creatorcontrib>Dong, Dongyao</creatorcontrib><creatorcontrib>Wujick, Evan</creatorcontrib><creatorcontrib>Shao, Qian</creatorcontrib><creatorcontrib>Wu, Minjian</creatorcontrib><creatorcontrib>Zhao, Jizhang</creatorcontrib><creatorcontrib>Guo, Zhanhu</creatorcontrib><title>Preparation of polystyrene-b-poly(ethylene/propylene)-b-polystyrene grafted glycidyl methacrylate and its compatibility with recycled polypropylene/recycled high impact polystyrene blends</title><title>Polymer (Guilford)</title><description>In this study, polystyrene-b-poly (ethylene/propylene)-b-polystyrene grafted glycidyl methacrylate (SEPS-g-GMA) copolymer was prepared by melt grafting in the mixer. The successful grafting of GMA on the SEPS molecular chain was analyzed by Fourier transform infrared spectroscopy (FT-IR). The grafting ratio of SEPS-g-GMA was measured by acid-base titration, which showed that N-vinylpyrrolidone (NVP) had a positive effect on the increased grafting ratio of SEPS-g-GMA. The recycled polypropylene (R-PP)/recycled high impact polystyrene (R-HIPS) blends were prepared by a melt extrusion, and the effect of SEPS-g-GMA copolymer with different ratios on the compatibility of blends was studied. The epoxy groups in SEPS-g-GMA copolymer were found to have a chemical reaction with the carboxyl groups in the waste materials. When the grafting ratio of SEPS-g-GMA was 2.44%, the notched impact strength and the elongation at break of the R-PP/R-HIPS blends with 10 phr SEPS-g-GMA reached 7.06 kJ/m2 and 34.25%, which were significantly increased by 186.99% and 68.30% compared with that of pure blends, respectively. Moreover, the observed decreased particle size and increased dispersion uniformity improved the compatibility using SEPS-g-GMA. The increased complex viscosity, storage modulus and loss modulus indicated that the chemical reaction between SEPS-g-GMA and R-PP/R-HIPS blends improved the component compatibility among the blends, resulting in the chain entanglement prominently. The presence of SEPS-g-GMA inhibited the degradation and increased the thermal stability of R-PP/R-HIPS blends.
[Display omitted]
•SEPS-g-GMA was successfully prepared and the effect of NVP content on the grafting ratio of SEPS-g-GMA was tested.•The notch impact strength of R-PP/R-HIPS blends was improved by 186.99% when the SEPS-g-GMA (G = 2.44%) content was 10 phr.•The compatibilization mechanism of SEPS-g-GMA to R-PP/R-HIPS blends was explained.•The SEPS-g-GMA compatibilization effect on R-PP/R-HIPS blends was interpreted.</description><subject>Biocompatibility</subject><subject>Chain entanglement</subject><subject>Chemical reactions</subject><subject>Compatibility</subject><subject>Compatibilization</subject><subject>Copolymers</subject><subject>Elongation</subject><subject>Entanglement</subject><subject>Ethylene</subject><subject>Extrusion</subject><subject>Fourier transforms</subject><subject>Graft copolymers</subject><subject>Hip</subject><subject>Impact strength</subject><subject>Infrared analysis</subject><subject>Infrared spectroscopy</subject><subject>Loss modulus</subject><subject>Molecular chains</subject><subject>Organic chemistry</subject><subject>Polymer blends</subject><subject>Polymers</subject><subject>Polymethyl methacrylate</subject><subject>Polypropylene</subject><subject>Polystyrene</subject><subject>Polystyrene resins</subject><subject>Propylene</subject><subject>Recycled high impact polystyrene</subject><subject>Recycled polypropylene</subject><subject>Storage modulus</subject><subject>Thermal stability</subject><subject>Titration</subject><subject>Vinylpyrrolidone</subject><subject>Viscosity</subject><subject>Waste materials</subject><issn>0032-3861</issn><issn>1873-2291</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNqFUc1u1DAQtlCR2BYeAckSFzgkO7bjODkhVAGtVAkOcLYcZ7LrVTYJtkvlZ-PlcLqrqree7PH3MzP-CHnPoGTA6u2hXOYxHdGXHFhTgiyBqVdkwxolCs5bdkE2AIIXoqnZG3IZwgEAuOTVhvz76XEx3kQ3T3Qe6OoUYvI4YdEVa_UR4z6Nud4ufl4eb5_O0JlId94MEXu6G5N1fRrpMWuM9Wk0EamZeupioHY-LrlP50YXE31wcU892mTHrFzdnuy3T897t9tTl2U2Pp-MdpnWh7fk9WDGgO_O5xX5_e3rr-ub4u7H99vrL3eFFaqKhYJGyZZLYFLlraERoJhSojVccBCITQ-DrGRX1ZBBVddGdG2FnarssJKuyIeTb57wzz2GqA_zvZ9yS82h4bXgbQ2ZJU8s6-cQPA568e5ofNIM9JqTPuhzTnrNSYPUOaes-3zSYV7hr8tosA4ni73L_xB1P7sXHP4Dy36kMw</recordid><startdate>20180606</startdate><enddate>20180606</enddate><creator>Kong, Yufei</creator><creator>Li, Yingchun</creator><creator>Hu, Guosheng</creator><creator>Lin, Jing</creator><creator>Pan, Duo</creator><creator>Dong, Dongyao</creator><creator>Wujick, Evan</creator><creator>Shao, Qian</creator><creator>Wu, Minjian</creator><creator>Zhao, Jizhang</creator><creator>Guo, Zhanhu</creator><general>Elsevier Ltd</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QF</scope><scope>7QO</scope><scope>7QQ</scope><scope>7SC</scope><scope>7SE</scope><scope>7SP</scope><scope>7SR</scope><scope>7T7</scope><scope>7TA</scope><scope>7TB</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>C1K</scope><scope>F28</scope><scope>FR3</scope><scope>H8D</scope><scope>H8G</scope><scope>JG9</scope><scope>JQ2</scope><scope>KR7</scope><scope>L7M</scope><scope>L~C</scope><scope>L~D</scope><scope>P64</scope><orcidid>https://orcid.org/0000-0003-0134-0210</orcidid><orcidid>https://orcid.org/0000-0002-4966-863X</orcidid></search><sort><creationdate>20180606</creationdate><title>Preparation of polystyrene-b-poly(ethylene/propylene)-b-polystyrene grafted glycidyl methacrylate and its compatibility with recycled polypropylene/recycled high impact polystyrene blends</title><author>Kong, Yufei ; Li, Yingchun ; Hu, Guosheng ; Lin, Jing ; Pan, Duo ; Dong, Dongyao ; Wujick, Evan ; Shao, Qian ; Wu, Minjian ; Zhao, Jizhang ; Guo, Zhanhu</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c374t-7087592501570250830717739a23203ee8d0f545b460083766a3b94eb74cf9a23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Biocompatibility</topic><topic>Chain entanglement</topic><topic>Chemical reactions</topic><topic>Compatibility</topic><topic>Compatibilization</topic><topic>Copolymers</topic><topic>Elongation</topic><topic>Entanglement</topic><topic>Ethylene</topic><topic>Extrusion</topic><topic>Fourier transforms</topic><topic>Graft copolymers</topic><topic>Hip</topic><topic>Impact strength</topic><topic>Infrared analysis</topic><topic>Infrared spectroscopy</topic><topic>Loss modulus</topic><topic>Molecular chains</topic><topic>Organic chemistry</topic><topic>Polymer blends</topic><topic>Polymers</topic><topic>Polymethyl methacrylate</topic><topic>Polypropylene</topic><topic>Polystyrene</topic><topic>Polystyrene resins</topic><topic>Propylene</topic><topic>Recycled high impact polystyrene</topic><topic>Recycled polypropylene</topic><topic>Storage modulus</topic><topic>Thermal stability</topic><topic>Titration</topic><topic>Vinylpyrrolidone</topic><topic>Viscosity</topic><topic>Waste materials</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Kong, Yufei</creatorcontrib><creatorcontrib>Li, Yingchun</creatorcontrib><creatorcontrib>Hu, Guosheng</creatorcontrib><creatorcontrib>Lin, Jing</creatorcontrib><creatorcontrib>Pan, Duo</creatorcontrib><creatorcontrib>Dong, Dongyao</creatorcontrib><creatorcontrib>Wujick, Evan</creatorcontrib><creatorcontrib>Shao, Qian</creatorcontrib><creatorcontrib>Wu, Minjian</creatorcontrib><creatorcontrib>Zhao, Jizhang</creatorcontrib><creatorcontrib>Guo, Zhanhu</creatorcontrib><collection>CrossRef</collection><collection>Aluminium Industry Abstracts</collection><collection>Biotechnology Research Abstracts</collection><collection>Ceramic Abstracts</collection><collection>Computer and Information Systems Abstracts</collection><collection>Corrosion Abstracts</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Industrial and Applied Microbiology Abstracts (Microbiology A)</collection><collection>Materials Business File</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Aerospace Database</collection><collection>Copper Technical Reference Library</collection><collection>Materials Research Database</collection><collection>ProQuest Computer Science Collection</collection><collection>Civil Engineering Abstracts</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Computer and Information Systems Abstracts Academic</collection><collection>Computer and Information Systems Abstracts Professional</collection><collection>Biotechnology and BioEngineering Abstracts</collection><jtitle>Polymer (Guilford)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kong, Yufei</au><au>Li, Yingchun</au><au>Hu, Guosheng</au><au>Lin, Jing</au><au>Pan, Duo</au><au>Dong, Dongyao</au><au>Wujick, Evan</au><au>Shao, Qian</au><au>Wu, Minjian</au><au>Zhao, Jizhang</au><au>Guo, Zhanhu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation of polystyrene-b-poly(ethylene/propylene)-b-polystyrene grafted glycidyl methacrylate and its compatibility with recycled polypropylene/recycled high impact polystyrene blends</atitle><jtitle>Polymer (Guilford)</jtitle><date>2018-06-06</date><risdate>2018</risdate><volume>145</volume><spage>232</spage><epage>241</epage><pages>232-241</pages><issn>0032-3861</issn><eissn>1873-2291</eissn><abstract>In this study, polystyrene-b-poly (ethylene/propylene)-b-polystyrene grafted glycidyl methacrylate (SEPS-g-GMA) copolymer was prepared by melt grafting in the mixer. The successful grafting of GMA on the SEPS molecular chain was analyzed by Fourier transform infrared spectroscopy (FT-IR). The grafting ratio of SEPS-g-GMA was measured by acid-base titration, which showed that N-vinylpyrrolidone (NVP) had a positive effect on the increased grafting ratio of SEPS-g-GMA. The recycled polypropylene (R-PP)/recycled high impact polystyrene (R-HIPS) blends were prepared by a melt extrusion, and the effect of SEPS-g-GMA copolymer with different ratios on the compatibility of blends was studied. The epoxy groups in SEPS-g-GMA copolymer were found to have a chemical reaction with the carboxyl groups in the waste materials. When the grafting ratio of SEPS-g-GMA was 2.44%, the notched impact strength and the elongation at break of the R-PP/R-HIPS blends with 10 phr SEPS-g-GMA reached 7.06 kJ/m2 and 34.25%, which were significantly increased by 186.99% and 68.30% compared with that of pure blends, respectively. Moreover, the observed decreased particle size and increased dispersion uniformity improved the compatibility using SEPS-g-GMA. The increased complex viscosity, storage modulus and loss modulus indicated that the chemical reaction between SEPS-g-GMA and R-PP/R-HIPS blends improved the component compatibility among the blends, resulting in the chain entanglement prominently. The presence of SEPS-g-GMA inhibited the degradation and increased the thermal stability of R-PP/R-HIPS blends.
[Display omitted]
•SEPS-g-GMA was successfully prepared and the effect of NVP content on the grafting ratio of SEPS-g-GMA was tested.•The notch impact strength of R-PP/R-HIPS blends was improved by 186.99% when the SEPS-g-GMA (G = 2.44%) content was 10 phr.•The compatibilization mechanism of SEPS-g-GMA to R-PP/R-HIPS blends was explained.•The SEPS-g-GMA compatibilization effect on R-PP/R-HIPS blends was interpreted.</abstract><cop>Kidlington</cop><pub>Elsevier Ltd</pub><doi>10.1016/j.polymer.2018.05.017</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0003-0134-0210</orcidid><orcidid>https://orcid.org/0000-0002-4966-863X</orcidid></addata></record> |
| fulltext | fulltext |
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| ispartof | Polymer (Guilford), 2018-06, Vol.145, p.232-241 |
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| language | eng |
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| source | Elsevier ScienceDirect Journals Complete |
| subjects | Biocompatibility Chain entanglement Chemical reactions Compatibility Compatibilization Copolymers Elongation Entanglement Ethylene Extrusion Fourier transforms Graft copolymers Hip Impact strength Infrared analysis Infrared spectroscopy Loss modulus Molecular chains Organic chemistry Polymer blends Polymers Polymethyl methacrylate Polypropylene Polystyrene Polystyrene resins Propylene Recycled high impact polystyrene Recycled polypropylene Storage modulus Thermal stability Titration Vinylpyrrolidone Viscosity Waste materials |
| title | Preparation of polystyrene-b-poly(ethylene/propylene)-b-polystyrene grafted glycidyl methacrylate and its compatibility with recycled polypropylene/recycled high impact polystyrene blends |
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