Taguchi Analysis of Relation Between Tensile Strength and Interfacial Phases Quantified via Image Processing

Quantitative analysis was performed via image processing to identify the relationship between the tensile strength and the thickness of the Cr x B y phase layer at the interface of brazed 304 stainless steel with Ni-based filler metal (MBF20). The experimental design was based on the Taguchi method...

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Veröffentlicht in:Metallurgical and materials transactions. A, Physical metallurgy and materials science Physical metallurgy and materials science, 2018-10, Vol.49 (10), p.4684-4699
Hauptverfasser: Park, Dong Yong, Lee, Sun Kyu, Oh, Yong Jun
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description Quantitative analysis was performed via image processing to identify the relationship between the tensile strength and the thickness of the Cr x B y phase layer at the interface of brazed 304 stainless steel with Ni-based filler metal (MBF20). The experimental design was based on the Taguchi method to determine the relative contributions of the processing conditions, including the brazing temperature, heating rate, holding time, and filler metal thickness. The Cr x B y phase at the brazement interface was extracted by an image-processing method from backscattered electron imaging; the numerically defined thicknesses of the Cr x B y phase layers developed under varied processing conditions were calculated. The tensile strengths at temperatures of 25 °C and 650 °C were measured for specimens brazed under identical experimental conditions based on the Taguchi method and the post-tensile testing fracture surfaces were analyzed. Regarding the relationship between the thickness of the Cr x B y phase layer, as determined through the image processing of the microstructure, and the tensile strength at 25 °C, thicker Cr x B y layers deteriorated the tensile strength of the brazement interfaces. Although a slight discrepancy occurred in the brazement tensile strengths between the testing temperatures of 25 °C and 650 °C, the elevated temperature during tensile testing affected the brazed interface microstructure; with this consideration, the overall results for both tensile strength tests corresponded to the quantitatively analyzed Cr x B y phase layer thicknesses. From the relationship between Cr x B y layer thickness and tensile strength, the heating rate is the most effective processing condition to achieve high bonding strength, because changes in heating rate compared to those of other processing conditions have the greatest effect in changing the Cr x B y phase layer thicknesses and tensile strength. Therefore, the results confirmed that the image-processing method enabled accurate quantitative analysis of the microstructure, permitting prediction of the mechanical strength of the joint.
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Although a slight discrepancy occurred in the brazement tensile strengths between the testing temperatures of 25 °C and 650 °C, the elevated temperature during tensile testing affected the brazed interface microstructure; with this consideration, the overall results for both tensile strength tests corresponded to the quantitatively analyzed Cr x B y phase layer thicknesses. From the relationship between Cr x B y layer thickness and tensile strength, the heating rate is the most effective processing condition to achieve high bonding strength, because changes in heating rate compared to those of other processing conditions have the greatest effect in changing the Cr x B y phase layer thicknesses and tensile strength. 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A, Physical metallurgy and materials science</title><addtitle>Metall Mater Trans A</addtitle><description>Quantitative analysis was performed via image processing to identify the relationship between the tensile strength and the thickness of the Cr x B y phase layer at the interface of brazed 304 stainless steel with Ni-based filler metal (MBF20). The experimental design was based on the Taguchi method to determine the relative contributions of the processing conditions, including the brazing temperature, heating rate, holding time, and filler metal thickness. The Cr x B y phase at the brazement interface was extracted by an image-processing method from backscattered electron imaging; the numerically defined thicknesses of the Cr x B y phase layers developed under varied processing conditions were calculated. The tensile strengths at temperatures of 25 °C and 650 °C were measured for specimens brazed under identical experimental conditions based on the Taguchi method and the post-tensile testing fracture surfaces were analyzed. Regarding the relationship between the thickness of the Cr x B y phase layer, as determined through the image processing of the microstructure, and the tensile strength at 25 °C, thicker Cr x B y layers deteriorated the tensile strength of the brazement interfaces. Although a slight discrepancy occurred in the brazement tensile strengths between the testing temperatures of 25 °C and 650 °C, the elevated temperature during tensile testing affected the brazed interface microstructure; with this consideration, the overall results for both tensile strength tests corresponded to the quantitatively analyzed Cr x B y phase layer thicknesses. From the relationship between Cr x B y layer thickness and tensile strength, the heating rate is the most effective processing condition to achieve high bonding strength, because changes in heating rate compared to those of other processing conditions have the greatest effect in changing the Cr x B y phase layer thicknesses and tensile strength. Therefore, the results confirmed that the image-processing method enabled accurate quantitative analysis of the microstructure, permitting prediction of the mechanical strength of the joint.</description><subject>Austenitic stainless steels</subject><subject>Backscattering</subject><subject>Bonding strength</subject><subject>Brazing</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Electron imaging</subject><subject>Filler metals</subject><subject>Fracture surfaces</subject><subject>Heating rate</subject><subject>High temperature</subject><subject>Image processing</subject><subject>Materials Science</subject><subject>Metallic Materials</subject><subject>Microstructure</subject><subject>Nanotechnology</subject><subject>Nickel</subject><subject>Quantitative analysis</subject><subject>Structural Materials</subject><subject>Surfaces and Interfaces</subject><subject>Taguchi methods</subject><subject>Tensile strength</subject><subject>Test procedures</subject><subject>Thickness</subject><subject>Thin Films</subject><issn>1073-5623</issn><issn>1543-1940</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><sourceid>8G5</sourceid><sourceid>BENPR</sourceid><sourceid>GUQSH</sourceid><sourceid>M2O</sourceid><recordid>eNp1kE1Lw0AQhoMoWKs_wNuC5-hMvnOsxY-CYNXcl2kym25JN3U3Vfrv3RLBk6eZw_u8zDxBcI1wiwD5nUPMMgwBizAp0C8nwQTTJA6xTODU75DHYZpF8Xlw4dwGALCMs0nQVdTu67UWM0PdwWkneiXeuaNB90bc8_DNbETFxumOxcdg2bTDWpBpxMIMbBXVmjqxXJNjJ972ZAatNDfiS5NYbKllsbR9zc5p014GZ4o6x1e_cxpUjw_V_Dl8eX1azGcvYR1jNoT-ykxxnkCdMifYKE7TJGrUqiRFq6JocgQqI5XVQMDlKs2xiWqlUlJYFkU8DW7G2p3tP_fsBrnp99b_52QEno0gKyKfwjFV2945y0rurN6SPUgEeXQqR6fSO5VHpxI8E42M81nTsv1r_h_6Aa1kess</recordid><startdate>20181001</startdate><enddate>20181001</enddate><creator>Park, Dong Yong</creator><creator>Lee, Sun Kyu</creator><creator>Oh, Yong Jun</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>4T-</scope><scope>4U-</scope><scope>7SR</scope><scope>7XB</scope><scope>88I</scope><scope>8AF</scope><scope>8AO</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FK</scope><scope>8G5</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>GNUQQ</scope><scope>GUQSH</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L6V</scope><scope>M2O</scope><scope>M2P</scope><scope>M7S</scope><scope>MBDVC</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><scope>Q9U</scope><scope>S0X</scope></search><sort><creationdate>20181001</creationdate><title>Taguchi Analysis of Relation Between Tensile Strength and Interfacial Phases Quantified via Image Processing</title><author>Park, Dong Yong ; Lee, Sun Kyu ; Oh, Yong Jun</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-6236fe740c5ee41dfe5542dfb9afab88d710a92f6c0a0e9b571d2cff5af19883</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Austenitic stainless steels</topic><topic>Backscattering</topic><topic>Bonding strength</topic><topic>Brazing</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Electron imaging</topic><topic>Filler metals</topic><topic>Fracture surfaces</topic><topic>Heating rate</topic><topic>High temperature</topic><topic>Image processing</topic><topic>Materials Science</topic><topic>Metallic Materials</topic><topic>Microstructure</topic><topic>Nanotechnology</topic><topic>Nickel</topic><topic>Quantitative analysis</topic><topic>Structural Materials</topic><topic>Surfaces and Interfaces</topic><topic>Taguchi methods</topic><topic>Tensile strength</topic><topic>Test procedures</topic><topic>Thickness</topic><topic>Thin Films</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Park, Dong Yong</creatorcontrib><creatorcontrib>Lee, Sun Kyu</creatorcontrib><creatorcontrib>Oh, Yong Jun</creatorcontrib><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Docstoc</collection><collection>University Readers</collection><collection>Engineered Materials Abstracts</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Science Database (Alumni Edition)</collection><collection>STEM Database</collection><collection>ProQuest Pharma Collection</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Research Library (Alumni Edition)</collection><collection>Materials Science &amp; 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A, Physical metallurgy and materials science</jtitle><stitle>Metall Mater Trans A</stitle><date>2018-10-01</date><risdate>2018</risdate><volume>49</volume><issue>10</issue><spage>4684</spage><epage>4699</epage><pages>4684-4699</pages><issn>1073-5623</issn><eissn>1543-1940</eissn><abstract>Quantitative analysis was performed via image processing to identify the relationship between the tensile strength and the thickness of the Cr x B y phase layer at the interface of brazed 304 stainless steel with Ni-based filler metal (MBF20). The experimental design was based on the Taguchi method to determine the relative contributions of the processing conditions, including the brazing temperature, heating rate, holding time, and filler metal thickness. The Cr x B y phase at the brazement interface was extracted by an image-processing method from backscattered electron imaging; the numerically defined thicknesses of the Cr x B y phase layers developed under varied processing conditions were calculated. The tensile strengths at temperatures of 25 °C and 650 °C were measured for specimens brazed under identical experimental conditions based on the Taguchi method and the post-tensile testing fracture surfaces were analyzed. Regarding the relationship between the thickness of the Cr x B y phase layer, as determined through the image processing of the microstructure, and the tensile strength at 25 °C, thicker Cr x B y layers deteriorated the tensile strength of the brazement interfaces. Although a slight discrepancy occurred in the brazement tensile strengths between the testing temperatures of 25 °C and 650 °C, the elevated temperature during tensile testing affected the brazed interface microstructure; with this consideration, the overall results for both tensile strength tests corresponded to the quantitatively analyzed Cr x B y phase layer thicknesses. From the relationship between Cr x B y layer thickness and tensile strength, the heating rate is the most effective processing condition to achieve high bonding strength, because changes in heating rate compared to those of other processing conditions have the greatest effect in changing the Cr x B y phase layer thicknesses and tensile strength. Therefore, the results confirmed that the image-processing method enabled accurate quantitative analysis of the microstructure, permitting prediction of the mechanical strength of the joint.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s11661-018-4811-0</doi><tpages>16</tpages></addata></record>
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subjects Austenitic stainless steels
Backscattering
Bonding strength
Brazing
Characterization and Evaluation of Materials
Chemistry and Materials Science
Electron imaging
Filler metals
Fracture surfaces
Heating rate
High temperature
Image processing
Materials Science
Metallic Materials
Microstructure
Nanotechnology
Nickel
Quantitative analysis
Structural Materials
Surfaces and Interfaces
Taguchi methods
Tensile strength
Test procedures
Thickness
Thin Films
title Taguchi Analysis of Relation Between Tensile Strength and Interfacial Phases Quantified via Image Processing
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