Rapid determination of volatile composition from Polygala furcata Royle by MAE–HS-SPME followed by GC–MS
Based on microwave-assisted extraction (MAE) and headspace solid-phase microextraction (HS-SPME) followed by gas chromatography mass spectrometry (GC–MS) was developed for the fast determination of volatile chemical compositions of Polygala furcata Royle, the experimental parameters of the MAE–HS-SP...
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| Veröffentlicht in: | European food research & technology 2010-03, Vol.230 (5), p.779-784 |
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| creator | Yang, Zaibo Mao, Haili Long, Chengmei Sun, Chengbin Guo, Zhiyou |
| description | Based on microwave-assisted extraction (MAE) and headspace solid-phase microextraction (HS-SPME) followed by gas chromatography mass spectrometry (GC–MS) was developed for the fast determination of volatile chemical compositions of
Polygala furcata
Royle, the experimental parameters of the MAE–HS-SPME were optimized by orthogonal experimental design. The results indicated that the optimum condition of the determination of the volatile compounds in
P. furcata
Royle. was achieved with the experimental parameters including microwave power of 400 W and irradiation time of 4 min, sample size 2.0 g. Under the optimal conditions, for the first time, 52 volatile compounds were separated and identified from the fresh plants of
P. furcata
Royle. The highest content component of the 52 compounds was 2-hydroxybenzoic acid methyl ester (21.65%). The relative standard deviation values |
| doi_str_mv | 10.1007/s00217-010-1214-x |
| format | Article |
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Polygala furcata
Royle, the experimental parameters of the MAE–HS-SPME were optimized by orthogonal experimental design. The results indicated that the optimum condition of the determination of the volatile compounds in
P. furcata
Royle. was achieved with the experimental parameters including microwave power of 400 W and irradiation time of 4 min, sample size 2.0 g. Under the optimal conditions, for the first time, 52 volatile compounds were separated and identified from the fresh plants of
P. furcata
Royle. The highest content component of the 52 compounds was 2-hydroxybenzoic acid methyl ester (21.65%). The relative standard deviation values <7% showed that the method of MAE–HS-SPME followed by GC–MS has good precision. The experimental results demonstrated that it is a simple, time-saving and solvent-free method, and it is a potential analytic tool for the determination of the volatile compounds of the vegetations materials and other materials.</description><identifier>ISSN: 1438-2377</identifier><identifier>EISSN: 1438-2385</identifier><identifier>DOI: 10.1007/s00217-010-1214-x</identifier><language>eng</language><publisher>Berlin/Heidelberg: Springer-Verlag</publisher><subject>Agricultural biotechnology ; Agriculture ; Analytical Chemistry ; Biochemistry ; Biological and medical sciences ; Biotechnology ; Chemistry ; Chemistry and Materials Science ; Chromatography ; Experimental design ; Food industries ; Food Science ; Forestry ; Fundamental and applied biological sciences. Psychology ; Gas chromatography ; Herbal medicine ; Irradiation ; Life sciences ; Mass spectrometry ; Microwaves ; Oils & fats ; Original Paper ; Standard deviation ; Studies ; Vegetation</subject><ispartof>European food research & technology, 2010-03, Vol.230 (5), p.779-784</ispartof><rights>The Author(s) 2010</rights><rights>2015 INIST-CNRS</rights><rights>Springer-Verlag 2010</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c388t-aa1cd76c2baad5d129878d37a29bf4f4055e949ba16fe6f10efbc1eb556fe8f33</citedby><cites>FETCH-LOGICAL-c388t-aa1cd76c2baad5d129878d37a29bf4f4055e949ba16fe6f10efbc1eb556fe8f33</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00217-010-1214-x$$EPDF$$P50$$Gspringer$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00217-010-1214-x$$EHTML$$P50$$Gspringer$$Hfree_for_read</linktohtml><link.rule.ids>314,777,781,27905,27906,41469,42538,51300</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=22428336$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Yang, Zaibo</creatorcontrib><creatorcontrib>Mao, Haili</creatorcontrib><creatorcontrib>Long, Chengmei</creatorcontrib><creatorcontrib>Sun, Chengbin</creatorcontrib><creatorcontrib>Guo, Zhiyou</creatorcontrib><title>Rapid determination of volatile composition from Polygala furcata Royle by MAE–HS-SPME followed by GC–MS</title><title>European food research & technology</title><addtitle>Eur Food Res Technol</addtitle><description>Based on microwave-assisted extraction (MAE) and headspace solid-phase microextraction (HS-SPME) followed by gas chromatography mass spectrometry (GC–MS) was developed for the fast determination of volatile chemical compositions of
Polygala furcata
Royle, the experimental parameters of the MAE–HS-SPME were optimized by orthogonal experimental design. The results indicated that the optimum condition of the determination of the volatile compounds in
P. furcata
Royle. was achieved with the experimental parameters including microwave power of 400 W and irradiation time of 4 min, sample size 2.0 g. Under the optimal conditions, for the first time, 52 volatile compounds were separated and identified from the fresh plants of
P. furcata
Royle. The highest content component of the 52 compounds was 2-hydroxybenzoic acid methyl ester (21.65%). The relative standard deviation values <7% showed that the method of MAE–HS-SPME followed by GC–MS has good precision. The experimental results demonstrated that it is a simple, time-saving and solvent-free method, and it is a potential analytic tool for the determination of the volatile compounds of the vegetations materials and other materials.</description><subject>Agricultural biotechnology</subject><subject>Agriculture</subject><subject>Analytical Chemistry</subject><subject>Biochemistry</subject><subject>Biological and medical sciences</subject><subject>Biotechnology</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chromatography</subject><subject>Experimental design</subject><subject>Food industries</subject><subject>Food Science</subject><subject>Forestry</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>Gas chromatography</subject><subject>Herbal medicine</subject><subject>Irradiation</subject><subject>Life sciences</subject><subject>Mass spectrometry</subject><subject>Microwaves</subject><subject>Oils & fats</subject><subject>Original Paper</subject><subject>Standard deviation</subject><subject>Studies</subject><subject>Vegetation</subject><issn>1438-2377</issn><issn>1438-2385</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><sourceid>C6C</sourceid><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNp1kE1OwzAQhSMEEqVwAHYWEsuA7fw5y6oqLVIrUAvraOLYVSonDnYKzY47cENOgkuqsmI1M37fPI-e510TfEcwTu4txpQkPibYJ5SE_u7EG5AwYD4NWHR67JPk3LuwdoNxlMYkHHhqCU1ZoEK0wlRlDW2pa6QletfK9UogrqtG2_L3XRpdoWetujUoQHJrOLSAlrpzXN6hxWjy_fk1W_mr58UESa2U_hDFXpmOnbBYXXpnEpQVV4c69F4fJi_jmT9_mj6OR3OfB4y1PgDhRRJzmgMUUUFoyhJWBAnQNJehDHEUiTRMcyCxFLEkWMicE5FHkZuZDIKhd9P7Nka_bYVts43emtp9mVEcsThMaeIg0kPcaGuNkFljygpMlxGc7TPN-kwzvJ9dptnO7dwejMFyUNJAzUt7XKQ0pCwIYsfRnrNOqtfC_B3wv_kPJeaJfg</recordid><startdate>20100301</startdate><enddate>20100301</enddate><creator>Yang, Zaibo</creator><creator>Mao, Haili</creator><creator>Long, Chengmei</creator><creator>Sun, Chengbin</creator><creator>Guo, Zhiyou</creator><general>Springer-Verlag</general><general>Springer</general><general>Springer Nature B.V</general><scope>C6C</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7QO</scope><scope>7QR</scope><scope>7RQ</scope><scope>7T7</scope><scope>7WY</scope><scope>7WZ</scope><scope>7X2</scope><scope>7XB</scope><scope>87Z</scope><scope>88I</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FH</scope><scope>8FK</scope><scope>8FL</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AEUYN</scope><scope>AFKRA</scope><scope>ATCPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BEZIV</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>C1K</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>FR3</scope><scope>FRNLG</scope><scope>F~G</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>K60</scope><scope>K6~</scope><scope>L.-</scope><scope>L6V</scope><scope>M0C</scope><scope>M0K</scope><scope>M2P</scope><scope>M7S</scope><scope>P64</scope><scope>PQBIZ</scope><scope>PQBZA</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope><scope>Q9U</scope></search><sort><creationdate>20100301</creationdate><title>Rapid determination of volatile composition from Polygala furcata Royle by MAE–HS-SPME followed by GC–MS</title><author>Yang, Zaibo ; Mao, Haili ; Long, Chengmei ; Sun, Chengbin ; Guo, Zhiyou</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c388t-aa1cd76c2baad5d129878d37a29bf4f4055e949ba16fe6f10efbc1eb556fe8f33</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Agricultural biotechnology</topic><topic>Agriculture</topic><topic>Analytical Chemistry</topic><topic>Biochemistry</topic><topic>Biological and medical sciences</topic><topic>Biotechnology</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chromatography</topic><topic>Experimental design</topic><topic>Food industries</topic><topic>Food Science</topic><topic>Forestry</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>Gas chromatography</topic><topic>Herbal medicine</topic><topic>Irradiation</topic><topic>Life sciences</topic><topic>Mass spectrometry</topic><topic>Microwaves</topic><topic>Oils & fats</topic><topic>Original Paper</topic><topic>Standard deviation</topic><topic>Studies</topic><topic>Vegetation</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yang, Zaibo</creatorcontrib><creatorcontrib>Mao, Haili</creatorcontrib><creatorcontrib>Long, Chengmei</creatorcontrib><creatorcontrib>Sun, Chengbin</creatorcontrib><creatorcontrib>Guo, Zhiyou</creatorcontrib><collection>Springer Nature OA Free Journals</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Biotechnology Research Abstracts</collection><collection>Chemoreception Abstracts</collection><collection>Career & Technical Education Database</collection><collection>Industrial and Applied Microbiology Abstracts (Microbiology A)</collection><collection>ABI/INFORM Collection</collection><collection>ABI/INFORM Global (PDF only)</collection><collection>Agricultural Science Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>ABI/INFORM Global (Alumni Edition)</collection><collection>Science Database (Alumni Edition)</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Natural Science Collection</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>ABI/INFORM Collection (Alumni Edition)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest One Sustainability</collection><collection>ProQuest Central UK/Ireland</collection><collection>Agricultural & Environmental Science Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Business Premium Collection</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>Engineering Research Database</collection><collection>Business Premium Collection (Alumni)</collection><collection>ABI/INFORM Global (Corporate)</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Business Collection (Alumni Edition)</collection><collection>ProQuest Business Collection</collection><collection>ABI/INFORM Professional Advanced</collection><collection>ProQuest Engineering Collection</collection><collection>ABI/INFORM Global</collection><collection>Agricultural Science Database</collection><collection>Science Database</collection><collection>Engineering Database</collection><collection>Biotechnology and BioEngineering Abstracts</collection><collection>One Business (ProQuest)</collection><collection>ProQuest One Business (Alumni)</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineering Collection</collection><collection>ProQuest Central Basic</collection><jtitle>European food research & technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yang, Zaibo</au><au>Mao, Haili</au><au>Long, Chengmei</au><au>Sun, Chengbin</au><au>Guo, Zhiyou</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Rapid determination of volatile composition from Polygala furcata Royle by MAE–HS-SPME followed by GC–MS</atitle><jtitle>European food research & technology</jtitle><stitle>Eur Food Res Technol</stitle><date>2010-03-01</date><risdate>2010</risdate><volume>230</volume><issue>5</issue><spage>779</spage><epage>784</epage><pages>779-784</pages><issn>1438-2377</issn><eissn>1438-2385</eissn><abstract>Based on microwave-assisted extraction (MAE) and headspace solid-phase microextraction (HS-SPME) followed by gas chromatography mass spectrometry (GC–MS) was developed for the fast determination of volatile chemical compositions of
Polygala furcata
Royle, the experimental parameters of the MAE–HS-SPME were optimized by orthogonal experimental design. The results indicated that the optimum condition of the determination of the volatile compounds in
P. furcata
Royle. was achieved with the experimental parameters including microwave power of 400 W and irradiation time of 4 min, sample size 2.0 g. Under the optimal conditions, for the first time, 52 volatile compounds were separated and identified from the fresh plants of
P. furcata
Royle. The highest content component of the 52 compounds was 2-hydroxybenzoic acid methyl ester (21.65%). The relative standard deviation values <7% showed that the method of MAE–HS-SPME followed by GC–MS has good precision. The experimental results demonstrated that it is a simple, time-saving and solvent-free method, and it is a potential analytic tool for the determination of the volatile compounds of the vegetations materials and other materials.</abstract><cop>Berlin/Heidelberg</cop><pub>Springer-Verlag</pub><doi>10.1007/s00217-010-1214-x</doi><tpages>6</tpages><oa>free_for_read</oa></addata></record> |
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| ispartof | European food research & technology, 2010-03, Vol.230 (5), p.779-784 |
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| subjects | Agricultural biotechnology Agriculture Analytical Chemistry Biochemistry Biological and medical sciences Biotechnology Chemistry Chemistry and Materials Science Chromatography Experimental design Food industries Food Science Forestry Fundamental and applied biological sciences. Psychology Gas chromatography Herbal medicine Irradiation Life sciences Mass spectrometry Microwaves Oils & fats Original Paper Standard deviation Studies Vegetation |
| title | Rapid determination of volatile composition from Polygala furcata Royle by MAE–HS-SPME followed by GC–MS |
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