Preparation and electrochemical capacitive performance of phenolated calcium lignosulfonate-based phenol formaldehyde resin porous carbon
Lignin-based phenol formaldehyde resin was synthesized using phenolated calcium lignosulfonate, and porous carbon with good wettability was prepared after carbonization and potassium hydroxide (KOH) activation. The results indicated that when the KOH to the carbonized sample mass ratio was 6:1, the...
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Veröffentlicht in: | Journal of materials research 2018-05, Vol.33 (9), p.1211-1218 |
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description | Lignin-based phenol formaldehyde resin was synthesized using phenolated calcium lignosulfonate, and porous carbon with good wettability was prepared after carbonization and potassium hydroxide (KOH) activation. The results indicated that when the KOH to the carbonized sample mass ratio was 6:1, the prepared carbon had a rich porous structure and higher surface area, with a specific surface area of 1320.13 m2/g. Furthermore, the porous carbon exhibited a maximum specific capacitance of 204.88 F/g at a current density of 0.5 A/g in the potential range −1.0 to 0 V in a 6 M KOH solution and a low equivalent series resistance of 0.64 Ω. The phenolated calcium lignosulfonate-based phenol formaldehyde resin porous carbon demonstrated a favorable electric double-layer performance. |
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The results indicated that when the KOH to the carbonized sample mass ratio was 6:1, the prepared carbon had a rich porous structure and higher surface area, with a specific surface area of 1320.13 m2/g. Furthermore, the porous carbon exhibited a maximum specific capacitance of 204.88 F/g at a current density of 0.5 A/g in the potential range −1.0 to 0 V in a 6 M KOH solution and a low equivalent series resistance of 0.64 Ω. The phenolated calcium lignosulfonate-based phenol formaldehyde resin porous carbon demonstrated a favorable electric double-layer performance.</description><identifier>ISSN: 0884-2914</identifier><identifier>EISSN: 2044-5326</identifier><identifier>DOI: 10.1557/jmr.2018.38</identifier><language>eng</language><publisher>New York, USA: Cambridge University Press</publisher><subject>Activated carbon ; Applied and Technical Physics ; Biomaterials ; Calcium ; Carbon ; Carbonization ; Electrodes ; Electrolytes ; Energy ; Energy storage ; Fourier transforms ; Inorganic Chemistry ; Lignin ; Lignosulfonates ; Materials Engineering ; Materials research ; Materials Science ; Microscopy ; Nanotechnology ; Phenol formaldehyde ; Phenol formaldehyde resins ; Phenols ; Pneumatics ; Pore size ; Potassium hydroxides ; Reagents ; Resins ; Scanning electron microscopy ; Spectrum analysis ; Surface area ; Sustainable development ; Transmission electron microscopy ; Wettability ; Work stations</subject><ispartof>Journal of materials research, 2018-05, Vol.33 (9), p.1211-1218</ispartof><rights>Copyright © Materials Research Society 2018</rights><rights>The Materials Research Society 2018</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c373t-ec6b5e0b96e755af70967583084154c96ee9a3705eff0b70a4fc654ed28f613c3</citedby><cites>FETCH-LOGICAL-c373t-ec6b5e0b96e755af70967583084154c96ee9a3705eff0b70a4fc654ed28f613c3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1557/jmr.2018.38$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://www.cambridge.org/core/product/identifier/S0884291418000389/type/journal_article$$EHTML$$P50$$Gcambridge$$H</linktohtml><link.rule.ids>164,314,776,780,27903,27904,41467,42536,51297,55606</link.rule.ids></links><search><creatorcontrib>Dai, Junxiu</creatorcontrib><creatorcontrib>Ma, Yanli</creatorcontrib><creatorcontrib>Ren, Shixue</creatorcontrib><creatorcontrib>Fang, Guizhen</creatorcontrib><title>Preparation and electrochemical capacitive performance of phenolated calcium lignosulfonate-based phenol formaldehyde resin porous carbon</title><title>Journal of materials research</title><addtitle>Journal of Materials Research</addtitle><addtitle>J. Mater. Res</addtitle><description>Lignin-based phenol formaldehyde resin was synthesized using phenolated calcium lignosulfonate, and porous carbon with good wettability was prepared after carbonization and potassium hydroxide (KOH) activation. The results indicated that when the KOH to the carbonized sample mass ratio was 6:1, the prepared carbon had a rich porous structure and higher surface area, with a specific surface area of 1320.13 m2/g. Furthermore, the porous carbon exhibited a maximum specific capacitance of 204.88 F/g at a current density of 0.5 A/g in the potential range −1.0 to 0 V in a 6 M KOH solution and a low equivalent series resistance of 0.64 Ω. The phenolated calcium lignosulfonate-based phenol formaldehyde resin porous carbon demonstrated a favorable electric double-layer performance.</description><subject>Activated carbon</subject><subject>Applied and Technical Physics</subject><subject>Biomaterials</subject><subject>Calcium</subject><subject>Carbon</subject><subject>Carbonization</subject><subject>Electrodes</subject><subject>Electrolytes</subject><subject>Energy</subject><subject>Energy storage</subject><subject>Fourier transforms</subject><subject>Inorganic Chemistry</subject><subject>Lignin</subject><subject>Lignosulfonates</subject><subject>Materials Engineering</subject><subject>Materials research</subject><subject>Materials Science</subject><subject>Microscopy</subject><subject>Nanotechnology</subject><subject>Phenol formaldehyde</subject><subject>Phenol formaldehyde resins</subject><subject>Phenols</subject><subject>Pneumatics</subject><subject>Pore size</subject><subject>Potassium hydroxides</subject><subject>Reagents</subject><subject>Resins</subject><subject>Scanning electron microscopy</subject><subject>Spectrum analysis</subject><subject>Surface area</subject><subject>Sustainable development</subject><subject>Transmission electron microscopy</subject><subject>Wettability</subject><subject>Work stations</subject><issn>0884-2914</issn><issn>2044-5326</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNp9kE1LxDAQhoMouK6e_AMBj9o1bZKmexTxCwQ96Lmk6WQ3S5vUSSv4E_zXZl3Bi3gamHned-Ah5DRni1xKdbnpcVGwvFrwao_MCiZEJnlR7pMZqyqRFctcHJKjGDeM5ZIpMSOfzwiDRj264Kn2LYUOzIjBrKF3RnfU6EEbN7p3oAOgDdhrb4AGS4c1-NDpEdoEdcZNPe3cyoc4dTb4tM8aHdNxx9HvaNfC-qMFihCdp0PAMMWUxib4Y3JgdRfh5GfOyevtzcv1ffb4dPdwffWYGa74mIEpGwmsWZagpNRWsWWpZMVZJXIpTFrDUnPFJFjLGsW0sKaUAtqismXODZ-Ts13vgOFtgjjWmzChTy_rgvGKi6RKJep8RxkMMSLYekDXa_yoc1ZvXdfJdb11XafMnFzs6JgovwL87fwbz37Kdd-ga1fwP_8FUjCTsQ</recordid><startdate>20180514</startdate><enddate>20180514</enddate><creator>Dai, Junxiu</creator><creator>Ma, Yanli</creator><creator>Ren, Shixue</creator><creator>Fang, Guizhen</creator><general>Cambridge University Press</general><general>Springer International Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>0U~</scope><scope>1-H</scope><scope>3V.</scope><scope>7SR</scope><scope>7WY</scope><scope>7WZ</scope><scope>7XB</scope><scope>87Z</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FK</scope><scope>8FL</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BEZIV</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>FRNLG</scope><scope>F~G</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>K60</scope><scope>K6~</scope><scope>KB.</scope><scope>L.-</scope><scope>L.0</scope><scope>M0C</scope><scope>PDBOC</scope><scope>PQBIZ</scope><scope>PQBZA</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>Q9U</scope><scope>S0W</scope></search><sort><creationdate>20180514</creationdate><title>Preparation and electrochemical capacitive performance of phenolated calcium lignosulfonate-based phenol formaldehyde resin porous carbon</title><author>Dai, Junxiu ; Ma, Yanli ; Ren, Shixue ; Fang, Guizhen</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c373t-ec6b5e0b96e755af70967583084154c96ee9a3705eff0b70a4fc654ed28f613c3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Activated carbon</topic><topic>Applied and Technical Physics</topic><topic>Biomaterials</topic><topic>Calcium</topic><topic>Carbon</topic><topic>Carbonization</topic><topic>Electrodes</topic><topic>Electrolytes</topic><topic>Energy</topic><topic>Energy storage</topic><topic>Fourier transforms</topic><topic>Inorganic Chemistry</topic><topic>Lignin</topic><topic>Lignosulfonates</topic><topic>Materials Engineering</topic><topic>Materials research</topic><topic>Materials Science</topic><topic>Microscopy</topic><topic>Nanotechnology</topic><topic>Phenol formaldehyde</topic><topic>Phenol formaldehyde resins</topic><topic>Phenols</topic><topic>Pneumatics</topic><topic>Pore size</topic><topic>Potassium hydroxides</topic><topic>Reagents</topic><topic>Resins</topic><topic>Scanning electron microscopy</topic><topic>Spectrum analysis</topic><topic>Surface area</topic><topic>Sustainable development</topic><topic>Transmission electron microscopy</topic><topic>Wettability</topic><topic>Work stations</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Dai, Junxiu</creatorcontrib><creatorcontrib>Ma, Yanli</creatorcontrib><creatorcontrib>Ren, Shixue</creatorcontrib><creatorcontrib>Fang, Guizhen</creatorcontrib><collection>CrossRef</collection><collection>Global News & ABI/Inform Professional</collection><collection>Trade PRO</collection><collection>ProQuest Central (Corporate)</collection><collection>Engineered Materials Abstracts</collection><collection>ABI/INFORM Collection</collection><collection>ABI/INFORM Global (PDF only)</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>ABI/INFORM Global (Alumni Edition)</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>ABI/INFORM Collection (Alumni Edition)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Business Premium Collection</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>Business Premium Collection (Alumni)</collection><collection>ABI/INFORM Global (Corporate)</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>ProQuest Business Collection (Alumni Edition)</collection><collection>ProQuest Business Collection</collection><collection>Materials Science Database</collection><collection>ABI/INFORM Professional Advanced</collection><collection>ABI/INFORM Professional Standard</collection><collection>ABI/INFORM Global</collection><collection>Materials Science Collection</collection><collection>ProQuest One Business</collection><collection>ProQuest One Business (Alumni)</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central Basic</collection><collection>DELNET Engineering & Technology Collection</collection><jtitle>Journal of materials research</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Dai, Junxiu</au><au>Ma, Yanli</au><au>Ren, Shixue</au><au>Fang, Guizhen</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation and electrochemical capacitive performance of phenolated calcium lignosulfonate-based phenol formaldehyde resin porous carbon</atitle><jtitle>Journal of materials research</jtitle><stitle>Journal of Materials Research</stitle><addtitle>J. Mater. Res</addtitle><date>2018-05-14</date><risdate>2018</risdate><volume>33</volume><issue>9</issue><spage>1211</spage><epage>1218</epage><pages>1211-1218</pages><issn>0884-2914</issn><eissn>2044-5326</eissn><abstract>Lignin-based phenol formaldehyde resin was synthesized using phenolated calcium lignosulfonate, and porous carbon with good wettability was prepared after carbonization and potassium hydroxide (KOH) activation. The results indicated that when the KOH to the carbonized sample mass ratio was 6:1, the prepared carbon had a rich porous structure and higher surface area, with a specific surface area of 1320.13 m2/g. Furthermore, the porous carbon exhibited a maximum specific capacitance of 204.88 F/g at a current density of 0.5 A/g in the potential range −1.0 to 0 V in a 6 M KOH solution and a low equivalent series resistance of 0.64 Ω. The phenolated calcium lignosulfonate-based phenol formaldehyde resin porous carbon demonstrated a favorable electric double-layer performance.</abstract><cop>New York, USA</cop><pub>Cambridge University Press</pub><doi>10.1557/jmr.2018.38</doi><tpages>8</tpages></addata></record> |
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subjects | Activated carbon Applied and Technical Physics Biomaterials Calcium Carbon Carbonization Electrodes Electrolytes Energy Energy storage Fourier transforms Inorganic Chemistry Lignin Lignosulfonates Materials Engineering Materials research Materials Science Microscopy Nanotechnology Phenol formaldehyde Phenol formaldehyde resins Phenols Pneumatics Pore size Potassium hydroxides Reagents Resins Scanning electron microscopy Spectrum analysis Surface area Sustainable development Transmission electron microscopy Wettability Work stations |
title | Preparation and electrochemical capacitive performance of phenolated calcium lignosulfonate-based phenol formaldehyde resin porous carbon |
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