Application of microsecond pulsed glow discharge to modern commercially available optical emission spectrometers for bulk elemental analysis

Microsecond Pulsed Glow Discharge (μs-PGD) was applied to commercially available spectrometers specified for OES elemental analysis with Grimm type sources, in order to have a look at the benefits which PGD can bring for practical bulk analysis. Intensities of more than 70 spectral lines of differen...

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Veröffentlicht in:	Journal of analytical atomic spectrometry 2018-04, Vol.33 (4), p.663-669
Hauptverfasser:	Voronov, M., Hoffmann, V.
Format:	Artikel
Sprache:	eng
Schlagworte:	Atmospheric pressure Background noise Continuity (mathematics) Discharge Electricity Emission analysis Line spectra Spectrometers
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container_title	Journal of analytical atomic spectrometry
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creator	Voronov, M. Hoffmann, V.
description	Microsecond Pulsed Glow Discharge (μs-PGD) was applied to commercially available spectrometers specified for OES elemental analysis with Grimm type sources, in order to have a look at the benefits which PGD can bring for practical bulk analysis. Intensities of more than 70 spectral lines of different elements together with background and noises were compared between μs-PGD and continuous Glow Discharge (GD) using CCD and PMT detectors. In comparison to continuous GD, the detection limits with PGD were 1.5–14 times lower for different spectral lines. The reasons for such a moderate improvement are discussed.
doi_str_mv	10.1039/C7JA00424A
format	Article
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source	Royal Society Of Chemistry Journals; Alma/SFX Local Collection
subjects	Atmospheric pressure Background noise Continuity (mathematics) Discharge Electricity Emission analysis Line spectra Spectrometers
title	Application of microsecond pulsed glow discharge to modern commercially available optical emission spectrometers for bulk elemental analysis
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