Hydrophilic Interaction Chromatography on Silica: Group Analysis of Grape Anthocyanins
A group control procedure is developed, in which the anthocyanin complex of a grape extract is divided into six groups without differentiation by aglycons: 3-glucosides (Zone III); 3-glucosides acylated with p -coumaric acid (Zone I); 3-glucosides acylated with acetic acid (Zone II); 3,5-diglucoside...
Gespeichert in:
| Veröffentlicht in: | Journal of analytical chemistry (New York, N.Y.) N.Y.), 2018-02, Vol.73 (2), p.190-194 |
|---|---|
| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 194 |
|---|---|
| container_issue | 2 |
| container_start_page | 190 |
| container_title | Journal of analytical chemistry (New York, N.Y.) |
| container_volume | 73 |
| creator | Deineka, V. I. Makarevich, S. L. Deineka, L. A. |
| description | A group control procedure is developed, in which the anthocyanin complex of a grape extract is divided into six groups without differentiation by aglycons: 3-glucosides (Zone III); 3-glucosides acylated with
p
-coumaric acid (Zone I); 3-glucosides acylated with acetic acid (Zone II); 3,5-diglucosides (Zone IV); 3,5-diglucosides acylated with
p
-coumaric acid (Zone IV); and 3,5-diglucosides acylated with acetic acid (Zone V). The anthocyanins were separated by hydrophilic interaction chromatography in a column packed with a silica using the mobile phases of acetonitrile–water (20–8 vol %) containing 0.5 vol % of orthophosphoric acid. Due to the low viscosity of the mobile phase and the complete separation of anthocyanin groups, the procedure suitable for determining the inheritance of genetic traits in the selection of grapes is transferred to a format of microcolumn chromatography using MiLiChrome chromatographs. |
| doi_str_mv | 10.1134/S106193481802003X |
| format | Article |
| fullrecord | <record><control><sourceid>gale_proqu</sourceid><recordid>TN_cdi_proquest_journals_2013147969</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><galeid>A541288823</galeid><sourcerecordid>A541288823</sourcerecordid><originalsourceid>FETCH-LOGICAL-c455t-a825f3781858a813d415bcaaade278f2e092c3bef8fdf5c23c62b693961f676d3</originalsourceid><addsrcrecordid>eNp1kU1LAzEQhhdRsH78AG8LnjxszSS726y3UvwoCIJV8RbSbLJN2SZrkoL7702pKMXKHDK887zDZCZJLgANAUh-PQNUQkVyChRhhMj7QTKAEtGMQFUdxjyWs039ODnxfokQqiiUg-Ttoa-d7Ra61SKdmiAdF0Fbk04Wzq54sI3j3aJPozLbMPwmvXd23aVjw9vea59aFRXeyaiEhRU9N9r4s-RI8dbL8-_3NHm9u32ZPGSPT_fTyfgxE3lRhIxTXCgyikMXlFMgdQ7FXHDOa4lHVGGJKizIXCqqalUITESJ52VFqhJUOSprcppcbvt2zn6spQ9sadcujuYZRkAgH1UR_6Ea3kqmjbIhfnOlvWDjIgdMKcUkUtkeqpEm7qS1Riod5R1-uIePUcuVFnsNVzuGyAT5GRq-9p5NZ8-7LGxZ4az3TirWOb3irmeA2Obi7M_FowdvPT6yppHudxn_m74ATMeqlg</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2013147969</pqid></control><display><type>article</type><title>Hydrophilic Interaction Chromatography on Silica: Group Analysis of Grape Anthocyanins</title><source>SpringerNature Journals</source><creator>Deineka, V. I. ; Makarevich, S. L. ; Deineka, L. A.</creator><creatorcontrib>Deineka, V. I. ; Makarevich, S. L. ; Deineka, L. A.</creatorcontrib><description>A group control procedure is developed, in which the anthocyanin complex of a grape extract is divided into six groups without differentiation by aglycons: 3-glucosides (Zone III); 3-glucosides acylated with
p
-coumaric acid (Zone I); 3-glucosides acylated with acetic acid (Zone II); 3,5-diglucosides (Zone IV); 3,5-diglucosides acylated with
p
-coumaric acid (Zone IV); and 3,5-diglucosides acylated with acetic acid (Zone V). The anthocyanins were separated by hydrophilic interaction chromatography in a column packed with a silica using the mobile phases of acetonitrile–water (20–8 vol %) containing 0.5 vol % of orthophosphoric acid. Due to the low viscosity of the mobile phase and the complete separation of anthocyanin groups, the procedure suitable for determining the inheritance of genetic traits in the selection of grapes is transferred to a format of microcolumn chromatography using MiLiChrome chromatographs.</description><identifier>ISSN: 1061-9348</identifier><identifier>EISSN: 1608-3199</identifier><identifier>DOI: 10.1134/S106193481802003X</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Acetic acid ; Acetonitrile ; Acids ; Analytical Chemistry ; Anthocyanins ; Chemical properties ; Chemistry ; Chemistry and Materials Science ; Chromatography ; Genetic aspects ; Glucosides ; Grapes ; Methods ; Silicon dioxide</subject><ispartof>Journal of analytical chemistry (New York, N.Y.), 2018-02, Vol.73 (2), p.190-194</ispartof><rights>Pleiades Publishing, Ltd. 2018</rights><rights>COPYRIGHT 2018 Springer</rights><rights>Copyright Springer Science & Business Media 2018</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c455t-a825f3781858a813d415bcaaade278f2e092c3bef8fdf5c23c62b693961f676d3</citedby><cites>FETCH-LOGICAL-c455t-a825f3781858a813d415bcaaade278f2e092c3bef8fdf5c23c62b693961f676d3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S106193481802003X$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S106193481802003X$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Deineka, V. I.</creatorcontrib><creatorcontrib>Makarevich, S. L.</creatorcontrib><creatorcontrib>Deineka, L. A.</creatorcontrib><title>Hydrophilic Interaction Chromatography on Silica: Group Analysis of Grape Anthocyanins</title><title>Journal of analytical chemistry (New York, N.Y.)</title><addtitle>J Anal Chem</addtitle><description>A group control procedure is developed, in which the anthocyanin complex of a grape extract is divided into six groups without differentiation by aglycons: 3-glucosides (Zone III); 3-glucosides acylated with
p
-coumaric acid (Zone I); 3-glucosides acylated with acetic acid (Zone II); 3,5-diglucosides (Zone IV); 3,5-diglucosides acylated with
p
-coumaric acid (Zone IV); and 3,5-diglucosides acylated with acetic acid (Zone V). The anthocyanins were separated by hydrophilic interaction chromatography in a column packed with a silica using the mobile phases of acetonitrile–water (20–8 vol %) containing 0.5 vol % of orthophosphoric acid. Due to the low viscosity of the mobile phase and the complete separation of anthocyanin groups, the procedure suitable for determining the inheritance of genetic traits in the selection of grapes is transferred to a format of microcolumn chromatography using MiLiChrome chromatographs.</description><subject>Acetic acid</subject><subject>Acetonitrile</subject><subject>Acids</subject><subject>Analytical Chemistry</subject><subject>Anthocyanins</subject><subject>Chemical properties</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chromatography</subject><subject>Genetic aspects</subject><subject>Glucosides</subject><subject>Grapes</subject><subject>Methods</subject><subject>Silicon dioxide</subject><issn>1061-9348</issn><issn>1608-3199</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNp1kU1LAzEQhhdRsH78AG8LnjxszSS726y3UvwoCIJV8RbSbLJN2SZrkoL7702pKMXKHDK887zDZCZJLgANAUh-PQNUQkVyChRhhMj7QTKAEtGMQFUdxjyWs039ODnxfokQqiiUg-Ttoa-d7Ra61SKdmiAdF0Fbk04Wzq54sI3j3aJPozLbMPwmvXd23aVjw9vea59aFRXeyaiEhRU9N9r4s-RI8dbL8-_3NHm9u32ZPGSPT_fTyfgxE3lRhIxTXCgyikMXlFMgdQ7FXHDOa4lHVGGJKizIXCqqalUITESJ52VFqhJUOSprcppcbvt2zn6spQ9sadcujuYZRkAgH1UR_6Ea3kqmjbIhfnOlvWDjIgdMKcUkUtkeqpEm7qS1Riod5R1-uIePUcuVFnsNVzuGyAT5GRq-9p5NZ8-7LGxZ4az3TirWOb3irmeA2Obi7M_FowdvPT6yppHudxn_m74ATMeqlg</recordid><startdate>20180201</startdate><enddate>20180201</enddate><creator>Deineka, V. I.</creator><creator>Makarevich, S. L.</creator><creator>Deineka, L. A.</creator><general>Pleiades Publishing</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope></search><sort><creationdate>20180201</creationdate><title>Hydrophilic Interaction Chromatography on Silica: Group Analysis of Grape Anthocyanins</title><author>Deineka, V. I. ; Makarevich, S. L. ; Deineka, L. A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c455t-a825f3781858a813d415bcaaade278f2e092c3bef8fdf5c23c62b693961f676d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Acetic acid</topic><topic>Acetonitrile</topic><topic>Acids</topic><topic>Analytical Chemistry</topic><topic>Anthocyanins</topic><topic>Chemical properties</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chromatography</topic><topic>Genetic aspects</topic><topic>Glucosides</topic><topic>Grapes</topic><topic>Methods</topic><topic>Silicon dioxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Deineka, V. I.</creatorcontrib><creatorcontrib>Makarevich, S. L.</creatorcontrib><creatorcontrib>Deineka, L. A.</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><jtitle>Journal of analytical chemistry (New York, N.Y.)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Deineka, V. I.</au><au>Makarevich, S. L.</au><au>Deineka, L. A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Hydrophilic Interaction Chromatography on Silica: Group Analysis of Grape Anthocyanins</atitle><jtitle>Journal of analytical chemistry (New York, N.Y.)</jtitle><stitle>J Anal Chem</stitle><date>2018-02-01</date><risdate>2018</risdate><volume>73</volume><issue>2</issue><spage>190</spage><epage>194</epage><pages>190-194</pages><issn>1061-9348</issn><eissn>1608-3199</eissn><abstract>A group control procedure is developed, in which the anthocyanin complex of a grape extract is divided into six groups without differentiation by aglycons: 3-glucosides (Zone III); 3-glucosides acylated with
p
-coumaric acid (Zone I); 3-glucosides acylated with acetic acid (Zone II); 3,5-diglucosides (Zone IV); 3,5-diglucosides acylated with
p
-coumaric acid (Zone IV); and 3,5-diglucosides acylated with acetic acid (Zone V). The anthocyanins were separated by hydrophilic interaction chromatography in a column packed with a silica using the mobile phases of acetonitrile–water (20–8 vol %) containing 0.5 vol % of orthophosphoric acid. Due to the low viscosity of the mobile phase and the complete separation of anthocyanin groups, the procedure suitable for determining the inheritance of genetic traits in the selection of grapes is transferred to a format of microcolumn chromatography using MiLiChrome chromatographs.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S106193481802003X</doi><tpages>5</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1061-9348 |
| ispartof | Journal of analytical chemistry (New York, N.Y.), 2018-02, Vol.73 (2), p.190-194 |
| issn | 1061-9348 1608-3199 |
| language | eng |
| recordid | cdi_proquest_journals_2013147969 |
| source | SpringerNature Journals |
| subjects | Acetic acid Acetonitrile Acids Analytical Chemistry Anthocyanins Chemical properties Chemistry Chemistry and Materials Science Chromatography Genetic aspects Glucosides Grapes Methods Silicon dioxide |
| title | Hydrophilic Interaction Chromatography on Silica: Group Analysis of Grape Anthocyanins |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-20T07%3A26%3A46IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-gale_proqu&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Hydrophilic%20Interaction%20Chromatography%20on%20Silica:%20Group%20Analysis%20of%20Grape%20Anthocyanins&rft.jtitle=Journal%20of%20analytical%20chemistry%20(New%20York,%20N.Y.)&rft.au=Deineka,%20V.%20I.&rft.date=2018-02-01&rft.volume=73&rft.issue=2&rft.spage=190&rft.epage=194&rft.pages=190-194&rft.issn=1061-9348&rft.eissn=1608-3199&rft_id=info:doi/10.1134/S106193481802003X&rft_dat=%3Cgale_proqu%3EA541288823%3C/gale_proqu%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2013147969&rft_id=info:pmid/&rft_galeid=A541288823&rfr_iscdi=true |