Binary systems based on aromatic amines with a view of development of novel hardeners for epoxy resins

Three binary systems based on aromatic amines [4,4′-diaminodiphenylmethane (DDM), 4,4′-diaminodiphenyl sulfone (DDS), 4,4′-diaminodiphenyl ether (DDE) and m -phenylenediamine (MPDA)] were investigated by differential scanning calorimetry (DSC). Phase diagrams for different compositions were construc...

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Veröffentlicht in:Journal of thermal analysis and calorimetry 2018-04, Vol.132 (1), p.643-650
Hauptverfasser: Amirova, Lyaysan R., Surnova, Albina V., Alchin, Ruslan M., Gatiatulin, Askar K., Ziganshin, Marat A., Ibragimov, Marsel R., Amirova, Liliya M.
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container_issue 1
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container_title Journal of thermal analysis and calorimetry
container_volume 132
creator Amirova, Lyaysan R.
Surnova, Albina V.
Alchin, Ruslan M.
Gatiatulin, Askar K.
Ziganshin, Marat A.
Ibragimov, Marsel R.
Amirova, Liliya M.
description Three binary systems based on aromatic amines [4,4′-diaminodiphenylmethane (DDM), 4,4′-diaminodiphenyl sulfone (DDS), 4,4′-diaminodiphenyl ether (DDE) and m -phenylenediamine (MPDA)] were investigated by differential scanning calorimetry (DSC). Phase diagrams for different compositions were constructed. The DSC results showed that all binary systems form simple eutectic mixtures. Formation of eutectic physical mixture of MPDA–DDM and MPDA–DDS was confirmed by powder XRD study. In the case of DDE–DDS system, it was found that besides the eutectic mixture a small amount of the charge transfer complex forms with the novel crystal structure.
doi_str_mv 10.1007/s10973-017-6922-z
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Phase diagrams for different compositions were constructed. The DSC results showed that all binary systems form simple eutectic mixtures. Formation of eutectic physical mixture of MPDA–DDM and MPDA–DDS was confirmed by powder XRD study. In the case of DDE–DDS system, it was found that besides the eutectic mixture a small amount of the charge transfer complex forms with the novel crystal structure.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s10973-017-6922-z</doi><tpages>8</tpages><orcidid>https://orcid.org/0000-0001-6306-4309</orcidid></addata></record>
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subjects Amines
Analytical Chemistry
Aromatic amines
Binary system
Binary systems
Charge transfer
Chemistry
Chemistry and Materials Science
Crystal structure
Diamines
Differential scanning calorimetry
Epoxy resins
Eutectics
Hardeners
Inorganic Chemistry
Measurement Science and Instrumentation
Methylene dianiline
Phenylenediamine
Physical Chemistry
Polymer Sciences
title Binary systems based on aromatic amines with a view of development of novel hardeners for epoxy resins
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