Synthesis route of reduced graphene oxide via thermal reduction of chemically exfoliated graphene oxide
Graphene, a two-dimensional material, is now considered as a rewarding contestant for nanodevices due to its morphology and novel properties. The chemical exfoliation and thermal annealing methods are appraised as an inventive route towards the production of graphene at prodigious scale. This method...
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Veröffentlicht in: | Materials chemistry and physics 2018-01, Vol.204, p.1-7 |
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creator | Saleem, Hareema Haneef, Mobeen Abbasi, Hina Y. |
description | Graphene, a two-dimensional material, is now considered as a rewarding contestant for nanodevices due to its morphology and novel properties. The chemical exfoliation and thermal annealing methods are appraised as an inventive route towards the production of graphene at prodigious scale. This method is utilized for the oxidation of graphite flakes having an oxidizing specialist and thermally reduced the graphene oxide into reduced graphene oxide. We have examined the samples through different characterization techniques. X-ray diffraction displayed the peaks of graphene oxide at 11.8° and reduced graphene oxide at 25.5°. Scanning electron microscopy images revealed the single and multilayers morphology. The optical microscopy examined the number of layers of graphene oxide through the various contrasts of light. UV-Vis spectroscopy showed the hills of graphene oxide and reduced graphene oxide at 215 nm and 267 nm. Fourier transform infrared spectroscopy has been utilized to examine the resonating modes.
•Chemical exfoliation of graphite flakes.•Thermal reduction of graphene oxide.•UV-Vis spectroscopy showed the hills of GO and rGO at 215 nm and 267 nm.•X-ray diffraction displayed the peaks of GO at 11.8° and rGO at 25.5°. |
doi_str_mv | 10.1016/j.matchemphys.2017.10.020 |
format | Article |
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•Chemical exfoliation of graphite flakes.•Thermal reduction of graphene oxide.•UV-Vis spectroscopy showed the hills of GO and rGO at 215 nm and 267 nm.•X-ray diffraction displayed the peaks of GO at 11.8° and rGO at 25.5°.</description><subject>Annealing</subject><subject>Carbon</subject><subject>Chemical exfoliation method</subject><subject>Diffraction</subject><subject>Electron microscopy</subject><subject>Exfoliation</subject><subject>Flakes</subject><subject>Fourier transforms</subject><subject>Graphene</subject><subject>Graphene oxide (GO)</subject><subject>Heat conductivity</subject><subject>Multilayers</subject><subject>Nanotechnology devices</subject><subject>Optical microscopy</subject><subject>Oxidation</subject><subject>Oxidizing agent</subject><subject>Reduced graphene oxide (rGO)</subject><subject>Scanning electron microscopy</subject><subject>Studies</subject><subject>Thermal annealing</subject><subject>Thermal reduction</subject><issn>0254-0584</issn><issn>1879-3312</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNqNkEtLxDAQx4MouK5-h4rnrnn0laMsvmDBg3oO2WSyTenLpF22396UehC8eBqY-f1nmB9CtwRvCCbZfbVp5KBKaPpy8huKSR76G0zxGVqRIucxY4SeoxWmaRLjtEgu0ZX3FQ4gIWyFDu9TO5TgrY9cNw4QdSZyoEcFOjo42ZfQht7JaoiOVkYBdY2sF2SwXTvz83mrZF1PEZxMV1s5_Elfowsjaw83P3WNPp8eP7Yv8e7t-XX7sIsVS_gQA8WcakWVyXUqc2BG4T2TIDO6V4lRmhY60wXjFIwxSZEqXpC9MQVLscE5Zmt0t-ztXfc1gh9E1Y2uDScF4ZxnlLOMB4ovlHKd9w6M6J1tpJsEwWL2Kirxy6uYvc6j4DVkt0sWwhtHC054ZaENwqwDNQjd2X9s-QYetoqA</recordid><startdate>20180115</startdate><enddate>20180115</enddate><creator>Saleem, Hareema</creator><creator>Haneef, Mobeen</creator><creator>Abbasi, Hina Y.</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20180115</creationdate><title>Synthesis route of reduced graphene oxide via thermal reduction of chemically exfoliated graphene oxide</title><author>Saleem, Hareema ; Haneef, Mobeen ; Abbasi, Hina Y.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c349t-e2092dc2cf7d5a7e3fc0b3aea62bc4fcd28d6d8392efff485c981bff8350f0703</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Annealing</topic><topic>Carbon</topic><topic>Chemical exfoliation method</topic><topic>Diffraction</topic><topic>Electron microscopy</topic><topic>Exfoliation</topic><topic>Flakes</topic><topic>Fourier transforms</topic><topic>Graphene</topic><topic>Graphene oxide (GO)</topic><topic>Heat conductivity</topic><topic>Multilayers</topic><topic>Nanotechnology devices</topic><topic>Optical microscopy</topic><topic>Oxidation</topic><topic>Oxidizing agent</topic><topic>Reduced graphene oxide (rGO)</topic><topic>Scanning electron microscopy</topic><topic>Studies</topic><topic>Thermal annealing</topic><topic>Thermal reduction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Saleem, Hareema</creatorcontrib><creatorcontrib>Haneef, Mobeen</creatorcontrib><creatorcontrib>Abbasi, Hina Y.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Materials chemistry and physics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Saleem, Hareema</au><au>Haneef, Mobeen</au><au>Abbasi, Hina Y.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis route of reduced graphene oxide via thermal reduction of chemically exfoliated graphene oxide</atitle><jtitle>Materials chemistry and physics</jtitle><date>2018-01-15</date><risdate>2018</risdate><volume>204</volume><spage>1</spage><epage>7</epage><pages>1-7</pages><issn>0254-0584</issn><eissn>1879-3312</eissn><abstract>Graphene, a two-dimensional material, is now considered as a rewarding contestant for nanodevices due to its morphology and novel properties. The chemical exfoliation and thermal annealing methods are appraised as an inventive route towards the production of graphene at prodigious scale. This method is utilized for the oxidation of graphite flakes having an oxidizing specialist and thermally reduced the graphene oxide into reduced graphene oxide. We have examined the samples through different characterization techniques. X-ray diffraction displayed the peaks of graphene oxide at 11.8° and reduced graphene oxide at 25.5°. Scanning electron microscopy images revealed the single and multilayers morphology. The optical microscopy examined the number of layers of graphene oxide through the various contrasts of light. UV-Vis spectroscopy showed the hills of graphene oxide and reduced graphene oxide at 215 nm and 267 nm. Fourier transform infrared spectroscopy has been utilized to examine the resonating modes.
•Chemical exfoliation of graphite flakes.•Thermal reduction of graphene oxide.•UV-Vis spectroscopy showed the hills of GO and rGO at 215 nm and 267 nm.•X-ray diffraction displayed the peaks of GO at 11.8° and rGO at 25.5°.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.matchemphys.2017.10.020</doi><tpages>7</tpages></addata></record> |
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subjects | Annealing Carbon Chemical exfoliation method Diffraction Electron microscopy Exfoliation Flakes Fourier transforms Graphene Graphene oxide (GO) Heat conductivity Multilayers Nanotechnology devices Optical microscopy Oxidation Oxidizing agent Reduced graphene oxide (rGO) Scanning electron microscopy Studies Thermal annealing Thermal reduction |
title | Synthesis route of reduced graphene oxide via thermal reduction of chemically exfoliated graphene oxide |
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