Development of electric resistance sintering process for the fabrication of hard metals: Processing, microstructure and mechanical properties
This work presents the development of the Electrical Resistance Sintering (ERS) process for the fabrication of hard metals. The compositions of the materials produced were WC with 6 and 10 wt% of Co. In addition to the specific characteristics of the technology, the characterization of the produced...
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Veröffentlicht in: | International journal of refractory metals & hard materials 2017-08, Vol.66, p.88-94 |
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container_title | International journal of refractory metals & hard materials |
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creator | Lagos, M.A. Agote, I. Schubert, T. Weissgaerber, T. Gallardo, J.M. Montes, J.M. Prakash, L. Andreouli, C. Oikonomou, V. Lopez, D. Calero, J.A. |
description | This work presents the development of the Electrical Resistance Sintering (ERS) process for the fabrication of hard metals. The compositions of the materials produced were WC with 6 and 10 wt% of Co. In addition to the specific characteristics of the technology, the characterization of the produced parts is presented and compared to materials obtained by conventional processes. The parts produced by ERS present densities comparable to the ones obtained by conventional methods. The microstructural comparison shows a considerable grain size reduction in the ERS materials which consequently brings a hardness increase. ERS materials show similar fracture toughness to conventional ones. The very fast sintering allows performing the process without any protective atmosphere, therefore making this process very attractive for the production of materials that need to be sintered under non-oxidising environments. The total duration of the cycle, including heating, holding time and cooling is few seconds. Finally, some considerations about the scale up and possible industrialization of the technology are explained. |
doi_str_mv | 10.1016/j.ijrmhm.2017.03.005 |
format | Article |
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The compositions of the materials produced were WC with 6 and 10 wt% of Co. In addition to the specific characteristics of the technology, the characterization of the produced parts is presented and compared to materials obtained by conventional processes. The parts produced by ERS present densities comparable to the ones obtained by conventional methods. The microstructural comparison shows a considerable grain size reduction in the ERS materials which consequently brings a hardness increase. ERS materials show similar fracture toughness to conventional ones. The very fast sintering allows performing the process without any protective atmosphere, therefore making this process very attractive for the production of materials that need to be sintered under non-oxidising environments. The total duration of the cycle, including heating, holding time and cooling is few seconds. 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The compositions of the materials produced were WC with 6 and 10 wt% of Co. In addition to the specific characteristics of the technology, the characterization of the produced parts is presented and compared to materials obtained by conventional processes. The parts produced by ERS present densities comparable to the ones obtained by conventional methods. The microstructural comparison shows a considerable grain size reduction in the ERS materials which consequently brings a hardness increase. ERS materials show similar fracture toughness to conventional ones. The very fast sintering allows performing the process without any protective atmosphere, therefore making this process very attractive for the production of materials that need to be sintered under non-oxidising environments. The total duration of the cycle, including heating, holding time and cooling is few seconds. Finally, some considerations about the scale up and possible industrialization of the technology are explained.</description><subject>Cemented carbides</subject><subject>Fracture toughness</subject><subject>Mechanical properties</subject><subject>Metals</subject><subject>Microstructure</subject><subject>Resistance sintering</subject><subject>Sintering</subject><subject>Size reduction</subject><subject>Studies</subject><issn>0263-4368</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNotkM1OhDAUhVlo4vjzBi6auBW8UFrAnRl_k0l0oeumdG6lBAq2xcSH8J0tGVd3833n3JwkucwhyyHnN31mejd2Y1ZAXmVAMwB2lGyg4DQtKa9PklPvewDgDc83ye89fuMwzSPaQCZNcEAVnFHEoTc-SKuQeGMDOmM_yewmhd4TPTkSOiRatpGVwUx2lTvp9mTEIAd_S94ObNSuyWiUm3xwiwqLQyLtiqlO2igPa-qMLhj058mxjjJe_N-z5OPx4X37nO5en162d7tU0YKFVCq-r1psCtlQiRpYuS9kW7UVk6pqGS-rQqqi1hrbRqoaGNNKA61BK1YqDvQsuTrkxuqvBX0Q_bQ4GytF3jRQFxWvm0iVB2p93jvUYnZmlO5H5CDWsUUvDmOLdWwBVMSx6R92anvX</recordid><startdate>201708</startdate><enddate>201708</enddate><creator>Lagos, M.A.</creator><creator>Agote, I.</creator><creator>Schubert, T.</creator><creator>Weissgaerber, T.</creator><creator>Gallardo, J.M.</creator><creator>Montes, J.M.</creator><creator>Prakash, L.</creator><creator>Andreouli, C.</creator><creator>Oikonomou, V.</creator><creator>Lopez, D.</creator><creator>Calero, J.A.</creator><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>201708</creationdate><title>Development of electric resistance sintering process for the fabrication of hard metals: Processing, microstructure and mechanical properties</title><author>Lagos, M.A. ; Agote, I. ; Schubert, T. ; Weissgaerber, T. ; Gallardo, J.M. ; Montes, J.M. ; Prakash, L. ; Andreouli, C. ; Oikonomou, V. ; Lopez, D. ; Calero, J.A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c325t-ac6d7be92a93aef054d2ab7b75ac7b56472ac28ffeb9ac8055fcf0380fc54c603</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Cemented carbides</topic><topic>Fracture toughness</topic><topic>Mechanical properties</topic><topic>Metals</topic><topic>Microstructure</topic><topic>Resistance sintering</topic><topic>Sintering</topic><topic>Size reduction</topic><topic>Studies</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lagos, M.A.</creatorcontrib><creatorcontrib>Agote, I.</creatorcontrib><creatorcontrib>Schubert, T.</creatorcontrib><creatorcontrib>Weissgaerber, T.</creatorcontrib><creatorcontrib>Gallardo, J.M.</creatorcontrib><creatorcontrib>Montes, J.M.</creatorcontrib><creatorcontrib>Prakash, L.</creatorcontrib><creatorcontrib>Andreouli, C.</creatorcontrib><creatorcontrib>Oikonomou, V.</creatorcontrib><creatorcontrib>Lopez, D.</creatorcontrib><creatorcontrib>Calero, J.A.</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>International journal of refractory metals & hard materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lagos, M.A.</au><au>Agote, I.</au><au>Schubert, T.</au><au>Weissgaerber, T.</au><au>Gallardo, J.M.</au><au>Montes, J.M.</au><au>Prakash, L.</au><au>Andreouli, C.</au><au>Oikonomou, V.</au><au>Lopez, D.</au><au>Calero, J.A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Development of electric resistance sintering process for the fabrication of hard metals: Processing, microstructure and mechanical properties</atitle><jtitle>International journal of refractory metals & hard materials</jtitle><date>2017-08</date><risdate>2017</risdate><volume>66</volume><spage>88</spage><epage>94</epage><pages>88-94</pages><issn>0263-4368</issn><abstract>This work presents the development of the Electrical Resistance Sintering (ERS) process for the fabrication of hard metals. The compositions of the materials produced were WC with 6 and 10 wt% of Co. In addition to the specific characteristics of the technology, the characterization of the produced parts is presented and compared to materials obtained by conventional processes. The parts produced by ERS present densities comparable to the ones obtained by conventional methods. The microstructural comparison shows a considerable grain size reduction in the ERS materials which consequently brings a hardness increase. ERS materials show similar fracture toughness to conventional ones. The very fast sintering allows performing the process without any protective atmosphere, therefore making this process very attractive for the production of materials that need to be sintered under non-oxidising environments. The total duration of the cycle, including heating, holding time and cooling is few seconds. 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subjects | Cemented carbides Fracture toughness Mechanical properties Metals Microstructure Resistance sintering Sintering Size reduction Studies |
title | Development of electric resistance sintering process for the fabrication of hard metals: Processing, microstructure and mechanical properties |
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