Rapid method for accurate determination of actinides (U, Th, Pu and Am) in water samples for emergency response
To rapidly assess the contamination of actinides in emergency water, a method was developed to simultaneously analyze U, Th, Pu and Am. The method consists of two steps: extraction chromatographic separation using UTEVA and DGA resins and isotopic determination of actinides by inductively coupled pl...
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| Veröffentlicht in: | Journal of radioanalytical and nuclear chemistry 2018-01, Vol.315 (1), p.103-110 |
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| container_title | Journal of radioanalytical and nuclear chemistry |
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| creator | Wang, Zhongtang Lin, Jinxian Li, Sixuan Guo, Qiuju Huang, Wenna Wen, Wei Dan, Guiping Tan, Zhaoyi |
| description | To rapidly assess the contamination of actinides in emergency water, a method was developed to simultaneously analyze U, Th, Pu and Am. The method consists of two steps: extraction chromatographic separation using UTEVA and DGA resins and isotopic determination of actinides by inductively coupled plasma mass spectrometry (ICPMS). The whole analytical procedure takes only 8 h and high chemical recoveries of actinides were obtained. The cross spectral interferences between actinides in ICPMS measurement were sufficiently removed. The accuracy was validated by analyzing IAEA-443 seawater sample. The low limits of detection of actinides allow this method to distinguish low level contamination. |
| doi_str_mv | 10.1007/s10967-017-5640-0 |
| format | Article |
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The method consists of two steps: extraction chromatographic separation using UTEVA and DGA resins and isotopic determination of actinides by inductively coupled plasma mass spectrometry (ICPMS). The whole analytical procedure takes only 8 h and high chemical recoveries of actinides were obtained. The cross spectral interferences between actinides in ICPMS measurement were sufficiently removed. The accuracy was validated by analyzing IAEA-443 seawater sample. The low limits of detection of actinides allow this method to distinguish low level contamination.</description><identifier>ISSN: 0236-5731</identifier><identifier>EISSN: 1588-2780</identifier><identifier>DOI: 10.1007/s10967-017-5640-0</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Actinides ; Analysis ; Chemistry ; Chemistry and Materials Science ; Chromatography ; Contamination ; Diagnostic Radiology ; Emergency response ; Hadrons ; Heavy Ions ; Inductively coupled plasma mass spectrometry ; Inorganic Chemistry ; Low level ; Mass spectrometry ; Methods ; Nuclear Chemistry ; Nuclear energy ; Nuclear Physics ; Physical Chemistry ; Radiation measurement ; Safety and security measures ; Seawater</subject><ispartof>Journal of radioanalytical and nuclear chemistry, 2018-01, Vol.315 (1), p.103-110</ispartof><rights>Akadémiai Kiadó, Budapest, Hungary 2017</rights><rights>COPYRIGHT 2018 Springer</rights><rights>Copyright Springer Science & Business Media 2018</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c421t-56601f92c32bdd5f2ec7ee56dcbfed0e39b6f1f39a391941927e5127268c9ea3</citedby><cites>FETCH-LOGICAL-c421t-56601f92c32bdd5f2ec7ee56dcbfed0e39b6f1f39a391941927e5127268c9ea3</cites><orcidid>0000-0003-3153-6775</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10967-017-5640-0$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10967-017-5640-0$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Wang, Zhongtang</creatorcontrib><creatorcontrib>Lin, Jinxian</creatorcontrib><creatorcontrib>Li, Sixuan</creatorcontrib><creatorcontrib>Guo, Qiuju</creatorcontrib><creatorcontrib>Huang, Wenna</creatorcontrib><creatorcontrib>Wen, Wei</creatorcontrib><creatorcontrib>Dan, Guiping</creatorcontrib><creatorcontrib>Tan, Zhaoyi</creatorcontrib><title>Rapid method for accurate determination of actinides (U, Th, Pu and Am) in water samples for emergency response</title><title>Journal of radioanalytical and nuclear chemistry</title><addtitle>J Radioanal Nucl Chem</addtitle><description>To rapidly assess the contamination of actinides in emergency water, a method was developed to simultaneously analyze U, Th, Pu and Am. The method consists of two steps: extraction chromatographic separation using UTEVA and DGA resins and isotopic determination of actinides by inductively coupled plasma mass spectrometry (ICPMS). The whole analytical procedure takes only 8 h and high chemical recoveries of actinides were obtained. The cross spectral interferences between actinides in ICPMS measurement were sufficiently removed. The accuracy was validated by analyzing IAEA-443 seawater sample. The low limits of detection of actinides allow this method to distinguish low level contamination.</description><subject>Actinides</subject><subject>Analysis</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chromatography</subject><subject>Contamination</subject><subject>Diagnostic Radiology</subject><subject>Emergency response</subject><subject>Hadrons</subject><subject>Heavy Ions</subject><subject>Inductively coupled plasma mass spectrometry</subject><subject>Inorganic Chemistry</subject><subject>Low level</subject><subject>Mass spectrometry</subject><subject>Methods</subject><subject>Nuclear Chemistry</subject><subject>Nuclear energy</subject><subject>Nuclear Physics</subject><subject>Physical Chemistry</subject><subject>Radiation measurement</subject><subject>Safety and security measures</subject><subject>Seawater</subject><issn>0236-5731</issn><issn>1588-2780</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNp1kcFqGzEQhkVIIY7bB-hN0EsC2UQjeXelowlJUwg0BOcsZGnkKHilrbSm5O0jsz3kUuYwMPN_I838hHwHdg2M9TcFmOr6hkHftN2KNeyELKCVsuG9ZKdkwbjomrYXcEbOS3ljjCkpxYKkZzMGRwecXpOjPmVqrD1kMyF1OGEeQjRTSJEmXztTiMFhoRcvV3TzekWfDtRER9fDJQ2R_q1UpsUM475qjrNwwLzDaN9pxjKmWPAr-eLNvuC3f3lJNvd3m9uH5vH3z1-368fGrjhMdYeOgVfcCr51rvUcbY_Yds5uPTqGQm07D14oIxSoFSjeYwu85520Co1Ykh_z2DGnPwcsk35LhxzrixqUXAkpJPCqup5VO7NHHaJPUza2hsMh2BTRh1pftxxE28l6vSWBGbA5lZLR6zGHweR3DUwffdCzD7r6oI8-aFYZPjOlauMO86ev_Bf6AHk_iks</recordid><startdate>20180101</startdate><enddate>20180101</enddate><creator>Wang, Zhongtang</creator><creator>Lin, Jinxian</creator><creator>Li, Sixuan</creator><creator>Guo, Qiuju</creator><creator>Huang, Wenna</creator><creator>Wen, Wei</creator><creator>Dan, Guiping</creator><creator>Tan, Zhaoyi</creator><general>Springer Netherlands</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0003-3153-6775</orcidid></search><sort><creationdate>20180101</creationdate><title>Rapid method for accurate determination of actinides (U, Th, Pu and Am) in water samples for emergency response</title><author>Wang, Zhongtang ; Lin, Jinxian ; Li, Sixuan ; Guo, Qiuju ; Huang, Wenna ; Wen, Wei ; Dan, Guiping ; Tan, Zhaoyi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c421t-56601f92c32bdd5f2ec7ee56dcbfed0e39b6f1f39a391941927e5127268c9ea3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Actinides</topic><topic>Analysis</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chromatography</topic><topic>Contamination</topic><topic>Diagnostic Radiology</topic><topic>Emergency response</topic><topic>Hadrons</topic><topic>Heavy Ions</topic><topic>Inductively coupled plasma mass spectrometry</topic><topic>Inorganic Chemistry</topic><topic>Low level</topic><topic>Mass spectrometry</topic><topic>Methods</topic><topic>Nuclear Chemistry</topic><topic>Nuclear energy</topic><topic>Nuclear Physics</topic><topic>Physical Chemistry</topic><topic>Radiation measurement</topic><topic>Safety and security measures</topic><topic>Seawater</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wang, Zhongtang</creatorcontrib><creatorcontrib>Lin, Jinxian</creatorcontrib><creatorcontrib>Li, Sixuan</creatorcontrib><creatorcontrib>Guo, Qiuju</creatorcontrib><creatorcontrib>Huang, Wenna</creatorcontrib><creatorcontrib>Wen, Wei</creatorcontrib><creatorcontrib>Dan, Guiping</creatorcontrib><creatorcontrib>Tan, Zhaoyi</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of radioanalytical and nuclear chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wang, Zhongtang</au><au>Lin, Jinxian</au><au>Li, Sixuan</au><au>Guo, Qiuju</au><au>Huang, Wenna</au><au>Wen, Wei</au><au>Dan, Guiping</au><au>Tan, Zhaoyi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Rapid method for accurate determination of actinides (U, Th, Pu and Am) in water samples for emergency response</atitle><jtitle>Journal of radioanalytical and nuclear chemistry</jtitle><stitle>J Radioanal Nucl Chem</stitle><date>2018-01-01</date><risdate>2018</risdate><volume>315</volume><issue>1</issue><spage>103</spage><epage>110</epage><pages>103-110</pages><issn>0236-5731</issn><eissn>1588-2780</eissn><abstract>To rapidly assess the contamination of actinides in emergency water, a method was developed to simultaneously analyze U, Th, Pu and Am. The method consists of two steps: extraction chromatographic separation using UTEVA and DGA resins and isotopic determination of actinides by inductively coupled plasma mass spectrometry (ICPMS). The whole analytical procedure takes only 8 h and high chemical recoveries of actinides were obtained. The cross spectral interferences between actinides in ICPMS measurement were sufficiently removed. The accuracy was validated by analyzing IAEA-443 seawater sample. The low limits of detection of actinides allow this method to distinguish low level contamination.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s10967-017-5640-0</doi><tpages>8</tpages><orcidid>https://orcid.org/0000-0003-3153-6775</orcidid></addata></record> |
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| ispartof | Journal of radioanalytical and nuclear chemistry, 2018-01, Vol.315 (1), p.103-110 |
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| subjects | Actinides Analysis Chemistry Chemistry and Materials Science Chromatography Contamination Diagnostic Radiology Emergency response Hadrons Heavy Ions Inductively coupled plasma mass spectrometry Inorganic Chemistry Low level Mass spectrometry Methods Nuclear Chemistry Nuclear energy Nuclear Physics Physical Chemistry Radiation measurement Safety and security measures Seawater |
| title | Rapid method for accurate determination of actinides (U, Th, Pu and Am) in water samples for emergency response |
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