Investigations on the structural, optical and visible light photocatalytic activity of Cu3SnS4 prepared by mechanical alloying
Cu 3 SnS 4 has been synthesized by mechano-chemical process and the structural and optical characterizations were performed by X-ray diffraction (XRD), Raman spectroscopy, scanning electron microscope (SEM), high resolution TEM, photoluminescence (PL), UV–vis diffuse reflectance spectra (DRS) and em...
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| Veröffentlicht in: | Journal of materials science. Materials in electronics 2017-12, Vol.28 (24), p.19081-19089 |
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| container_title | Journal of materials science. Materials in electronics |
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| creator | Maheskumar, V. Gururajan, Balaji Vidhya, B. |
| description | Cu
3
SnS
4
has been synthesized by mechano-chemical process and the structural and optical characterizations were performed by X-ray diffraction (XRD), Raman spectroscopy, scanning electron microscope (SEM), high resolution TEM, photoluminescence (PL), UV–vis diffuse reflectance spectra (DRS) and emission spectroscopy. The XRD data showed that the most intense peak at 28.32° belongs to (112) plane of Cu
3
SnS
4
. The SEM and TEM confirmed the strong agglomeration of particles. The band gap value was estimated to be 1.53 eV with direct transition. The visible light photocatalytic response of Cu
3
SnS
4
was determined and 78% degradation of MB has been observed. It has been confirmed that the direct participation of holes form the major role in degradation of MB. The results indicate the potential applications of the mechano-chemically synthesized Cu
3
SnS
4
as visible light-photocatalyst. |
| doi_str_mv | 10.1007/s10854-017-7862-x |
| format | Article |
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3
SnS
4
has been synthesized by mechano-chemical process and the structural and optical characterizations were performed by X-ray diffraction (XRD), Raman spectroscopy, scanning electron microscope (SEM), high resolution TEM, photoluminescence (PL), UV–vis diffuse reflectance spectra (DRS) and emission spectroscopy. The XRD data showed that the most intense peak at 28.32° belongs to (112) plane of Cu
3
SnS
4
. The SEM and TEM confirmed the strong agglomeration of particles. The band gap value was estimated to be 1.53 eV with direct transition. The visible light photocatalytic response of Cu
3
SnS
4
was determined and 78% degradation of MB has been observed. It has been confirmed that the direct participation of holes form the major role in degradation of MB. The results indicate the potential applications of the mechano-chemically synthesized Cu
3
SnS
4
as visible light-photocatalyst.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-017-7862-x</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Catalytic activity ; Characterization and Evaluation of Materials ; Chemical synthesis ; Chemistry and Materials Science ; Degradation ; Emission spectra ; Materials Science ; Mechanical alloying ; Optical and Electronic Materials ; Organic chemistry ; Photocatalysis ; Photoluminescence ; Raman spectroscopy ; Reflectance ; Scanning electron microscopy ; Spectrum analysis ; Transmission electron microscopy ; X-ray diffraction ; X-rays</subject><ispartof>Journal of materials science. Materials in electronics, 2017-12, Vol.28 (24), p.19081-19089</ispartof><rights>Springer Science+Business Media, LLC 2017</rights><rights>Journal of Materials Science: Materials in Electronics is a copyright of Springer, (2017). All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c353t-ee7cb5411b37fcec4330479db4767d15f0c94a6053b2aee462905d461c1039593</citedby><cites>FETCH-LOGICAL-c353t-ee7cb5411b37fcec4330479db4767d15f0c94a6053b2aee462905d461c1039593</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10854-017-7862-x$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10854-017-7862-x$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Maheskumar, V.</creatorcontrib><creatorcontrib>Gururajan, Balaji</creatorcontrib><creatorcontrib>Vidhya, B.</creatorcontrib><title>Investigations on the structural, optical and visible light photocatalytic activity of Cu3SnS4 prepared by mechanical alloying</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>Cu
3
SnS
4
has been synthesized by mechano-chemical process and the structural and optical characterizations were performed by X-ray diffraction (XRD), Raman spectroscopy, scanning electron microscope (SEM), high resolution TEM, photoluminescence (PL), UV–vis diffuse reflectance spectra (DRS) and emission spectroscopy. The XRD data showed that the most intense peak at 28.32° belongs to (112) plane of Cu
3
SnS
4
. The SEM and TEM confirmed the strong agglomeration of particles. The band gap value was estimated to be 1.53 eV with direct transition. The visible light photocatalytic response of Cu
3
SnS
4
was determined and 78% degradation of MB has been observed. It has been confirmed that the direct participation of holes form the major role in degradation of MB. The results indicate the potential applications of the mechano-chemically synthesized Cu
3
SnS
4
as visible light-photocatalyst.</description><subject>Catalytic activity</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical synthesis</subject><subject>Chemistry and Materials Science</subject><subject>Degradation</subject><subject>Emission spectra</subject><subject>Materials Science</subject><subject>Mechanical alloying</subject><subject>Optical and Electronic Materials</subject><subject>Organic chemistry</subject><subject>Photocatalysis</subject><subject>Photoluminescence</subject><subject>Raman spectroscopy</subject><subject>Reflectance</subject><subject>Scanning electron microscopy</subject><subject>Spectrum analysis</subject><subject>Transmission electron microscopy</subject><subject>X-ray diffraction</subject><subject>X-rays</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNp1kDtPwzAUhS0EEuXxA9gssRLwM05GVPGoVImhILFZjuO0rlI72E7VLPx2UoWBheku3zlH9wPgBqN7jJB4iBgVnGUIi0wUOckOJ2CGuaAZK8jnKZihkouMcULOwUWMW4RQzmgxA98Ltzcx2bVK1rsIvYNpY2BModepD6q9g75LVqsWKlfDvY22ag1s7XqTYLfxyWuVVDuMCFQ62b1NA_QNnPd05VYMdsF0KpgaVgPcGb1RbupqWz9Yt74CZ41qo7n-vZfg4_npff6aLd9eFvPHZaYppykzRuiKM4wrKhptNKMUMVHWFRO5qDFvkC6ZyhGnFVHGsJyUiNcsxxojWvKSXoLbqbcL_qsfH5Zb3wc3TkpcFoSIHFM0UniidPAxBtPILtidCoPESB41y0mzHDXLo2Z5GDNkysSRdWsT_jT_G_oBx2eCbA</recordid><startdate>20171201</startdate><enddate>20171201</enddate><creator>Maheskumar, V.</creator><creator>Gururajan, Balaji</creator><creator>Vidhya, B.</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F28</scope><scope>FR3</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L7M</scope><scope>P5Z</scope><scope>P62</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>S0W</scope></search><sort><creationdate>20171201</creationdate><title>Investigations on the structural, optical and visible light photocatalytic activity of Cu3SnS4 prepared by mechanical alloying</title><author>Maheskumar, V. ; Gururajan, Balaji ; Vidhya, B.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c353t-ee7cb5411b37fcec4330479db4767d15f0c94a6053b2aee462905d461c1039593</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Catalytic activity</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical synthesis</topic><topic>Chemistry and Materials Science</topic><topic>Degradation</topic><topic>Emission spectra</topic><topic>Materials Science</topic><topic>Mechanical alloying</topic><topic>Optical and Electronic Materials</topic><topic>Organic chemistry</topic><topic>Photocatalysis</topic><topic>Photoluminescence</topic><topic>Raman spectroscopy</topic><topic>Reflectance</topic><topic>Scanning electron microscopy</topic><topic>Spectrum analysis</topic><topic>Transmission electron microscopy</topic><topic>X-ray diffraction</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Maheskumar, V.</creatorcontrib><creatorcontrib>Gururajan, Balaji</creatorcontrib><creatorcontrib>Vidhya, B.</creatorcontrib><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>Advanced Technologies & Aerospace Collection</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DELNET Engineering & Technology Collection</collection><jtitle>Journal of materials science. Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Maheskumar, V.</au><au>Gururajan, Balaji</au><au>Vidhya, B.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Investigations on the structural, optical and visible light photocatalytic activity of Cu3SnS4 prepared by mechanical alloying</atitle><jtitle>Journal of materials science. Materials in electronics</jtitle><stitle>J Mater Sci: Mater Electron</stitle><date>2017-12-01</date><risdate>2017</risdate><volume>28</volume><issue>24</issue><spage>19081</spage><epage>19089</epage><pages>19081-19089</pages><issn>0957-4522</issn><eissn>1573-482X</eissn><abstract>Cu
3
SnS
4
has been synthesized by mechano-chemical process and the structural and optical characterizations were performed by X-ray diffraction (XRD), Raman spectroscopy, scanning electron microscope (SEM), high resolution TEM, photoluminescence (PL), UV–vis diffuse reflectance spectra (DRS) and emission spectroscopy. The XRD data showed that the most intense peak at 28.32° belongs to (112) plane of Cu
3
SnS
4
. The SEM and TEM confirmed the strong agglomeration of particles. The band gap value was estimated to be 1.53 eV with direct transition. The visible light photocatalytic response of Cu
3
SnS
4
was determined and 78% degradation of MB has been observed. It has been confirmed that the direct participation of holes form the major role in degradation of MB. The results indicate the potential applications of the mechano-chemically synthesized Cu
3
SnS
4
as visible light-photocatalyst.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-017-7862-x</doi><tpages>9</tpages></addata></record> |
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| subjects | Catalytic activity Characterization and Evaluation of Materials Chemical synthesis Chemistry and Materials Science Degradation Emission spectra Materials Science Mechanical alloying Optical and Electronic Materials Organic chemistry Photocatalysis Photoluminescence Raman spectroscopy Reflectance Scanning electron microscopy Spectrum analysis Transmission electron microscopy X-ray diffraction X-rays |
| title | Investigations on the structural, optical and visible light photocatalytic activity of Cu3SnS4 prepared by mechanical alloying |
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