Photoluminescence and photocatalytic properties of Ag/AgCl synthesized by sonochemistry: statistical experimental design
Silver chloride (AgCl) particles were produced by sonochemistry synthesis. The effect of the variables such as the time of synthesis, amount of surfactant and reagent in the photocatalytic property of AgCl have were all investigated. AgCl particles became well known for their high photocatalytic act...
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| Veröffentlicht in: | Journal of materials science. Materials in electronics 2017-08, Vol.28 (16), p.12273-12281 |
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| creator | Neto, N. F. Andrade Garcia, L. M. P. Longo, E. Li, M. S. Paskocimas, C. A. Bomio, M. R. D. Motta, F. V. |
| description | Silver chloride (AgCl) particles were produced by sonochemistry synthesis. The effect of the variables such as the time of synthesis, amount of surfactant and reagent in the photocatalytic property of AgCl have were all investigated. AgCl particles became well known for their high photocatalytic activity and their plasmonic properties because of the metallic silver on their surface. In this study, AgCl particles were prepared with sodium chloride (NaCl), polyvinylpyrrolidone and silver nitrate (AgNO
3
), using a full 2
3
factorial design and three central points, resulting in 11 experiments. The synthesis was carried out using ultrasonic tip at time intervals of 5, 20 and 35 min. It was used X-ray diffraction, scanning electron microscopy with field emission (SEM-FEG), UV–Vis degradation test and photoluminescence to characterize the particles. The experimental design not only used variables present in the photocatalytic ability of the particles, but also provided a mathematical model. The (ANOVA) analysis of variance was used to confirm this model. Thus the values predicted could be observed. It is provided a response surface that characterizes the optimization zone of the photocatalytic activity of the AgCl particles to better visualize the information about its effects. |
| doi_str_mv | 10.1007/s10854-017-7044-x |
| format | Article |
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3
), using a full 2
3
factorial design and three central points, resulting in 11 experiments. The synthesis was carried out using ultrasonic tip at time intervals of 5, 20 and 35 min. It was used X-ray diffraction, scanning electron microscopy with field emission (SEM-FEG), UV–Vis degradation test and photoluminescence to characterize the particles. The experimental design not only used variables present in the photocatalytic ability of the particles, but also provided a mathematical model. The (ANOVA) analysis of variance was used to confirm this model. Thus the values predicted could be observed. It is provided a response surface that characterizes the optimization zone of the photocatalytic activity of the AgCl particles to better visualize the information about its effects.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-017-7044-x</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Catalytic activity ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Design of experiments ; Emission analysis ; Factorial design ; Field emission microscopy ; Materials Science ; Mathematical models ; Optical and Electronic Materials ; Optimization ; Photocatalysis ; Photoluminescence ; Polyvinylpyrrolidone ; Reagents ; Response surface methodology ; Scanning electron microscopy ; Silver chloride ; Sodium chloride ; Synthesis ; Variance analysis ; X-ray diffraction</subject><ispartof>Journal of materials science. Materials in electronics, 2017-08, Vol.28 (16), p.12273-12281</ispartof><rights>Springer Science+Business Media New York 2017</rights><rights>Journal of Materials Science: Materials in Electronics is a copyright of Springer, (2017). All Rights Reserved.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c353t-6cf0b935afc41b023b5184d8520560584a1d21ceee7a9eb60ea1f90ddd13b8fe3</citedby><cites>FETCH-LOGICAL-c353t-6cf0b935afc41b023b5184d8520560584a1d21ceee7a9eb60ea1f90ddd13b8fe3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10854-017-7044-x$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10854-017-7044-x$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,777,781,27905,27906,41469,42538,51300</link.rule.ids></links><search><creatorcontrib>Neto, N. F. Andrade</creatorcontrib><creatorcontrib>Garcia, L. M. P.</creatorcontrib><creatorcontrib>Longo, E.</creatorcontrib><creatorcontrib>Li, M. S.</creatorcontrib><creatorcontrib>Paskocimas, C. A.</creatorcontrib><creatorcontrib>Bomio, M. R. D.</creatorcontrib><creatorcontrib>Motta, F. V.</creatorcontrib><title>Photoluminescence and photocatalytic properties of Ag/AgCl synthesized by sonochemistry: statistical experimental design</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>Silver chloride (AgCl) particles were produced by sonochemistry synthesis. The effect of the variables such as the time of synthesis, amount of surfactant and reagent in the photocatalytic property of AgCl have were all investigated. AgCl particles became well known for their high photocatalytic activity and their plasmonic properties because of the metallic silver on their surface. In this study, AgCl particles were prepared with sodium chloride (NaCl), polyvinylpyrrolidone and silver nitrate (AgNO
3
), using a full 2
3
factorial design and three central points, resulting in 11 experiments. The synthesis was carried out using ultrasonic tip at time intervals of 5, 20 and 35 min. It was used X-ray diffraction, scanning electron microscopy with field emission (SEM-FEG), UV–Vis degradation test and photoluminescence to characterize the particles. The experimental design not only used variables present in the photocatalytic ability of the particles, but also provided a mathematical model. The (ANOVA) analysis of variance was used to confirm this model. Thus the values predicted could be observed. It is provided a response surface that characterizes the optimization zone of the photocatalytic activity of the AgCl particles to better visualize the information about its effects.</description><subject>Catalytic activity</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Design of experiments</subject><subject>Emission analysis</subject><subject>Factorial design</subject><subject>Field emission microscopy</subject><subject>Materials Science</subject><subject>Mathematical models</subject><subject>Optical and Electronic Materials</subject><subject>Optimization</subject><subject>Photocatalysis</subject><subject>Photoluminescence</subject><subject>Polyvinylpyrrolidone</subject><subject>Reagents</subject><subject>Response surface methodology</subject><subject>Scanning electron microscopy</subject><subject>Silver chloride</subject><subject>Sodium chloride</subject><subject>Synthesis</subject><subject>Variance analysis</subject><subject>X-ray diffraction</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp1kE1LxDAQhoMouK7-AG8Bz3UnadIPb8viFwh6UPAW0nTa7dJNa5OF1l9vlnrw4mmG4X3emXkJuWZwywDSlWOQSREBS6MUhIjGE7JgMo0jkfHPU7KAXKaRkJyfkwvndgCQiDhbkPFt2_muPewbi86gNUi1LWl_nBrtdTv5xtB-6HocfIOOdhVd16t1vWmpm6zfomu-saTFRF1nO7PFfeP8MN1R57UPbWN0S3EMeLNHGwxpGZDaXpKzSrcOr37rknw83L9vnqKX18fnzfolMrGMfZSYCoo8lroyghXA40KyTJSZ5CATkJnQrOTMIGKqcywSQM2qHMqyZHGRVRgvyc3sG374OqDzatcdBhtWKpZnnKeQ52lQsVllhs65ASvVh3v1MCkG6hiwmgNWIWB1DFiNgeEz44LW1jj8cf4X-gERUIJi</recordid><startdate>20170801</startdate><enddate>20170801</enddate><creator>Neto, N. 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V.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c353t-6cf0b935afc41b023b5184d8520560584a1d21ceee7a9eb60ea1f90ddd13b8fe3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Catalytic activity</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Design of experiments</topic><topic>Emission analysis</topic><topic>Factorial design</topic><topic>Field emission microscopy</topic><topic>Materials Science</topic><topic>Mathematical models</topic><topic>Optical and Electronic Materials</topic><topic>Optimization</topic><topic>Photocatalysis</topic><topic>Photoluminescence</topic><topic>Polyvinylpyrrolidone</topic><topic>Reagents</topic><topic>Response surface methodology</topic><topic>Scanning electron microscopy</topic><topic>Silver chloride</topic><topic>Sodium chloride</topic><topic>Synthesis</topic><topic>Variance analysis</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Neto, N. F. Andrade</creatorcontrib><creatorcontrib>Garcia, L. M. P.</creatorcontrib><creatorcontrib>Longo, E.</creatorcontrib><creatorcontrib>Li, M. S.</creatorcontrib><creatorcontrib>Paskocimas, C. A.</creatorcontrib><creatorcontrib>Bomio, M. R. D.</creatorcontrib><creatorcontrib>Motta, F. 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Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Neto, N. F. Andrade</au><au>Garcia, L. M. P.</au><au>Longo, E.</au><au>Li, M. S.</au><au>Paskocimas, C. A.</au><au>Bomio, M. R. D.</au><au>Motta, F. V.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Photoluminescence and photocatalytic properties of Ag/AgCl synthesized by sonochemistry: statistical experimental design</atitle><jtitle>Journal of materials science. Materials in electronics</jtitle><stitle>J Mater Sci: Mater Electron</stitle><date>2017-08-01</date><risdate>2017</risdate><volume>28</volume><issue>16</issue><spage>12273</spage><epage>12281</epage><pages>12273-12281</pages><issn>0957-4522</issn><eissn>1573-482X</eissn><abstract>Silver chloride (AgCl) particles were produced by sonochemistry synthesis. The effect of the variables such as the time of synthesis, amount of surfactant and reagent in the photocatalytic property of AgCl have were all investigated. AgCl particles became well known for their high photocatalytic activity and their plasmonic properties because of the metallic silver on their surface. In this study, AgCl particles were prepared with sodium chloride (NaCl), polyvinylpyrrolidone and silver nitrate (AgNO
3
), using a full 2
3
factorial design and three central points, resulting in 11 experiments. The synthesis was carried out using ultrasonic tip at time intervals of 5, 20 and 35 min. It was used X-ray diffraction, scanning electron microscopy with field emission (SEM-FEG), UV–Vis degradation test and photoluminescence to characterize the particles. The experimental design not only used variables present in the photocatalytic ability of the particles, but also provided a mathematical model. The (ANOVA) analysis of variance was used to confirm this model. Thus the values predicted could be observed. It is provided a response surface that characterizes the optimization zone of the photocatalytic activity of the AgCl particles to better visualize the information about its effects.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-017-7044-x</doi><tpages>9</tpages><oa>free_for_read</oa></addata></record> |
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| subjects | Catalytic activity Characterization and Evaluation of Materials Chemistry and Materials Science Design of experiments Emission analysis Factorial design Field emission microscopy Materials Science Mathematical models Optical and Electronic Materials Optimization Photocatalysis Photoluminescence Polyvinylpyrrolidone Reagents Response surface methodology Scanning electron microscopy Silver chloride Sodium chloride Synthesis Variance analysis X-ray diffraction |
| title | Photoluminescence and photocatalytic properties of Ag/AgCl synthesized by sonochemistry: statistical experimental design |
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