Preparation and properties of methylcellulose/nanocellulose/??F^sub 2^:?? polymer-inorganic composite films for two-micron radiation visualizers
The series of polymer-inorganic composite films, containing methylcellulose with incorporated cellulose nanocrystals, and synthesized fluorite-type Ca1-xHoxF2+x nanoparticles or thermally treated particle Ca1-xHoxF2+x, were prepared by mixing aqueous dispersions of the aforementioned ingredients fol...
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| Veröffentlicht in: | Journal of fluorine chemistry 2017-10, Vol.202, p.9 |
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| creator | Fedorov, PP Luginina, AA Kuznetsov, SV Voronov, VV Lyapin, AA Ryabochkina, PA Chernov, MV Mayakova, MN Pominova, DV Uvarov, OV Baranchikov, AE Ivanov, VK Pynenkov, AA Nishchev, KN |
| description | The series of polymer-inorganic composite films, containing methylcellulose with incorporated cellulose nanocrystals, and synthesized fluorite-type Ca1-xHoxF2+x nanoparticles or thermally treated particle Ca1-xHoxF2+x, were prepared by mixing aqueous dispersions of the aforementioned ingredients followed by film formation on polystyrene support and drying under air at room temperature and then at 85 °C. Fluorite-type Ca1-xHoxF2+x samples and corresponding films were characterized by X-ray diffraction (XRD), differential scanning calorimetry (DSC), thermogravimetry analysis (TGA), dynamic light scattering (DLS), scanning (SEM) and transmission (TEM) electron microscopy. For the first time, the up-conversion luminescence of the Ho3+-containing composite films (5I7 energy level excitation) has been described for the visible spectrum range. The present paper also proposes a method for visualizing the near infrared (IR) laser radiation with the use of the prepared methylcellulose/nanocellulose/Ca1-xHoxF2+x composite films as well as discussion of the optimal compositions for the said films. |
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Fluorite-type Ca1-xHoxF2+x samples and corresponding films were characterized by X-ray diffraction (XRD), differential scanning calorimetry (DSC), thermogravimetry analysis (TGA), dynamic light scattering (DLS), scanning (SEM) and transmission (TEM) electron microscopy. For the first time, the up-conversion luminescence of the Ho3+-containing composite films (5I7 energy level excitation) has been described for the visible spectrum range. The present paper also proposes a method for visualizing the near infrared (IR) laser radiation with the use of the prepared methylcellulose/nanocellulose/Ca1-xHoxF2+x composite films as well as discussion of the optimal compositions for the said films.</description><identifier>ISSN: 0022-1139</identifier><identifier>EISSN: 1873-3328</identifier><language>eng</language><publisher>Lausanne: Elsevier BV</publisher><subject>Air temperature ; Calorimetry ; Cellulose ; Chemical synthesis ; Composite materials ; Differential scanning calorimetry ; Dispersions ; Drying ; Electron microscopy ; Energy levels ; Fluorite ; Holmium ; I.R. radiation ; Infrared lasers ; Laser radiation ; Light diffraction ; Light scattering ; Methylcellulose ; Nanocomposites ; Nanocrystals ; Nanoparticles ; Near infrared radiation ; Photon correlation spectroscopy ; Polymer films ; Polymers ; Polystyrene ; Polystyrene resins ; Thermal analysis ; Thermogravimetric analysis ; Thermogravimetry ; Upconversion ; Visible spectrum ; X-ray diffraction</subject><ispartof>Journal of fluorine chemistry, 2017-10, Vol.202, p.9</ispartof><rights>Copyright Elsevier BV Oct 2017</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,777,781</link.rule.ids></links><search><creatorcontrib>Fedorov, PP</creatorcontrib><creatorcontrib>Luginina, AA</creatorcontrib><creatorcontrib>Kuznetsov, SV</creatorcontrib><creatorcontrib>Voronov, VV</creatorcontrib><creatorcontrib>Lyapin, AA</creatorcontrib><creatorcontrib>Ryabochkina, PA</creatorcontrib><creatorcontrib>Chernov, MV</creatorcontrib><creatorcontrib>Mayakova, MN</creatorcontrib><creatorcontrib>Pominova, DV</creatorcontrib><creatorcontrib>Uvarov, OV</creatorcontrib><creatorcontrib>Baranchikov, AE</creatorcontrib><creatorcontrib>Ivanov, VK</creatorcontrib><creatorcontrib>Pynenkov, AA</creatorcontrib><creatorcontrib>Nishchev, KN</creatorcontrib><title>Preparation and properties of methylcellulose/nanocellulose/??F^sub 2^:?? polymer-inorganic composite films for two-micron radiation visualizers</title><title>Journal of fluorine chemistry</title><description>The series of polymer-inorganic composite films, containing methylcellulose with incorporated cellulose nanocrystals, and synthesized fluorite-type Ca1-xHoxF2+x nanoparticles or thermally treated particle Ca1-xHoxF2+x, were prepared by mixing aqueous dispersions of the aforementioned ingredients followed by film formation on polystyrene support and drying under air at room temperature and then at 85 °C. Fluorite-type Ca1-xHoxF2+x samples and corresponding films were characterized by X-ray diffraction (XRD), differential scanning calorimetry (DSC), thermogravimetry analysis (TGA), dynamic light scattering (DLS), scanning (SEM) and transmission (TEM) electron microscopy. For the first time, the up-conversion luminescence of the Ho3+-containing composite films (5I7 energy level excitation) has been described for the visible spectrum range. The present paper also proposes a method for visualizing the near infrared (IR) laser radiation with the use of the prepared methylcellulose/nanocellulose/Ca1-xHoxF2+x composite films as well as discussion of the optimal compositions for the said films.</description><subject>Air temperature</subject><subject>Calorimetry</subject><subject>Cellulose</subject><subject>Chemical synthesis</subject><subject>Composite materials</subject><subject>Differential scanning calorimetry</subject><subject>Dispersions</subject><subject>Drying</subject><subject>Electron microscopy</subject><subject>Energy levels</subject><subject>Fluorite</subject><subject>Holmium</subject><subject>I.R. radiation</subject><subject>Infrared lasers</subject><subject>Laser radiation</subject><subject>Light diffraction</subject><subject>Light scattering</subject><subject>Methylcellulose</subject><subject>Nanocomposites</subject><subject>Nanocrystals</subject><subject>Nanoparticles</subject><subject>Near infrared radiation</subject><subject>Photon correlation spectroscopy</subject><subject>Polymer films</subject><subject>Polymers</subject><subject>Polystyrene</subject><subject>Polystyrene resins</subject><subject>Thermal analysis</subject><subject>Thermogravimetric analysis</subject><subject>Thermogravimetry</subject><subject>Upconversion</subject><subject>Visible spectrum</subject><subject>X-ray diffraction</subject><issn>0022-1139</issn><issn>1873-3328</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNqNjs1KxDAUhYMoWH_eIeA6mDYybd10IQ4uXbieIXZu9Q5pbrw3Ucan8JEtKLh1dTicD75zpKq6a51xrumOVWVt05i6dv2pOhPZW2tb23aV-npkSJ59Rorax51OTAk4I4imSc-QXw9hhBBKIIHr6CP9tWFYb6Q862ZzOww6UTjMwAYj8YuPOOqR5kSCGfSEYRY9Eev8QWbGkRcd-x3-iN9Rig_4CSwX6mTyQeDyN8_V1fr-6e7BLMfeCkje7qlwXKZt3a9at3L9Tef-R30DJddZqg</recordid><startdate>20171001</startdate><enddate>20171001</enddate><creator>Fedorov, PP</creator><creator>Luginina, AA</creator><creator>Kuznetsov, SV</creator><creator>Voronov, VV</creator><creator>Lyapin, AA</creator><creator>Ryabochkina, PA</creator><creator>Chernov, MV</creator><creator>Mayakova, MN</creator><creator>Pominova, DV</creator><creator>Uvarov, OV</creator><creator>Baranchikov, AE</creator><creator>Ivanov, VK</creator><creator>Pynenkov, AA</creator><creator>Nishchev, KN</creator><general>Elsevier BV</general><scope>7QF</scope><scope>7QO</scope><scope>7QP</scope><scope>7QQ</scope><scope>7SC</scope><scope>7SE</scope><scope>7SP</scope><scope>7SR</scope><scope>7TA</scope><scope>7TB</scope><scope>7U5</scope><scope>7U7</scope><scope>8BQ</scope><scope>8FD</scope><scope>C1K</scope><scope>F28</scope><scope>FR3</scope><scope>H8D</scope><scope>H8G</scope><scope>JG9</scope><scope>JQ2</scope><scope>KR7</scope><scope>L7M</scope><scope>L~C</scope><scope>L~D</scope><scope>P64</scope></search><sort><creationdate>20171001</creationdate><title>Preparation and properties of methylcellulose/nanocellulose/??F^sub 2^:?? polymer-inorganic composite films for two-micron radiation visualizers</title><author>Fedorov, PP ; Luginina, AA ; Kuznetsov, SV ; Voronov, VV ; Lyapin, AA ; Ryabochkina, PA ; Chernov, MV ; Mayakova, MN ; Pominova, DV ; Uvarov, OV ; Baranchikov, AE ; Ivanov, VK ; Pynenkov, AA ; Nishchev, KN</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-proquest_journals_19673639483</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Air temperature</topic><topic>Calorimetry</topic><topic>Cellulose</topic><topic>Chemical synthesis</topic><topic>Composite materials</topic><topic>Differential scanning calorimetry</topic><topic>Dispersions</topic><topic>Drying</topic><topic>Electron microscopy</topic><topic>Energy levels</topic><topic>Fluorite</topic><topic>Holmium</topic><topic>I.R. radiation</topic><topic>Infrared lasers</topic><topic>Laser radiation</topic><topic>Light diffraction</topic><topic>Light scattering</topic><topic>Methylcellulose</topic><topic>Nanocomposites</topic><topic>Nanocrystals</topic><topic>Nanoparticles</topic><topic>Near infrared radiation</topic><topic>Photon correlation spectroscopy</topic><topic>Polymer films</topic><topic>Polymers</topic><topic>Polystyrene</topic><topic>Polystyrene resins</topic><topic>Thermal analysis</topic><topic>Thermogravimetric analysis</topic><topic>Thermogravimetry</topic><topic>Upconversion</topic><topic>Visible spectrum</topic><topic>X-ray diffraction</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Fedorov, PP</creatorcontrib><creatorcontrib>Luginina, AA</creatorcontrib><creatorcontrib>Kuznetsov, SV</creatorcontrib><creatorcontrib>Voronov, VV</creatorcontrib><creatorcontrib>Lyapin, AA</creatorcontrib><creatorcontrib>Ryabochkina, PA</creatorcontrib><creatorcontrib>Chernov, MV</creatorcontrib><creatorcontrib>Mayakova, MN</creatorcontrib><creatorcontrib>Pominova, DV</creatorcontrib><creatorcontrib>Uvarov, OV</creatorcontrib><creatorcontrib>Baranchikov, AE</creatorcontrib><creatorcontrib>Ivanov, VK</creatorcontrib><creatorcontrib>Pynenkov, AA</creatorcontrib><creatorcontrib>Nishchev, KN</creatorcontrib><collection>Aluminium Industry Abstracts</collection><collection>Biotechnology Research Abstracts</collection><collection>Calcium & Calcified Tissue Abstracts</collection><collection>Ceramic Abstracts</collection><collection>Computer and Information Systems Abstracts</collection><collection>Corrosion Abstracts</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Materials Business File</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Toxicology Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Aerospace Database</collection><collection>Copper Technical Reference Library</collection><collection>Materials Research Database</collection><collection>ProQuest Computer Science Collection</collection><collection>Civil Engineering Abstracts</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Computer and Information Systems Abstracts Academic</collection><collection>Computer and Information Systems Abstracts Professional</collection><collection>Biotechnology and BioEngineering Abstracts</collection><jtitle>Journal of fluorine chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Fedorov, PP</au><au>Luginina, AA</au><au>Kuznetsov, SV</au><au>Voronov, VV</au><au>Lyapin, AA</au><au>Ryabochkina, PA</au><au>Chernov, MV</au><au>Mayakova, MN</au><au>Pominova, DV</au><au>Uvarov, OV</au><au>Baranchikov, AE</au><au>Ivanov, VK</au><au>Pynenkov, AA</au><au>Nishchev, KN</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation and properties of methylcellulose/nanocellulose/??F^sub 2^:?? 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Fluorite-type Ca1-xHoxF2+x samples and corresponding films were characterized by X-ray diffraction (XRD), differential scanning calorimetry (DSC), thermogravimetry analysis (TGA), dynamic light scattering (DLS), scanning (SEM) and transmission (TEM) electron microscopy. For the first time, the up-conversion luminescence of the Ho3+-containing composite films (5I7 energy level excitation) has been described for the visible spectrum range. The present paper also proposes a method for visualizing the near infrared (IR) laser radiation with the use of the prepared methylcellulose/nanocellulose/Ca1-xHoxF2+x composite films as well as discussion of the optimal compositions for the said films.</abstract><cop>Lausanne</cop><pub>Elsevier BV</pub></addata></record> |
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| source | Elsevier ScienceDirect Journals |
| subjects | Air temperature Calorimetry Cellulose Chemical synthesis Composite materials Differential scanning calorimetry Dispersions Drying Electron microscopy Energy levels Fluorite Holmium I.R. radiation Infrared lasers Laser radiation Light diffraction Light scattering Methylcellulose Nanocomposites Nanocrystals Nanoparticles Near infrared radiation Photon correlation spectroscopy Polymer films Polymers Polystyrene Polystyrene resins Thermal analysis Thermogravimetric analysis Thermogravimetry Upconversion Visible spectrum X-ray diffraction |
| title | Preparation and properties of methylcellulose/nanocellulose/??F^sub 2^:?? polymer-inorganic composite films for two-micron radiation visualizers |
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