Transition metal complexes of a hydrazone derived from hydralazine hydrochloride and 3,5-di-tert-butylsalicylaldehyde
Mononuclear Co(III), Ni(II) and Cu(II) coordination compounds of ( E )-1-(3,5-di-tert-butyl-2-hydroxybenzylidene)-2-(phthalazin-1-yl)hydrazine ( LH ) were prepared and characterized by physicochemical and spectroscopic methods. The metal-to-ligand ratio was found to be 1:2 in [Co( L ) 2 ]Cl·2H 2 O (...
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| Veröffentlicht in: | Transition metal chemistry (Weinheim) 2018-02, Vol.43 (1), p.65-72 |
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| creator | Patil, Sunil M. Vadavi, Ramesh S. Dodamani, Suneel Kendur, Umashri Chimmalagi, Geeta Jalalpure, Sunil Frampton, Christopher S. Gudasi, Kalagouda B. |
| description | Mononuclear Co(III), Ni(II) and Cu(II) coordination compounds of (
E
)-1-(3,5-di-tert-butyl-2-hydroxybenzylidene)-2-(phthalazin-1-yl)hydrazine (
LH
) were prepared and characterized by physicochemical and spectroscopic methods. The metal-to-ligand ratio was found to be 1:2 in [Co(
L
)
2
]Cl·2H
2
O (
1
) and [Ni(
L
)
2
]·2H
2
O (
2
), while it is 1:1 in [Cu(
L
)Cl]·2CH
3
OH (
3
). The X-ray crystal structures of
LH
and complex
1
is are reported.
LH
shows monobasic behavior, coordinating through NNO donor atoms. The complexes were investigated for their antimicrobial properties. Complexes
1
and
3
show excellent antibacterial and antifungal activities, respectively. |
| doi_str_mv | 10.1007/s11243-017-0194-0 |
| format | Article |
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E
)-1-(3,5-di-tert-butyl-2-hydroxybenzylidene)-2-(phthalazin-1-yl)hydrazine (
LH
) were prepared and characterized by physicochemical and spectroscopic methods. The metal-to-ligand ratio was found to be 1:2 in [Co(
L
)
2
]Cl·2H
2
O (
1
) and [Ni(
L
)
2
]·2H
2
O (
2
), while it is 1:1 in [Cu(
L
)Cl]·2CH
3
OH (
3
). The X-ray crystal structures of
LH
and complex
1
is are reported.
LH
shows monobasic behavior, coordinating through NNO donor atoms. The complexes were investigated for their antimicrobial properties. Complexes
1
and
3
show excellent antibacterial and antifungal activities, respectively.</description><identifier>ISSN: 0340-4285</identifier><identifier>EISSN: 1572-901X</identifier><identifier>DOI: 10.1007/s11243-017-0194-0</identifier><language>eng</language><publisher>Cham: Springer International Publishing</publisher><subject>Catalysis ; Chemistry ; Chemistry and Materials Science ; Coordination compounds ; Copper ; Crystal structure ; Fungicides ; Hydrochlorides ; Inorganic Chemistry ; Nickel ; Organometallic Chemistry ; Physical Chemistry ; Transition metal compounds</subject><ispartof>Transition metal chemistry (Weinheim), 2018-02, Vol.43 (1), p.65-72</ispartof><rights>Springer International Publishing AG, part of Springer Nature 2017</rights><rights>Transition Metal Chemistry is a copyright of Springer, (2017). All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-bf0de70d0ec282866a13a3f749014ab6b8f9c25760a3011c8aa4d6dc6b03d34a3</citedby><cites>FETCH-LOGICAL-c316t-bf0de70d0ec282866a13a3f749014ab6b8f9c25760a3011c8aa4d6dc6b03d34a3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11243-017-0194-0$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11243-017-0194-0$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27923,27924,41487,42556,51318</link.rule.ids></links><search><creatorcontrib>Patil, Sunil M.</creatorcontrib><creatorcontrib>Vadavi, Ramesh S.</creatorcontrib><creatorcontrib>Dodamani, Suneel</creatorcontrib><creatorcontrib>Kendur, Umashri</creatorcontrib><creatorcontrib>Chimmalagi, Geeta</creatorcontrib><creatorcontrib>Jalalpure, Sunil</creatorcontrib><creatorcontrib>Frampton, Christopher S.</creatorcontrib><creatorcontrib>Gudasi, Kalagouda B.</creatorcontrib><title>Transition metal complexes of a hydrazone derived from hydralazine hydrochloride and 3,5-di-tert-butylsalicylaldehyde</title><title>Transition metal chemistry (Weinheim)</title><addtitle>Transit Met Chem</addtitle><description>Mononuclear Co(III), Ni(II) and Cu(II) coordination compounds of (
E
)-1-(3,5-di-tert-butyl-2-hydroxybenzylidene)-2-(phthalazin-1-yl)hydrazine (
LH
) were prepared and characterized by physicochemical and spectroscopic methods. The metal-to-ligand ratio was found to be 1:2 in [Co(
L
)
2
]Cl·2H
2
O (
1
) and [Ni(
L
)
2
]·2H
2
O (
2
), while it is 1:1 in [Cu(
L
)Cl]·2CH
3
OH (
3
). The X-ray crystal structures of
LH
and complex
1
is are reported.
LH
shows monobasic behavior, coordinating through NNO donor atoms. The complexes were investigated for their antimicrobial properties. Complexes
1
and
3
show excellent antibacterial and antifungal activities, respectively.</description><subject>Catalysis</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Coordination compounds</subject><subject>Copper</subject><subject>Crystal structure</subject><subject>Fungicides</subject><subject>Hydrochlorides</subject><subject>Inorganic Chemistry</subject><subject>Nickel</subject><subject>Organometallic Chemistry</subject><subject>Physical Chemistry</subject><subject>Transition metal compounds</subject><issn>0340-4285</issn><issn>1572-901X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><recordid>eNp1kE1LBDEMhosouH78AG8Fr1bTj5nOHEX8AsGLgreSbTvuLN3p2s6K66-3y3jw4iEkJO-TkJeQMw6XHEBfZc6Fkgy4LtEqBntkxistWAv8bZ_MQCpgSjTVITnKeQkAldBqRjYvCYfcj30c6MqPGKiNq3XwXz7T2FGki61L-B0HT51P_ad3tEtxNbUDfvdlsKujXYSYeucpDo7Ki4q5no0-jWy-GbchY-jtNmBwvqj9CTnoMGR_-puPyevd7cvNA3t6vn-8uX5iVvK6oB04r8GBt6IRTV0jlyg7rcpTCuf1vOlaKypdA0rg3DaIytXO1nOQTiqUx-R82rtO8WPj82iWcZOGctLwttZC6la3RcUnlU0x5-Q7s079CtPWcDA7d83krinump27BgojJiYX7fDu05_N_0I_UIF-6w</recordid><startdate>20180201</startdate><enddate>20180201</enddate><creator>Patil, Sunil M.</creator><creator>Vadavi, Ramesh S.</creator><creator>Dodamani, Suneel</creator><creator>Kendur, Umashri</creator><creator>Chimmalagi, Geeta</creator><creator>Jalalpure, Sunil</creator><creator>Frampton, Christopher S.</creator><creator>Gudasi, Kalagouda B.</creator><general>Springer International Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20180201</creationdate><title>Transition metal complexes of a hydrazone derived from hydralazine hydrochloride and 3,5-di-tert-butylsalicylaldehyde</title><author>Patil, Sunil M. ; Vadavi, Ramesh S. ; Dodamani, Suneel ; Kendur, Umashri ; Chimmalagi, Geeta ; Jalalpure, Sunil ; Frampton, Christopher S. ; Gudasi, Kalagouda B.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-bf0de70d0ec282866a13a3f749014ab6b8f9c25760a3011c8aa4d6dc6b03d34a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Catalysis</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Coordination compounds</topic><topic>Copper</topic><topic>Crystal structure</topic><topic>Fungicides</topic><topic>Hydrochlorides</topic><topic>Inorganic Chemistry</topic><topic>Nickel</topic><topic>Organometallic Chemistry</topic><topic>Physical Chemistry</topic><topic>Transition metal compounds</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Patil, Sunil M.</creatorcontrib><creatorcontrib>Vadavi, Ramesh S.</creatorcontrib><creatorcontrib>Dodamani, Suneel</creatorcontrib><creatorcontrib>Kendur, Umashri</creatorcontrib><creatorcontrib>Chimmalagi, Geeta</creatorcontrib><creatorcontrib>Jalalpure, Sunil</creatorcontrib><creatorcontrib>Frampton, Christopher S.</creatorcontrib><creatorcontrib>Gudasi, Kalagouda B.</creatorcontrib><collection>CrossRef</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Transition metal chemistry (Weinheim)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Patil, Sunil M.</au><au>Vadavi, Ramesh S.</au><au>Dodamani, Suneel</au><au>Kendur, Umashri</au><au>Chimmalagi, Geeta</au><au>Jalalpure, Sunil</au><au>Frampton, Christopher S.</au><au>Gudasi, Kalagouda B.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Transition metal complexes of a hydrazone derived from hydralazine hydrochloride and 3,5-di-tert-butylsalicylaldehyde</atitle><jtitle>Transition metal chemistry (Weinheim)</jtitle><stitle>Transit Met Chem</stitle><date>2018-02-01</date><risdate>2018</risdate><volume>43</volume><issue>1</issue><spage>65</spage><epage>72</epage><pages>65-72</pages><issn>0340-4285</issn><eissn>1572-901X</eissn><abstract>Mononuclear Co(III), Ni(II) and Cu(II) coordination compounds of (
E
)-1-(3,5-di-tert-butyl-2-hydroxybenzylidene)-2-(phthalazin-1-yl)hydrazine (
LH
) were prepared and characterized by physicochemical and spectroscopic methods. The metal-to-ligand ratio was found to be 1:2 in [Co(
L
)
2
]Cl·2H
2
O (
1
) and [Ni(
L
)
2
]·2H
2
O (
2
), while it is 1:1 in [Cu(
L
)Cl]·2CH
3
OH (
3
). The X-ray crystal structures of
LH
and complex
1
is are reported.
LH
shows monobasic behavior, coordinating through NNO donor atoms. The complexes were investigated for their antimicrobial properties. Complexes
1
and
3
show excellent antibacterial and antifungal activities, respectively.</abstract><cop>Cham</cop><pub>Springer International Publishing</pub><doi>10.1007/s11243-017-0194-0</doi><tpages>8</tpages></addata></record> |
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| source | SpringerLink Journals - AutoHoldings |
| subjects | Catalysis Chemistry Chemistry and Materials Science Coordination compounds Copper Crystal structure Fungicides Hydrochlorides Inorganic Chemistry Nickel Organometallic Chemistry Physical Chemistry Transition metal compounds |
| title | Transition metal complexes of a hydrazone derived from hydralazine hydrochloride and 3,5-di-tert-butylsalicylaldehyde |
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