Structural, morphological and magnetic characters of PVP coated ZnFe2O4 nanoparticles
The most stable and magnetic recoverable material XY 2 Z 4 (X = Zn, Y = Fe and Z = O) having spinel ferrite nanoparticles were synthesized by chemical co-precipitation technique using polyvinyl pyrrolidone (PVP) as the surfactant. The synthesized nanoparticles were characterized by using various cha...
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| Veröffentlicht in: | Journal of materials science. Materials in electronics 2018-02, Vol.29 (3), p.2151-2158 |
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| container_title | Journal of materials science. Materials in electronics |
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| creator | Sagayaraj, R. Aravazhi, S. Praveen, P. Chandrasekaran, G. |
| description | The most stable and magnetic recoverable material XY
2
Z
4
(X = Zn, Y = Fe and Z = O) having spinel ferrite nanoparticles were synthesized by chemical co-precipitation technique using polyvinyl pyrrolidone (PVP) as the surfactant. The synthesized nanoparticles were characterized by using various characterization techniques. The X-ray diffraction (XRD) analyses revealed that, the ZnFe
2
O
4
have normal spinel structure of phase pure polycrystalline in nature. The FT-IR analysis revealed that the two prestigious vibration bands recorded near (540–550 cm
−1
) and (455–470 cm
−1
) show the presence of tetrahedral and octahedral voids in zinc ferrite. The transmission electron microscopy (TEM) photographs showed the synthesized ZnFe
2
O
4
nanoparticles are spherical in shape and has magnetic domain structure. The vibrating sample magnetometer (VSM) spectra indicated that the prepared ZnFe
2
O
4
nanoparticles exhibited super paramagnetic behavior along with high saturation magnetization at room temperature. Such synthesis ZnFe
2
O
4
nanoparticles with sympathetic size and tunable magnetic properties are used for various promising biomedical applications. |
| doi_str_mv | 10.1007/s10854-017-8127-4 |
| format | Article |
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2
Z
4
(X = Zn, Y = Fe and Z = O) having spinel ferrite nanoparticles were synthesized by chemical co-precipitation technique using polyvinyl pyrrolidone (PVP) as the surfactant. The synthesized nanoparticles were characterized by using various characterization techniques. The X-ray diffraction (XRD) analyses revealed that, the ZnFe
2
O
4
have normal spinel structure of phase pure polycrystalline in nature. The FT-IR analysis revealed that the two prestigious vibration bands recorded near (540–550 cm
−1
) and (455–470 cm
−1
) show the presence of tetrahedral and octahedral voids in zinc ferrite. The transmission electron microscopy (TEM) photographs showed the synthesized ZnFe
2
O
4
nanoparticles are spherical in shape and has magnetic domain structure. The vibrating sample magnetometer (VSM) spectra indicated that the prepared ZnFe
2
O
4
nanoparticles exhibited super paramagnetic behavior along with high saturation magnetization at room temperature. Such synthesis ZnFe
2
O
4
nanoparticles with sympathetic size and tunable magnetic properties are used for various promising biomedical applications.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-017-8127-4</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Biomedical materials ; Characterization and Evaluation of Materials ; Chemical precipitation ; Chemical synthesis ; Chemistry and Materials Science ; Electron microscopy ; Infrared radiation ; Iron ; Magnetic properties ; Magnetic saturation ; Materials Science ; Nanoparticles ; Optical and Electronic Materials ; Spinel ; Vibration analysis ; X-ray diffraction ; Zinc ferrites</subject><ispartof>Journal of materials science. Materials in electronics, 2018-02, Vol.29 (3), p.2151-2158</ispartof><rights>The Author(s) 2017</rights><rights>Journal of Materials Science: Materials in Electronics is a copyright of Springer, (2017). All Rights Reserved.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c396t-91e19103b2d7a29ff1b07fe9a37023b9619efa23b380f6e91402b81c6c030f703</citedby><cites>FETCH-LOGICAL-c396t-91e19103b2d7a29ff1b07fe9a37023b9619efa23b380f6e91402b81c6c030f703</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10854-017-8127-4$$EPDF$$P50$$Gspringer$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10854-017-8127-4$$EHTML$$P50$$Gspringer$$Hfree_for_read</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Sagayaraj, R.</creatorcontrib><creatorcontrib>Aravazhi, S.</creatorcontrib><creatorcontrib>Praveen, P.</creatorcontrib><creatorcontrib>Chandrasekaran, G.</creatorcontrib><title>Structural, morphological and magnetic characters of PVP coated ZnFe2O4 nanoparticles</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>The most stable and magnetic recoverable material XY
2
Z
4
(X = Zn, Y = Fe and Z = O) having spinel ferrite nanoparticles were synthesized by chemical co-precipitation technique using polyvinyl pyrrolidone (PVP) as the surfactant. The synthesized nanoparticles were characterized by using various characterization techniques. The X-ray diffraction (XRD) analyses revealed that, the ZnFe
2
O
4
have normal spinel structure of phase pure polycrystalline in nature. The FT-IR analysis revealed that the two prestigious vibration bands recorded near (540–550 cm
−1
) and (455–470 cm
−1
) show the presence of tetrahedral and octahedral voids in zinc ferrite. The transmission electron microscopy (TEM) photographs showed the synthesized ZnFe
2
O
4
nanoparticles are spherical in shape and has magnetic domain structure. The vibrating sample magnetometer (VSM) spectra indicated that the prepared ZnFe
2
O
4
nanoparticles exhibited super paramagnetic behavior along with high saturation magnetization at room temperature. Such synthesis ZnFe
2
O
4
nanoparticles with sympathetic size and tunable magnetic properties are used for various promising biomedical applications.</description><subject>Biomedical materials</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical precipitation</subject><subject>Chemical synthesis</subject><subject>Chemistry and Materials Science</subject><subject>Electron microscopy</subject><subject>Infrared radiation</subject><subject>Iron</subject><subject>Magnetic properties</subject><subject>Magnetic saturation</subject><subject>Materials Science</subject><subject>Nanoparticles</subject><subject>Optical and Electronic Materials</subject><subject>Spinel</subject><subject>Vibration analysis</subject><subject>X-ray diffraction</subject><subject>Zinc ferrites</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2018</creationdate><recordtype>article</recordtype><sourceid>C6C</sourceid><sourceid>BENPR</sourceid><recordid>eNp1kE1LxDAQhoMouK7-AG8Br1ZnkrZpjrK4Kizsgq6Il5Bmk_2g29SkPfjvbakHL55mGJ73HXgIuUa4QwBxHxGKLE0ARVIgE0l6QiaYCZ6kBfs4JROQWX_MGDsnFzEeACBPeTEh69c2dKbtgq5u6dGHZucrv90bXVFdb-hRb2vb7g01Ox20aW2I1Du6el9R43VrN_Sznlu2TGmta9_o0LOVjZfkzOkq2qvfOSXr-ePb7DlZLJ9eZg-LxHCZt4lEixKBl2wjNJPOYQnCWam5AMZLmaO0TvcbL8DlVmIKrCzQ5AY4OAF8Sm7G3ib4r87GVh18F-r-pUKZcyEywLSncKRM8DEG61QT9kcdvhWCGuyp0Z7q7anBnhoybMzEnq23Nvxp_jf0AwHqcV8</recordid><startdate>20180201</startdate><enddate>20180201</enddate><creator>Sagayaraj, R.</creator><creator>Aravazhi, S.</creator><creator>Praveen, P.</creator><creator>Chandrasekaran, G.</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>C6C</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F28</scope><scope>FR3</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L7M</scope><scope>P5Z</scope><scope>P62</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>S0W</scope></search><sort><creationdate>20180201</creationdate><title>Structural, morphological and magnetic characters of PVP coated ZnFe2O4 nanoparticles</title><author>Sagayaraj, R. ; Aravazhi, S. ; Praveen, P. ; Chandrasekaran, G.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c396t-91e19103b2d7a29ff1b07fe9a37023b9619efa23b380f6e91402b81c6c030f703</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2018</creationdate><topic>Biomedical materials</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical precipitation</topic><topic>Chemical synthesis</topic><topic>Chemistry and Materials Science</topic><topic>Electron microscopy</topic><topic>Infrared radiation</topic><topic>Iron</topic><topic>Magnetic properties</topic><topic>Magnetic saturation</topic><topic>Materials Science</topic><topic>Nanoparticles</topic><topic>Optical and Electronic Materials</topic><topic>Spinel</topic><topic>Vibration analysis</topic><topic>X-ray diffraction</topic><topic>Zinc ferrites</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sagayaraj, R.</creatorcontrib><creatorcontrib>Aravazhi, S.</creatorcontrib><creatorcontrib>Praveen, P.</creatorcontrib><creatorcontrib>Chandrasekaran, G.</creatorcontrib><collection>Springer Nature OA Free Journals</collection><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>Advanced Technologies & Aerospace Collection</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DELNET Engineering & Technology Collection</collection><jtitle>Journal of materials science. Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sagayaraj, R.</au><au>Aravazhi, S.</au><au>Praveen, P.</au><au>Chandrasekaran, G.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Structural, morphological and magnetic characters of PVP coated ZnFe2O4 nanoparticles</atitle><jtitle>Journal of materials science. Materials in electronics</jtitle><stitle>J Mater Sci: Mater Electron</stitle><date>2018-02-01</date><risdate>2018</risdate><volume>29</volume><issue>3</issue><spage>2151</spage><epage>2158</epage><pages>2151-2158</pages><issn>0957-4522</issn><eissn>1573-482X</eissn><abstract>The most stable and magnetic recoverable material XY
2
Z
4
(X = Zn, Y = Fe and Z = O) having spinel ferrite nanoparticles were synthesized by chemical co-precipitation technique using polyvinyl pyrrolidone (PVP) as the surfactant. The synthesized nanoparticles were characterized by using various characterization techniques. The X-ray diffraction (XRD) analyses revealed that, the ZnFe
2
O
4
have normal spinel structure of phase pure polycrystalline in nature. The FT-IR analysis revealed that the two prestigious vibration bands recorded near (540–550 cm
−1
) and (455–470 cm
−1
) show the presence of tetrahedral and octahedral voids in zinc ferrite. The transmission electron microscopy (TEM) photographs showed the synthesized ZnFe
2
O
4
nanoparticles are spherical in shape and has magnetic domain structure. The vibrating sample magnetometer (VSM) spectra indicated that the prepared ZnFe
2
O
4
nanoparticles exhibited super paramagnetic behavior along with high saturation magnetization at room temperature. Such synthesis ZnFe
2
O
4
nanoparticles with sympathetic size and tunable magnetic properties are used for various promising biomedical applications.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-017-8127-4</doi><tpages>8</tpages><oa>free_for_read</oa></addata></record> |
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| subjects | Biomedical materials Characterization and Evaluation of Materials Chemical precipitation Chemical synthesis Chemistry and Materials Science Electron microscopy Infrared radiation Iron Magnetic properties Magnetic saturation Materials Science Nanoparticles Optical and Electronic Materials Spinel Vibration analysis X-ray diffraction Zinc ferrites |
| title | Structural, morphological and magnetic characters of PVP coated ZnFe2O4 nanoparticles |
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