Rocking curves of gold nitride species prepared by arc pulsed - physical assisted plasma vapor deposition

Gold nitride is important for potential applications, such as, to replace metallic gold in electronics, coatings, jewelry and micro-engineering. However, the experimental determination of crystalline structure is still controversial due to difficulties in the synthesis (it is difficult to obtain a s...

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Veröffentlicht in:Surface & coatings technology 2017-01, Vol.309, p.249-257
Hauptverfasser: Quintero, J.H., Mariño, A., Šiller, L., Restrepo-Parra, E., Caro-Lopera, F.J.
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container_issue
container_start_page 249
container_title Surface & coatings technology
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creator Quintero, J.H.
Mariño, A.
Šiller, L.
Restrepo-Parra, E.
Caro-Lopera, F.J.
description Gold nitride is important for potential applications, such as, to replace metallic gold in electronics, coatings, jewelry and micro-engineering. However, the experimental determination of crystalline structure is still controversial due to difficulties in the synthesis (it is difficult to obtain a sufficient amount). In this work gold nitride species are obtained at the 304 stainless steel substrates by using an arc pulsed - physical assisted plasma vapor deposition system. The pressure of nitrogen at the discharge time was varied between 3.5 at 8.0mbar to increase the amount of gold nitride species in the sample. By X-ray diffraction, changes in the texture coefficient of (111) to (200) planes are observed, and increase of the micro strain, asymmetries and widening of the rocking curves shown. By the X-ray photoemission spectroscopy, the N 1s core levels observed at binding energies of 398.1eV and 398.3eV, are attributed to formation of gold nitride species. The rocking curves of gold nitride films are modeled by using a recent theory of shape and influential curves. From this modelling, a cubic crystalline structure of the gold nitride is proposed. •Orientation of crystallographic planes in the gold diffraction pattern were changed, due to presence of gold nitride species.•A symmetries, widening and shifts of the diffraction Bragg lines were attributed to the presence of gold nitride species.•A method to separate experimental curves of AuN with Au in different proportions was obtained.
doi_str_mv 10.1016/j.surfcoat.2016.11.081
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subjects Arc deposition
Asymmetries
Austenitic stainless steels
Crystal structure
Gold
Gold nitride
Influential curves
Jewelry
Metal nitrides
Microengineering
Nitrogen
Photoelectric emission
Physical vapor deposition
Planes
Rocking curve
Stainless steel
Substrates
Widening
title Rocking curves of gold nitride species prepared by arc pulsed - physical assisted plasma vapor deposition
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