Characterization of a downer reactor for particle rounding
The gradual shift of rapid prototyping towards additive manufacturing (AM) implies higher demands on the available material. So far, most of the processes as laser beam melting (LBM) rely on polyamide as PA12. To overcome limitations and to address this lack of suitable polymer material with a fine...
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Veröffentlicht in: | Powder technology 2017-07, Vol.316, p.357-366 |
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creator | Sachs, Marius Friedle, Maximilian Schmidt, Jochen Peukert, Wolfgang Wirth, Karl-Ernst |
description | The gradual shift of rapid prototyping towards additive manufacturing (AM) implies higher demands on the available material. So far, most of the processes as laser beam melting (LBM) rely on polyamide as PA12. To overcome limitations and to address this lack of suitable polymer material with a fine particle size, Schmidt et al. [1] have established a wet-grinding process which allows the production of very fine polymer particles. Since the ground product shows a rather bad flowability, further treatment is necessary to enable the use of this material in AM. A rounding of the chiseled particles can improve the flowability [2]. This treatment changes the morphology of the particles by surface tension forces in the molten state [3]. To accomplish rounding of the polymer powder, a downer reactor in semi-industrial scale has been established and will be characterized in this article. Main topics are the powder dispersion, the inlet geometry and its influence on the gas flow behavior inside the downer. This was achieved by combining basic simulation and experimental data. Furthermore, the heat distribution and agglomeration in the gas phase were investigated as important parameters of the process. Finally, a proof of concept by rounding wet ground PBT material was successfully conducted. The product was investigated to obtain data about a change in particle size and polymeric structure.
[Display omitted]
•A reactor for the rounding of irregular formed polymer particles is presented.•An analysis of the flow pattern is conducted using CFD. The influence of the flow pattern on the rounding is discussed.•The rounding is described by viscous flow sintering. Agglomeration effects during rounding are addressed. |
doi_str_mv | 10.1016/j.powtec.2017.01.006 |
format | Article |
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[Display omitted]
•A reactor for the rounding of irregular formed polymer particles is presented.•An analysis of the flow pattern is conducted using CFD. The influence of the flow pattern on the rounding is discussed.•The rounding is described by viscous flow sintering. Agglomeration effects during rounding are addressed.</description><identifier>ISSN: 0032-5910</identifier><identifier>EISSN: 1873-328X</identifier><identifier>DOI: 10.1016/j.powtec.2017.01.006</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Additive manufacturing ; CFD ; Downer reactors ; Gas flow ; Grinding ; Heat distribution ; Laser beam melting ; Mathematical morphology ; Particle rounding ; Particle size ; Polybutylene terephthalates ; Polymers ; Powder ; Process parameters ; Rapid prototyping ; Reactors ; Rounding ; Simulation ; Studies ; Surface tension</subject><ispartof>Powder technology, 2017-07, Vol.316, p.357-366</ispartof><rights>2017 Elsevier B.V.</rights><rights>Copyright Elsevier BV Jul 1, 2017</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c371t-6933360010ddc31c190c17e65c39c69f99e8404e933b409b6cdba58ba3801ccb3</citedby><cites>FETCH-LOGICAL-c371t-6933360010ddc31c190c17e65c39c69f99e8404e933b409b6cdba58ba3801ccb3</cites><orcidid>0000-0003-3720-0383</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.powtec.2017.01.006$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,778,782,3539,27907,27908,45978</link.rule.ids></links><search><creatorcontrib>Sachs, Marius</creatorcontrib><creatorcontrib>Friedle, Maximilian</creatorcontrib><creatorcontrib>Schmidt, Jochen</creatorcontrib><creatorcontrib>Peukert, Wolfgang</creatorcontrib><creatorcontrib>Wirth, Karl-Ernst</creatorcontrib><title>Characterization of a downer reactor for particle rounding</title><title>Powder technology</title><description>The gradual shift of rapid prototyping towards additive manufacturing (AM) implies higher demands on the available material. So far, most of the processes as laser beam melting (LBM) rely on polyamide as PA12. To overcome limitations and to address this lack of suitable polymer material with a fine particle size, Schmidt et al. [1] have established a wet-grinding process which allows the production of very fine polymer particles. Since the ground product shows a rather bad flowability, further treatment is necessary to enable the use of this material in AM. A rounding of the chiseled particles can improve the flowability [2]. This treatment changes the morphology of the particles by surface tension forces in the molten state [3]. To accomplish rounding of the polymer powder, a downer reactor in semi-industrial scale has been established and will be characterized in this article. Main topics are the powder dispersion, the inlet geometry and its influence on the gas flow behavior inside the downer. This was achieved by combining basic simulation and experimental data. Furthermore, the heat distribution and agglomeration in the gas phase were investigated as important parameters of the process. Finally, a proof of concept by rounding wet ground PBT material was successfully conducted. The product was investigated to obtain data about a change in particle size and polymeric structure.
[Display omitted]
•A reactor for the rounding of irregular formed polymer particles is presented.•An analysis of the flow pattern is conducted using CFD. The influence of the flow pattern on the rounding is discussed.•The rounding is described by viscous flow sintering. Agglomeration effects during rounding are addressed.</description><subject>Additive manufacturing</subject><subject>CFD</subject><subject>Downer reactors</subject><subject>Gas flow</subject><subject>Grinding</subject><subject>Heat distribution</subject><subject>Laser beam melting</subject><subject>Mathematical morphology</subject><subject>Particle rounding</subject><subject>Particle size</subject><subject>Polybutylene terephthalates</subject><subject>Polymers</subject><subject>Powder</subject><subject>Process parameters</subject><subject>Rapid prototyping</subject><subject>Reactors</subject><subject>Rounding</subject><subject>Simulation</subject><subject>Studies</subject><subject>Surface tension</subject><issn>0032-5910</issn><issn>1873-328X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNp9kE1LxEAMhgdRcF39Bx4KnluTTr_GgyCLX7DgRcHbME1TnbJ26kzXRX-9XerZQ8ghT96QR4hzhAQBi8suGdxuZEpSwDIBTACKA7HAqpSxTKvXQ7EAkGmcK4RjcRJCBxMhERbiavVuvKGRvf0xo3V95NrIRI3b9ewjz9PI-aidajB-tLThyLtt39j-7VQctWYT-OyvL8XL3e3z6iFeP90_rm7WMckSx7hQUsoCAKFpSCKhAsKSi5ykokK1SnGVQcYTVmeg6oKa2uRVbWQFSFTLpbiYcwfvPrccRt25re-nkxpVVkKJkKcTlc0UeReC51YP3n4Y_60R9N6S7vRsSe8taUC9d7AU1_MaTx98WfY6kOWeuLGeadSNs_8H_AJchHGK</recordid><startdate>20170701</startdate><enddate>20170701</enddate><creator>Sachs, Marius</creator><creator>Friedle, Maximilian</creator><creator>Schmidt, Jochen</creator><creator>Peukert, Wolfgang</creator><creator>Wirth, Karl-Ernst</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7ST</scope><scope>8BQ</scope><scope>8FD</scope><scope>C1K</scope><scope>JG9</scope><scope>SOI</scope><orcidid>https://orcid.org/0000-0003-3720-0383</orcidid></search><sort><creationdate>20170701</creationdate><title>Characterization of a downer reactor for particle rounding</title><author>Sachs, Marius ; Friedle, Maximilian ; Schmidt, Jochen ; Peukert, Wolfgang ; Wirth, Karl-Ernst</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c371t-6933360010ddc31c190c17e65c39c69f99e8404e933b409b6cdba58ba3801ccb3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Additive manufacturing</topic><topic>CFD</topic><topic>Downer reactors</topic><topic>Gas flow</topic><topic>Grinding</topic><topic>Heat distribution</topic><topic>Laser beam melting</topic><topic>Mathematical morphology</topic><topic>Particle rounding</topic><topic>Particle size</topic><topic>Polybutylene terephthalates</topic><topic>Polymers</topic><topic>Powder</topic><topic>Process parameters</topic><topic>Rapid prototyping</topic><topic>Reactors</topic><topic>Rounding</topic><topic>Simulation</topic><topic>Studies</topic><topic>Surface tension</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Sachs, Marius</creatorcontrib><creatorcontrib>Friedle, Maximilian</creatorcontrib><creatorcontrib>Schmidt, Jochen</creatorcontrib><creatorcontrib>Peukert, Wolfgang</creatorcontrib><creatorcontrib>Wirth, Karl-Ernst</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Environment Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Environmental Sciences and Pollution Management</collection><collection>Materials Research Database</collection><collection>Environment Abstracts</collection><jtitle>Powder technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Sachs, Marius</au><au>Friedle, Maximilian</au><au>Schmidt, Jochen</au><au>Peukert, Wolfgang</au><au>Wirth, Karl-Ernst</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Characterization of a downer reactor for particle rounding</atitle><jtitle>Powder technology</jtitle><date>2017-07-01</date><risdate>2017</risdate><volume>316</volume><spage>357</spage><epage>366</epage><pages>357-366</pages><issn>0032-5910</issn><eissn>1873-328X</eissn><abstract>The gradual shift of rapid prototyping towards additive manufacturing (AM) implies higher demands on the available material. So far, most of the processes as laser beam melting (LBM) rely on polyamide as PA12. To overcome limitations and to address this lack of suitable polymer material with a fine particle size, Schmidt et al. [1] have established a wet-grinding process which allows the production of very fine polymer particles. Since the ground product shows a rather bad flowability, further treatment is necessary to enable the use of this material in AM. A rounding of the chiseled particles can improve the flowability [2]. This treatment changes the morphology of the particles by surface tension forces in the molten state [3]. To accomplish rounding of the polymer powder, a downer reactor in semi-industrial scale has been established and will be characterized in this article. Main topics are the powder dispersion, the inlet geometry and its influence on the gas flow behavior inside the downer. This was achieved by combining basic simulation and experimental data. Furthermore, the heat distribution and agglomeration in the gas phase were investigated as important parameters of the process. Finally, a proof of concept by rounding wet ground PBT material was successfully conducted. The product was investigated to obtain data about a change in particle size and polymeric structure.
[Display omitted]
•A reactor for the rounding of irregular formed polymer particles is presented.•An analysis of the flow pattern is conducted using CFD. The influence of the flow pattern on the rounding is discussed.•The rounding is described by viscous flow sintering. Agglomeration effects during rounding are addressed.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.powtec.2017.01.006</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0003-3720-0383</orcidid></addata></record> |
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subjects | Additive manufacturing CFD Downer reactors Gas flow Grinding Heat distribution Laser beam melting Mathematical morphology Particle rounding Particle size Polybutylene terephthalates Polymers Powder Process parameters Rapid prototyping Reactors Rounding Simulation Studies Surface tension |
title | Characterization of a downer reactor for particle rounding |
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