Characterization of a downer reactor for particle rounding

The gradual shift of rapid prototyping towards additive manufacturing (AM) implies higher demands on the available material. So far, most of the processes as laser beam melting (LBM) rely on polyamide as PA12. To overcome limitations and to address this lack of suitable polymer material with a fine...

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Veröffentlicht in:Powder technology 2017-07, Vol.316, p.357-366
Hauptverfasser: Sachs, Marius, Friedle, Maximilian, Schmidt, Jochen, Peukert, Wolfgang, Wirth, Karl-Ernst
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container_end_page 366
container_issue
container_start_page 357
container_title Powder technology
container_volume 316
creator Sachs, Marius
Friedle, Maximilian
Schmidt, Jochen
Peukert, Wolfgang
Wirth, Karl-Ernst
description The gradual shift of rapid prototyping towards additive manufacturing (AM) implies higher demands on the available material. So far, most of the processes as laser beam melting (LBM) rely on polyamide as PA12. To overcome limitations and to address this lack of suitable polymer material with a fine particle size, Schmidt et al. [1] have established a wet-grinding process which allows the production of very fine polymer particles. Since the ground product shows a rather bad flowability, further treatment is necessary to enable the use of this material in AM. A rounding of the chiseled particles can improve the flowability [2]. This treatment changes the morphology of the particles by surface tension forces in the molten state [3]. To accomplish rounding of the polymer powder, a downer reactor in semi-industrial scale has been established and will be characterized in this article. Main topics are the powder dispersion, the inlet geometry and its influence on the gas flow behavior inside the downer. This was achieved by combining basic simulation and experimental data. Furthermore, the heat distribution and agglomeration in the gas phase were investigated as important parameters of the process. Finally, a proof of concept by rounding wet ground PBT material was successfully conducted. The product was investigated to obtain data about a change in particle size and polymeric structure. [Display omitted] •A reactor for the rounding of irregular formed polymer particles is presented.•An analysis of the flow pattern is conducted using CFD. The influence of the flow pattern on the rounding is discussed.•The rounding is described by viscous flow sintering. Agglomeration effects during rounding are addressed.
doi_str_mv 10.1016/j.powtec.2017.01.006
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So far, most of the processes as laser beam melting (LBM) rely on polyamide as PA12. To overcome limitations and to address this lack of suitable polymer material with a fine particle size, Schmidt et al. [1] have established a wet-grinding process which allows the production of very fine polymer particles. Since the ground product shows a rather bad flowability, further treatment is necessary to enable the use of this material in AM. A rounding of the chiseled particles can improve the flowability [2]. This treatment changes the morphology of the particles by surface tension forces in the molten state [3]. To accomplish rounding of the polymer powder, a downer reactor in semi-industrial scale has been established and will be characterized in this article. Main topics are the powder dispersion, the inlet geometry and its influence on the gas flow behavior inside the downer. This was achieved by combining basic simulation and experimental data. 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subjects Additive manufacturing
CFD
Downer reactors
Gas flow
Grinding
Heat distribution
Laser beam melting
Mathematical morphology
Particle rounding
Particle size
Polybutylene terephthalates
Polymers
Powder
Process parameters
Rapid prototyping
Reactors
Rounding
Simulation
Studies
Surface tension
title Characterization of a downer reactor for particle rounding
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