Synthesis and properties of water-soluble silica nanoparticles
Methods for synthesis and optimum conditions of the formation of stable water-soluble silica nanoparticles are presented. The silica nanoparticles were synthesized by the hydrolytic polycondensation of tetraethoxysilane using two methods: under alkaline conditions (Stöber´s method) or in an acetic a...
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| Veröffentlicht in: | Russian chemical bulletin 2017-03, Vol.66 (3), p.409-417 |
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| creator | Gorbatsevich, O. B. Kholodkov, D. N. Kurkin, T. S. Malakhova, Yu. N. Strel’tsov, D. R. Buzin, A. I. Kazakova, V. V. Muzafarov, A. M. |
| description | Methods for synthesis and optimum conditions of the formation of stable water-soluble silica nanoparticles are presented. The silica nanoparticles were synthesized by the hydrolytic polycondensation of tetraethoxysilane using two methods: under alkaline conditions (Stöber´s method) or in an acetic acid medium followed by the modification by grafting triethylene oxide moieties on the particle surface. The structure of the modified silica nanoparticles was confirmed by the data of IR and NMR spectroscopy. Polydispersity was evaluated by gel permeation chromatography and dynamic light scattering. The formation and stability of Langmuir monolayers of the silica nanoparticles modified by triethylene oxide moieties were studied. |
| doi_str_mv | 10.1007/s11172-017-1748-1 |
| format | Article |
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The structure of the modified silica nanoparticles was confirmed by the data of IR and NMR spectroscopy. Polydispersity was evaluated by gel permeation chromatography and dynamic light scattering. 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| ispartof | Russian chemical bulletin, 2017-03, Vol.66 (3), p.409-417 |
| issn | 1066-5285 1573-9171 |
| language | eng |
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| source | SpringerLink Journals |
| subjects | Acetic acid Chemistry Chemistry and Materials Science Chemistry/Food Science Dynamic stability Full Articles Infrared spectroscopy Inorganic Chemistry Liquid chromatography Monolayers Nanoparticles NMR spectroscopy Organic Chemistry Photon correlation spectroscopy Polydispersity Silicon dioxide Spectroscopic analysis Synthesis Tetraethyl orthosilicate |
| title | Synthesis and properties of water-soluble silica nanoparticles |
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