Oriented-attachment growth of diamond single crystal from detonation nanodiamonds
Possibility of growth of diamond single crystals from nanodiamond particles by oriented attachment mechanism under influence of organic substances has been suggested and experimentally confirmed. It has been found that diamond single crystals ranging up to 1.5μm are formed from the 4–5nm nanodiamond...
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| Veröffentlicht in: | Diamond and related materials 2017-05, Vol.75, p.85-90 |
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| creator | Dideikin, A.T. Eidelman, E.D. Kidalov, S.V. Kirilenko, D.A. Meilakhs, A.P. Shakhov, F.M. Shvidchenko, A.V. Sokolov, V.V. Babunz, R.A. Vul, A.Ya |
| description | Possibility of growth of diamond single crystals from nanodiamond particles by oriented attachment mechanism under influence of organic substances has been suggested and experimentally confirmed.
It has been found that diamond single crystals ranging up to 1.5μm are formed from the 4–5nm nanodiamond particles at high pressures and high temperatures treatment (HPHT; P~7GPa, T~1300°C). It has been experimentally shown that the necessary condition for the formation of the diamond single crystals is an addition of substances containing CH groups into HPHT chamber.
The formation of the diamond single crystals has been confirmed by several experimental methods, including Raman scattering, scanning electron microscopy (SEM) and electron energy loss spectroscopy (EELS). Analysis of experimental results has shown that mechanism of oriented-attachment growth is responsible for formation of diamond single crystals. A model explained details of the mechanism has been suggested.
[Display omitted]
•Growth of diamond single crystal from nanoparticles of detonation nanodiamond due to oriented attachment mechanism has been observed for the first time.•Simplified scheme of oriented attachment growth of diamond single crystal from detonation nanodiamonds.•Faceted nanodiamonds assemble into microsized faceted single crystal.•SEM image of faceted diamond single crystals obtained by HPHT treatment of nanodiamonds. |
| doi_str_mv | 10.1016/j.diamond.2017.02.009 |
| format | Article |
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It has been found that diamond single crystals ranging up to 1.5μm are formed from the 4–5nm nanodiamond particles at high pressures and high temperatures treatment (HPHT; P~7GPa, T~1300°C). It has been experimentally shown that the necessary condition for the formation of the diamond single crystals is an addition of substances containing CH groups into HPHT chamber.
The formation of the diamond single crystals has been confirmed by several experimental methods, including Raman scattering, scanning electron microscopy (SEM) and electron energy loss spectroscopy (EELS). Analysis of experimental results has shown that mechanism of oriented-attachment growth is responsible for formation of diamond single crystals. A model explained details of the mechanism has been suggested.
[Display omitted]
•Growth of diamond single crystal from nanoparticles of detonation nanodiamond due to oriented attachment mechanism has been observed for the first time.•Simplified scheme of oriented attachment growth of diamond single crystal from detonation nanodiamonds.•Faceted nanodiamonds assemble into microsized faceted single crystal.•SEM image of faceted diamond single crystals obtained by HPHT treatment of nanodiamonds.</description><identifier>ISSN: 0925-9635</identifier><identifier>EISSN: 1879-0062</identifier><identifier>DOI: 10.1016/j.diamond.2017.02.009</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>Attachment ; Crystal growth ; Crystal structure ; Detonation ; Detonation nanodiamond ; Diamond single crystal ; Diamonds ; Electron energy ; Electron energy loss spectroscopy ; HPHT synthesis ; Nanostructure ; Oriented attachment growth ; Particle physics ; Raman spectra ; Research methodology ; Scanning electron microscopy ; Scattering ; Single crystals ; Spectroscopic analysis</subject><ispartof>Diamond and related materials, 2017-05, Vol.75, p.85-90</ispartof><rights>2017 Elsevier B.V.</rights><rights>Copyright Elsevier BV May 2017</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c403t-2f5456a36b30de124bb79082c1ca764f650e938f0914c5d3f0938ac3babf9bee3</citedby><cites>FETCH-LOGICAL-c403t-2f5456a36b30de124bb79082c1ca764f650e938f0914c5d3f0938ac3babf9bee3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0925963516306203$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65534</link.rule.ids></links><search><creatorcontrib>Dideikin, A.T.</creatorcontrib><creatorcontrib>Eidelman, E.D.</creatorcontrib><creatorcontrib>Kidalov, S.V.</creatorcontrib><creatorcontrib>Kirilenko, D.A.</creatorcontrib><creatorcontrib>Meilakhs, A.P.</creatorcontrib><creatorcontrib>Shakhov, F.M.</creatorcontrib><creatorcontrib>Shvidchenko, A.V.</creatorcontrib><creatorcontrib>Sokolov, V.V.</creatorcontrib><creatorcontrib>Babunz, R.A.</creatorcontrib><creatorcontrib>Vul, A.Ya</creatorcontrib><title>Oriented-attachment growth of diamond single crystal from detonation nanodiamonds</title><title>Diamond and related materials</title><description>Possibility of growth of diamond single crystals from nanodiamond particles by oriented attachment mechanism under influence of organic substances has been suggested and experimentally confirmed.
It has been found that diamond single crystals ranging up to 1.5μm are formed from the 4–5nm nanodiamond particles at high pressures and high temperatures treatment (HPHT; P~7GPa, T~1300°C). It has been experimentally shown that the necessary condition for the formation of the diamond single crystals is an addition of substances containing CH groups into HPHT chamber.
The formation of the diamond single crystals has been confirmed by several experimental methods, including Raman scattering, scanning electron microscopy (SEM) and electron energy loss spectroscopy (EELS). Analysis of experimental results has shown that mechanism of oriented-attachment growth is responsible for formation of diamond single crystals. A model explained details of the mechanism has been suggested.
[Display omitted]
•Growth of diamond single crystal from nanoparticles of detonation nanodiamond due to oriented attachment mechanism has been observed for the first time.•Simplified scheme of oriented attachment growth of diamond single crystal from detonation nanodiamonds.•Faceted nanodiamonds assemble into microsized faceted single crystal.•SEM image of faceted diamond single crystals obtained by HPHT treatment of nanodiamonds.</description><subject>Attachment</subject><subject>Crystal growth</subject><subject>Crystal structure</subject><subject>Detonation</subject><subject>Detonation nanodiamond</subject><subject>Diamond single crystal</subject><subject>Diamonds</subject><subject>Electron energy</subject><subject>Electron energy loss spectroscopy</subject><subject>HPHT synthesis</subject><subject>Nanostructure</subject><subject>Oriented attachment growth</subject><subject>Particle physics</subject><subject>Raman spectra</subject><subject>Research methodology</subject><subject>Scanning electron microscopy</subject><subject>Scattering</subject><subject>Single crystals</subject><subject>Spectroscopic analysis</subject><issn>0925-9635</issn><issn>1879-0062</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNqFkE9LAzEQxYMoWKsfQVjwvOsk2WQ3J5HiPygUQc8hm2TbLN1NTVLFb29Ke_c0M_Dem5kfQrcYKgyY3w-VcWr0k6kI4KYCUgGIMzTDbSNKAE7O0QwEYaXglF2iqxgHAExEjWfofRWcnZI1pUpJ6c2Yh2Id_E_aFL4vTsFFdNN6awsdfmNS26IPfiyMTX5SyfmpmNTkT9J4jS56tY325lTn6PP56WPxWi5XL2-Lx2Wpa6CpJD2rGVeUdxSMxaTuukZASzTWquF1zxlYQdseBK41MzQ3tFWadqrrRWctnaO7Y-4u-K-9jUkOfh-mvFJiQQk0dcNZVrGjSgcfY7C93AU3qvArMcgDPTnI0-XyQE8CkZle9j0cfTa_8O1skFFnUNoaF6xO0nj3T8IfVbp8Ow</recordid><startdate>201705</startdate><enddate>201705</enddate><creator>Dideikin, A.T.</creator><creator>Eidelman, E.D.</creator><creator>Kidalov, S.V.</creator><creator>Kirilenko, D.A.</creator><creator>Meilakhs, A.P.</creator><creator>Shakhov, F.M.</creator><creator>Shvidchenko, A.V.</creator><creator>Sokolov, V.V.</creator><creator>Babunz, R.A.</creator><creator>Vul, A.Ya</creator><general>Elsevier B.V</general><general>Elsevier BV</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>201705</creationdate><title>Oriented-attachment growth of diamond single crystal from detonation nanodiamonds</title><author>Dideikin, A.T. ; Eidelman, E.D. ; Kidalov, S.V. ; Kirilenko, D.A. ; Meilakhs, A.P. ; Shakhov, F.M. ; Shvidchenko, A.V. ; Sokolov, V.V. ; Babunz, R.A. ; Vul, A.Ya</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c403t-2f5456a36b30de124bb79082c1ca764f650e938f0914c5d3f0938ac3babf9bee3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Attachment</topic><topic>Crystal growth</topic><topic>Crystal structure</topic><topic>Detonation</topic><topic>Detonation nanodiamond</topic><topic>Diamond single crystal</topic><topic>Diamonds</topic><topic>Electron energy</topic><topic>Electron energy loss spectroscopy</topic><topic>HPHT synthesis</topic><topic>Nanostructure</topic><topic>Oriented attachment growth</topic><topic>Particle physics</topic><topic>Raman spectra</topic><topic>Research methodology</topic><topic>Scanning electron microscopy</topic><topic>Scattering</topic><topic>Single crystals</topic><topic>Spectroscopic analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Dideikin, A.T.</creatorcontrib><creatorcontrib>Eidelman, E.D.</creatorcontrib><creatorcontrib>Kidalov, S.V.</creatorcontrib><creatorcontrib>Kirilenko, D.A.</creatorcontrib><creatorcontrib>Meilakhs, A.P.</creatorcontrib><creatorcontrib>Shakhov, F.M.</creatorcontrib><creatorcontrib>Shvidchenko, A.V.</creatorcontrib><creatorcontrib>Sokolov, V.V.</creatorcontrib><creatorcontrib>Babunz, R.A.</creatorcontrib><creatorcontrib>Vul, A.Ya</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Diamond and related materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Dideikin, A.T.</au><au>Eidelman, E.D.</au><au>Kidalov, S.V.</au><au>Kirilenko, D.A.</au><au>Meilakhs, A.P.</au><au>Shakhov, F.M.</au><au>Shvidchenko, A.V.</au><au>Sokolov, V.V.</au><au>Babunz, R.A.</au><au>Vul, A.Ya</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Oriented-attachment growth of diamond single crystal from detonation nanodiamonds</atitle><jtitle>Diamond and related materials</jtitle><date>2017-05</date><risdate>2017</risdate><volume>75</volume><spage>85</spage><epage>90</epage><pages>85-90</pages><issn>0925-9635</issn><eissn>1879-0062</eissn><abstract>Possibility of growth of diamond single crystals from nanodiamond particles by oriented attachment mechanism under influence of organic substances has been suggested and experimentally confirmed.
It has been found that diamond single crystals ranging up to 1.5μm are formed from the 4–5nm nanodiamond particles at high pressures and high temperatures treatment (HPHT; P~7GPa, T~1300°C). It has been experimentally shown that the necessary condition for the formation of the diamond single crystals is an addition of substances containing CH groups into HPHT chamber.
The formation of the diamond single crystals has been confirmed by several experimental methods, including Raman scattering, scanning electron microscopy (SEM) and electron energy loss spectroscopy (EELS). Analysis of experimental results has shown that mechanism of oriented-attachment growth is responsible for formation of diamond single crystals. A model explained details of the mechanism has been suggested.
[Display omitted]
•Growth of diamond single crystal from nanoparticles of detonation nanodiamond due to oriented attachment mechanism has been observed for the first time.•Simplified scheme of oriented attachment growth of diamond single crystal from detonation nanodiamonds.•Faceted nanodiamonds assemble into microsized faceted single crystal.•SEM image of faceted diamond single crystals obtained by HPHT treatment of nanodiamonds.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.diamond.2017.02.009</doi><tpages>6</tpages></addata></record> |
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| subjects | Attachment Crystal growth Crystal structure Detonation Detonation nanodiamond Diamond single crystal Diamonds Electron energy Electron energy loss spectroscopy HPHT synthesis Nanostructure Oriented attachment growth Particle physics Raman spectra Research methodology Scanning electron microscopy Scattering Single crystals Spectroscopic analysis |
| title | Oriented-attachment growth of diamond single crystal from detonation nanodiamonds |
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