Emission Mössbauer spectroscopy of grain boundaries in ultrafine-grained W and Mo produced by severe plastic deformation

Grain boundaries in ultrafine-grained W and Mo produced by severe plastic deformation (SPD) by high-pressure torsion method have been studied by emission Mössbauer spectroscopy on 57 Co ( 57 Fe) nuclei. The evolution of the state of the grain boundaries has been studied upon heating. It has been sho...

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Veröffentlicht in:Physics of metals and metallography 2017-04, Vol.118 (4), p.354-361, Article 354
Hauptverfasser: Popov, V. V., Sergeev, A. V., Stolbovsky, A. V.
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creator Popov, V. V.
Sergeev, A. V.
Stolbovsky, A. V.
description Grain boundaries in ultrafine-grained W and Mo produced by severe plastic deformation (SPD) by high-pressure torsion method have been studied by emission Mössbauer spectroscopy on 57 Co ( 57 Fe) nuclei. The evolution of the state of the grain boundaries has been studied upon heating. It has been shown that, after SPD, the grain boundaries are in a nonequilibrium state, which is characterized by an excess free volume. Upon annealing, the state of the grain boundaries changes as it approaches the state typical of coarse-grained materials.
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subjects Alloys
Annealing
Chemistry and Materials Science
Diffusion
Emission spectroscopy
Grain boundaries
Materials Science
Metallic Materials
Molybdenum
Mossbauer spectroscopy
Phase Transformations
Plastic deformation
Spectroscopy
Structure
Torsion
Tungsten
Ultrafines
title Emission Mössbauer spectroscopy of grain boundaries in ultrafine-grained W and Mo produced by severe plastic deformation
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