Reference material for temperature calibration of differential scanning calorimeters above 1400 °C
Platinum crucible pans are widely used for differential scanning calorimetry (DSC) at temperatures above the aluminum melting point (about 660 °C) due to good signal quality, chemical inertness and easiness of cleaning. However, reference materials commonly used for the calibration of DSC equipment...
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| Veröffentlicht in: | Journal of thermal analysis and calorimetry 2017-06, Vol.128 (3), p.1547-1554 |
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| container_title | Journal of thermal analysis and calorimetry |
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| creator | Zorzi, J. E. Segadães, A. M. Perottoni, C. A. |
| description | Platinum crucible pans are widely used for differential scanning calorimetry (DSC) at temperatures above the aluminum melting point (about 660 °C) due to good signal quality, chemical inertness and easiness of cleaning. However, reference materials commonly used for the calibration of DSC equipment operating with platinum pans exhibit phase transition temperatures no higher than about 1000 °C. In this work, the solid–solid, reversible,
α
H
′
→
α
phase transition of calcio-olivine,
Ca
2
SiO
4
,
was found to produce a marked DSC peak with an onset temperature of
1453
-
2
+
1
∘
C
and a relatively small hysteresis. This compound is compatible with platinum crucibles and fulfills the requirements to be used as reference material for high-temperature calibration of differential scanning calorimeters. |
| doi_str_mv | 10.1007/s10973-016-6048-8 |
| format | Article |
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α
H
′
→
α
phase transition of calcio-olivine,
Ca
2
SiO
4
,
was found to produce a marked DSC peak with an onset temperature of
1453
-
2
+
1
∘
C
and a relatively small hysteresis. This compound is compatible with platinum crucibles and fulfills the requirements to be used as reference material for high-temperature calibration of differential scanning calorimeters.</description><identifier>ISSN: 1388-6150</identifier><identifier>EISSN: 1588-2926</identifier><identifier>DOI: 10.1007/s10973-016-6048-8</identifier><language>eng</language><publisher>Dordrecht: Springer Netherlands</publisher><subject>Aluminum ; Analytical Chemistry ; Calibration ; Calorimetry ; Chemistry ; Chemistry and Materials Science ; Crucibles ; Differential scanning calorimetry ; Heat measurement ; Inorganic Chemistry ; Measurement Science and Instrumentation ; Olivine ; Phase transitions ; Physical Chemistry ; Platinum ; Polymer Sciences ; Reference materials ; Signal quality ; Temperature</subject><ispartof>Journal of thermal analysis and calorimetry, 2017-06, Vol.128 (3), p.1547-1554</ispartof><rights>Akadémiai Kiadó, Budapest, Hungary 2016</rights><rights>COPYRIGHT 2017 Springer</rights><rights>Copyright Springer Science & Business Media 2017</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c378t-20ea454c0dbbdc0fc0b9baea39b9bfc1d7757d75a8ce9892e9638736067d42143</cites><orcidid>0000-0002-8425-845X</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10973-016-6048-8$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10973-016-6048-8$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27922,27923,41486,42555,51317</link.rule.ids></links><search><creatorcontrib>Zorzi, J. E.</creatorcontrib><creatorcontrib>Segadães, A. M.</creatorcontrib><creatorcontrib>Perottoni, C. A.</creatorcontrib><title>Reference material for temperature calibration of differential scanning calorimeters above 1400 °C</title><title>Journal of thermal analysis and calorimetry</title><addtitle>J Therm Anal Calorim</addtitle><description>Platinum crucible pans are widely used for differential scanning calorimetry (DSC) at temperatures above the aluminum melting point (about 660 °C) due to good signal quality, chemical inertness and easiness of cleaning. However, reference materials commonly used for the calibration of DSC equipment operating with platinum pans exhibit phase transition temperatures no higher than about 1000 °C. In this work, the solid–solid, reversible,
α
H
′
→
α
phase transition of calcio-olivine,
Ca
2
SiO
4
,
was found to produce a marked DSC peak with an onset temperature of
1453
-
2
+
1
∘
C
and a relatively small hysteresis. This compound is compatible with platinum crucibles and fulfills the requirements to be used as reference material for high-temperature calibration of differential scanning calorimeters.</description><subject>Aluminum</subject><subject>Analytical Chemistry</subject><subject>Calibration</subject><subject>Calorimetry</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Crucibles</subject><subject>Differential scanning calorimetry</subject><subject>Heat measurement</subject><subject>Inorganic Chemistry</subject><subject>Measurement Science and Instrumentation</subject><subject>Olivine</subject><subject>Phase transitions</subject><subject>Physical Chemistry</subject><subject>Platinum</subject><subject>Polymer Sciences</subject><subject>Reference materials</subject><subject>Signal quality</subject><subject>Temperature</subject><issn>1388-6150</issn><issn>1588-2926</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNp1kclKBDEURQtRcPwAdwWuXJS-1JBhKY0TCILDOqRSL02kO2mTtOjf-Al-g19mynKhC8niXcK594XcojgkcEIA2GkkIFhTAaEVhZZXfKPYIR3nVS1qupl1kzUlHWwXuzE-AYAQQHaK4Q4NBnQay6VKGKxalMaHMuFyhUGldcBSq4Xts7beld6UgzXfljSyUSvnrJuPkA92iTkjlqr3L1iSFuDz_fNjtl9sGbWIePAz94rHi_OH2VV1c3t5PTu7qXTDeKpqQNV2rYah7wcNRkMveoWqEXkaTQbGOjawTnGNgosaBW04ayhQNrQ1aZu94mjKXQX_vMaY5JNfB5dXSsIFb1lbU5qpk4maqwVK64xPQel8Blxa7R0am-_Pug5EV1M2xh7_MWQm4Wuaq3WM8vr-7i9LJlYHH2NAI1f5V1R4kwTk2JScmpK5KTk2JXn21JMnZtbNMfx69r-mLz7Glz8</recordid><startdate>20170601</startdate><enddate>20170601</enddate><creator>Zorzi, J. E.</creator><creator>Segadães, A. M.</creator><creator>Perottoni, C. A.</creator><general>Springer Netherlands</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope><orcidid>https://orcid.org/0000-0002-8425-845X</orcidid></search><sort><creationdate>20170601</creationdate><title>Reference material for temperature calibration of differential scanning calorimeters above 1400 °C</title><author>Zorzi, J. E. ; Segadães, A. M. ; Perottoni, C. A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c378t-20ea454c0dbbdc0fc0b9baea39b9bfc1d7757d75a8ce9892e9638736067d42143</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Aluminum</topic><topic>Analytical Chemistry</topic><topic>Calibration</topic><topic>Calorimetry</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Crucibles</topic><topic>Differential scanning calorimetry</topic><topic>Heat measurement</topic><topic>Inorganic Chemistry</topic><topic>Measurement Science and Instrumentation</topic><topic>Olivine</topic><topic>Phase transitions</topic><topic>Physical Chemistry</topic><topic>Platinum</topic><topic>Polymer Sciences</topic><topic>Reference materials</topic><topic>Signal quality</topic><topic>Temperature</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zorzi, J. E.</creatorcontrib><creatorcontrib>Segadães, A. M.</creatorcontrib><creatorcontrib>Perottoni, C. A.</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><jtitle>Journal of thermal analysis and calorimetry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zorzi, J. E.</au><au>Segadães, A. M.</au><au>Perottoni, C. A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Reference material for temperature calibration of differential scanning calorimeters above 1400 °C</atitle><jtitle>Journal of thermal analysis and calorimetry</jtitle><stitle>J Therm Anal Calorim</stitle><date>2017-06-01</date><risdate>2017</risdate><volume>128</volume><issue>3</issue><spage>1547</spage><epage>1554</epage><pages>1547-1554</pages><issn>1388-6150</issn><eissn>1588-2926</eissn><abstract>Platinum crucible pans are widely used for differential scanning calorimetry (DSC) at temperatures above the aluminum melting point (about 660 °C) due to good signal quality, chemical inertness and easiness of cleaning. However, reference materials commonly used for the calibration of DSC equipment operating with platinum pans exhibit phase transition temperatures no higher than about 1000 °C. In this work, the solid–solid, reversible,
α
H
′
→
α
phase transition of calcio-olivine,
Ca
2
SiO
4
,
was found to produce a marked DSC peak with an onset temperature of
1453
-
2
+
1
∘
C
and a relatively small hysteresis. This compound is compatible with platinum crucibles and fulfills the requirements to be used as reference material for high-temperature calibration of differential scanning calorimeters.</abstract><cop>Dordrecht</cop><pub>Springer Netherlands</pub><doi>10.1007/s10973-016-6048-8</doi><tpages>8</tpages><orcidid>https://orcid.org/0000-0002-8425-845X</orcidid></addata></record> |
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| subjects | Aluminum Analytical Chemistry Calibration Calorimetry Chemistry Chemistry and Materials Science Crucibles Differential scanning calorimetry Heat measurement Inorganic Chemistry Measurement Science and Instrumentation Olivine Phase transitions Physical Chemistry Platinum Polymer Sciences Reference materials Signal quality Temperature |
| title | Reference material for temperature calibration of differential scanning calorimeters above 1400 °C |
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