Polycrystalline silicon nitride fibers by combustion synthesis
SHS nitriding of Si in the presence of added (NН 4 ) 2 (COO) 2 ∙ H 2 O and FeCl 3 ∙ 6Н 2 О under pressure of nitrogen gas was explored by XRD and SEM. The additives were used with an intention to transpose the nitriding reaction into the gas phase and thus to allow the deposition of Si 3 N 4 from th...
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| Veröffentlicht in: | International journal of self-propagating high-temperature synthesis 2016-10, Vol.25 (4), p.224-228 |
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| container_issue | 4 |
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| container_title | International journal of self-propagating high-temperature synthesis |
| container_volume | 25 |
| creator | Barinova, T. V. Borovinskaya, I. P. Ignat’eva, T. I. Barinov, Yu. N. Shchukin, A. S. |
| description | SHS nitriding of Si in the presence of added (NН
4
)
2
(COO)
2
∙ H
2
O and FeCl
3
∙ 6Н
2
О under pressure of nitrogen gas was explored by XRD and SEM. The additives were used with an intention to transpose the nitriding reaction into the gas phase and thus to allow the deposition of Si
3
N
4
from the gas phase. Thus prepared Si
3
N
4
had a shape of polycrystalline fibers formed by 1D crystals of varied morphology and by the assemblies of nanosized crystals. Phase composition, fiber length, and shape of nanocrystals were found to depend on nitrogen pressure. Synthesized fibers can find their application in heat insulation of aircrafts, fabrication of coatings, deep purification filters, etc. |
| doi_str_mv | 10.3103/S1061386216040038 |
| format | Article |
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4
)
2
(COO)
2
∙ H
2
O and FeCl
3
∙ 6Н
2
О under pressure of nitrogen gas was explored by XRD and SEM. The additives were used with an intention to transpose the nitriding reaction into the gas phase and thus to allow the deposition of Si
3
N
4
from the gas phase. Thus prepared Si
3
N
4
had a shape of polycrystalline fibers formed by 1D crystals of varied morphology and by the assemblies of nanosized crystals. Phase composition, fiber length, and shape of nanocrystals were found to depend on nitrogen pressure. Synthesized fibers can find their application in heat insulation of aircrafts, fabrication of coatings, deep purification filters, etc.</description><identifier>ISSN: 1061-3862</identifier><identifier>EISSN: 1934-788X</identifier><identifier>DOI: 10.3103/S1061386216040038</identifier><language>eng</language><publisher>New York: Allerton Press</publisher><subject>Chemistry and Materials Science ; Combustion synthesis ; Materials Science ; Silicon nitride</subject><ispartof>International journal of self-propagating high-temperature synthesis, 2016-10, Vol.25 (4), p.224-228</ispartof><rights>Allerton Press, Inc. 2016</rights><rights>Copyright Springer Science & Business Media 2016</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-fbed054ca755e451aebe9acf096b99d0cff4cbdf9a7ce74a9980a638717aaed53</citedby><cites>FETCH-LOGICAL-c316t-fbed054ca755e451aebe9acf096b99d0cff4cbdf9a7ce74a9980a638717aaed53</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.3103/S1061386216040038$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.3103/S1061386216040038$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Barinova, T. V.</creatorcontrib><creatorcontrib>Borovinskaya, I. P.</creatorcontrib><creatorcontrib>Ignat’eva, T. I.</creatorcontrib><creatorcontrib>Barinov, Yu. N.</creatorcontrib><creatorcontrib>Shchukin, A. S.</creatorcontrib><title>Polycrystalline silicon nitride fibers by combustion synthesis</title><title>International journal of self-propagating high-temperature synthesis</title><addtitle>Int. J Self-Propag. High-Temp. Synth</addtitle><description>SHS nitriding of Si in the presence of added (NН
4
)
2
(COO)
2
∙ H
2
O and FeCl
3
∙ 6Н
2
О under pressure of nitrogen gas was explored by XRD and SEM. The additives were used with an intention to transpose the nitriding reaction into the gas phase and thus to allow the deposition of Si
3
N
4
from the gas phase. Thus prepared Si
3
N
4
had a shape of polycrystalline fibers formed by 1D crystals of varied morphology and by the assemblies of nanosized crystals. Phase composition, fiber length, and shape of nanocrystals were found to depend on nitrogen pressure. Synthesized fibers can find their application in heat insulation of aircrafts, fabrication of coatings, deep purification filters, etc.</description><subject>Chemistry and Materials Science</subject><subject>Combustion synthesis</subject><subject>Materials Science</subject><subject>Silicon nitride</subject><issn>1061-3862</issn><issn>1934-788X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><recordid>eNp1kM1LxDAQxYMouK7-Ad4KnquTps3HRZDFL1hQUMFbSdOJZum2a6Z76H9vlvUgiJeZgd97b-Axds7hUnAQVy8cJBdaFlxCCSD0AZtxI8pcaf1-mO6E8x0_ZidEK4BKKq1m7Pp56CYXJxpt14UeMwpdcEOf9WGMocXMhwYjZc2UuWHdbGkMCdLUj59IgU7Zkbcd4dnPnrO3u9vXxUO-fLp_XNwscye4HHPfYAtV6ayqKiwrbrFBY50HIxtjWnDel65pvbHKoSqtMRqsFFpxZS22lZizi33uJg5fW6SxXg3b2KeXNdcadBqFSiq-V7k4EEX09SaGtY1TzaHe1VT_qSl5ir2Hkrb_wPgr-V_TNwVdayU</recordid><startdate>20161001</startdate><enddate>20161001</enddate><creator>Barinova, T. V.</creator><creator>Borovinskaya, I. P.</creator><creator>Ignat’eva, T. I.</creator><creator>Barinov, Yu. N.</creator><creator>Shchukin, A. S.</creator><general>Allerton Press</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20161001</creationdate><title>Polycrystalline silicon nitride fibers by combustion synthesis</title><author>Barinova, T. V. ; Borovinskaya, I. P. ; Ignat’eva, T. I. ; Barinov, Yu. N. ; Shchukin, A. S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-fbed054ca755e451aebe9acf096b99d0cff4cbdf9a7ce74a9980a638717aaed53</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Chemistry and Materials Science</topic><topic>Combustion synthesis</topic><topic>Materials Science</topic><topic>Silicon nitride</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Barinova, T. V.</creatorcontrib><creatorcontrib>Borovinskaya, I. P.</creatorcontrib><creatorcontrib>Ignat’eva, T. I.</creatorcontrib><creatorcontrib>Barinov, Yu. N.</creatorcontrib><creatorcontrib>Shchukin, A. S.</creatorcontrib><collection>CrossRef</collection><jtitle>International journal of self-propagating high-temperature synthesis</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Barinova, T. V.</au><au>Borovinskaya, I. P.</au><au>Ignat’eva, T. I.</au><au>Barinov, Yu. N.</au><au>Shchukin, A. S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Polycrystalline silicon nitride fibers by combustion synthesis</atitle><jtitle>International journal of self-propagating high-temperature synthesis</jtitle><stitle>Int. J Self-Propag. High-Temp. Synth</stitle><date>2016-10-01</date><risdate>2016</risdate><volume>25</volume><issue>4</issue><spage>224</spage><epage>228</epage><pages>224-228</pages><issn>1061-3862</issn><eissn>1934-788X</eissn><abstract>SHS nitriding of Si in the presence of added (NН
4
)
2
(COO)
2
∙ H
2
O and FeCl
3
∙ 6Н
2
О under pressure of nitrogen gas was explored by XRD and SEM. The additives were used with an intention to transpose the nitriding reaction into the gas phase and thus to allow the deposition of Si
3
N
4
from the gas phase. Thus prepared Si
3
N
4
had a shape of polycrystalline fibers formed by 1D crystals of varied morphology and by the assemblies of nanosized crystals. Phase composition, fiber length, and shape of nanocrystals were found to depend on nitrogen pressure. Synthesized fibers can find their application in heat insulation of aircrafts, fabrication of coatings, deep purification filters, etc.</abstract><cop>New York</cop><pub>Allerton Press</pub><doi>10.3103/S1061386216040038</doi><tpages>5</tpages></addata></record> |
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| identifier | ISSN: 1061-3862 |
| ispartof | International journal of self-propagating high-temperature synthesis, 2016-10, Vol.25 (4), p.224-228 |
| issn | 1061-3862 1934-788X |
| language | eng |
| recordid | cdi_proquest_journals_1880818827 |
| source | Springer Nature - Complete Springer Journals |
| subjects | Chemistry and Materials Science Combustion synthesis Materials Science Silicon nitride |
| title | Polycrystalline silicon nitride fibers by combustion synthesis |
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