Metal-Assisted Laser-Induced Gas Plasma for the Direct Analysis of Powder Using Pulse CO2 Laser
Analysis of powder samples available in small quantities has been carried out using metal-assisted gas plasma by utilizing a transversely excited atmospheric (TEA) CO 2 laser. The powder was homogeneously mixed with Si grease, and the mixed powder was painted on a metal subtarget. When a TEA CO 2 la...
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| Veröffentlicht in: | Journal of applied spectroscopy 2017, Vol.83 (6), p.1061-1067 |
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| container_issue | 6 |
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| container_title | Journal of applied spectroscopy |
| container_volume | 83 |
| creator | Khumaeni, A. Lie, Z. S. Kurniawan, K. H. Kagawa, K. |
| description | Analysis of powder samples available in small quantities has been carried out using metal-assisted gas plasma by utilizing a transversely excited atmospheric (TEA) CO
2
laser. The powder was homogeneously mixed with Si grease, and the mixed powder was painted on a metal subtarget. When a TEA CO
2
laser was directly focused on the metal subtarget at atmospheric pressure of He gas, a high-temperature He gas plasma was induced. It is assumed that the powder particles were vaporized to be effectively atomized and excited in the gas plasma region. This method has been employed in the rapid analyses of elements in organic and inorganic powder samples present in small quantities. Detection of trace elements of Cr and Pb has been successfully made by using the supplement powder and loam soil, respectively. The detection limits of Pb in loam soil were approximately 20 mg/kg. |
| doi_str_mv | 10.1007/s10812-017-0408-4 |
| format | Article |
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2
laser. The powder was homogeneously mixed with Si grease, and the mixed powder was painted on a metal subtarget. When a TEA CO
2
laser was directly focused on the metal subtarget at atmospheric pressure of He gas, a high-temperature He gas plasma was induced. It is assumed that the powder particles were vaporized to be effectively atomized and excited in the gas plasma region. This method has been employed in the rapid analyses of elements in organic and inorganic powder samples present in small quantities. Detection of trace elements of Cr and Pb has been successfully made by using the supplement powder and loam soil, respectively. The detection limits of Pb in loam soil were approximately 20 mg/kg.</description><identifier>ISSN: 0021-9037</identifier><identifier>EISSN: 1573-8647</identifier><identifier>DOI: 10.1007/s10812-017-0408-4</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Analytical Chemistry ; Atmospheric pressure ; Atomic/Molecular Structure and Spectra ; Atomizing ; Carbon dioxide lasers ; Lead ; Loam soils ; Physics ; Physics and Astronomy ; Plasma ; Plasmas (physics) ; TEA lasers ; Trace elements ; VDTs ; Video display terminals</subject><ispartof>Journal of applied spectroscopy, 2017, Vol.83 (6), p.1061-1067</ispartof><rights>Springer Science+Business Media New York 2017</rights><rights>Copyright Springer Science & Business Media 2017</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-da641b1390f558f7eb2934f9c7e08ab15d12ddaca8f41031d0e09c0f17db8c923</citedby><cites>FETCH-LOGICAL-c316t-da641b1390f558f7eb2934f9c7e08ab15d12ddaca8f41031d0e09c0f17db8c923</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10812-017-0408-4$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10812-017-0408-4$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Khumaeni, A.</creatorcontrib><creatorcontrib>Lie, Z. S.</creatorcontrib><creatorcontrib>Kurniawan, K. H.</creatorcontrib><creatorcontrib>Kagawa, K.</creatorcontrib><title>Metal-Assisted Laser-Induced Gas Plasma for the Direct Analysis of Powder Using Pulse CO2 Laser</title><title>Journal of applied spectroscopy</title><addtitle>J Appl Spectrosc</addtitle><description>Analysis of powder samples available in small quantities has been carried out using metal-assisted gas plasma by utilizing a transversely excited atmospheric (TEA) CO
2
laser. The powder was homogeneously mixed with Si grease, and the mixed powder was painted on a metal subtarget. When a TEA CO
2
laser was directly focused on the metal subtarget at atmospheric pressure of He gas, a high-temperature He gas plasma was induced. It is assumed that the powder particles were vaporized to be effectively atomized and excited in the gas plasma region. This method has been employed in the rapid analyses of elements in organic and inorganic powder samples present in small quantities. Detection of trace elements of Cr and Pb has been successfully made by using the supplement powder and loam soil, respectively. The detection limits of Pb in loam soil were approximately 20 mg/kg.</description><subject>Analytical Chemistry</subject><subject>Atmospheric pressure</subject><subject>Atomic/Molecular Structure and Spectra</subject><subject>Atomizing</subject><subject>Carbon dioxide lasers</subject><subject>Lead</subject><subject>Loam soils</subject><subject>Physics</subject><subject>Physics and Astronomy</subject><subject>Plasma</subject><subject>Plasmas (physics)</subject><subject>TEA lasers</subject><subject>Trace elements</subject><subject>VDTs</subject><subject>Video display terminals</subject><issn>0021-9037</issn><issn>1573-8647</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNp1kD1PwzAQhi0EEqXwA9gsMRvunKR2xqpAqVTUDnS2HH-UVG1S7ESo_x5XYWBhOt3pfV6dHkLuER4RQDxFBImcAQoGOUiWX5ARFiJjcpKLSzIC4MhKyMQ1uYlxBwCl5DAi6t11es-mMdaxc5YudXSBLRrbm7TNdaTrvY4HTX0baPfp6HMdnOnotNH7U2Jo6-m6_bYu0E2smy1d9_vo6GzFh6pbcuV1utz9zjHZvL58zN7YcjVfzKZLZjKcdMzqSY4VZiX4opBeuIqXWe5LIxxIXWFhkVurjZY-R8jQgoPSgEdhK2lKno3Jw9B7DO1X72Kndm0f0pNRoZQgJM-lTCkcUia0MQbn1THUBx1OCkGdParBo0oe1dmjyhPDByambLN14U_zv9AP7I90Og</recordid><startdate>2017</startdate><enddate>2017</enddate><creator>Khumaeni, A.</creator><creator>Lie, Z. S.</creator><creator>Kurniawan, K. H.</creator><creator>Kagawa, K.</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>2017</creationdate><title>Metal-Assisted Laser-Induced Gas Plasma for the Direct Analysis of Powder Using Pulse CO2 Laser</title><author>Khumaeni, A. ; Lie, Z. S. ; Kurniawan, K. H. ; Kagawa, K.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-da641b1390f558f7eb2934f9c7e08ab15d12ddaca8f41031d0e09c0f17db8c923</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Analytical Chemistry</topic><topic>Atmospheric pressure</topic><topic>Atomic/Molecular Structure and Spectra</topic><topic>Atomizing</topic><topic>Carbon dioxide lasers</topic><topic>Lead</topic><topic>Loam soils</topic><topic>Physics</topic><topic>Physics and Astronomy</topic><topic>Plasma</topic><topic>Plasmas (physics)</topic><topic>TEA lasers</topic><topic>Trace elements</topic><topic>VDTs</topic><topic>Video display terminals</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Khumaeni, A.</creatorcontrib><creatorcontrib>Lie, Z. S.</creatorcontrib><creatorcontrib>Kurniawan, K. H.</creatorcontrib><creatorcontrib>Kagawa, K.</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of applied spectroscopy</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Khumaeni, A.</au><au>Lie, Z. S.</au><au>Kurniawan, K. H.</au><au>Kagawa, K.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Metal-Assisted Laser-Induced Gas Plasma for the Direct Analysis of Powder Using Pulse CO2 Laser</atitle><jtitle>Journal of applied spectroscopy</jtitle><stitle>J Appl Spectrosc</stitle><date>2017</date><risdate>2017</risdate><volume>83</volume><issue>6</issue><spage>1061</spage><epage>1067</epage><pages>1061-1067</pages><issn>0021-9037</issn><eissn>1573-8647</eissn><abstract>Analysis of powder samples available in small quantities has been carried out using metal-assisted gas plasma by utilizing a transversely excited atmospheric (TEA) CO
2
laser. The powder was homogeneously mixed with Si grease, and the mixed powder was painted on a metal subtarget. When a TEA CO
2
laser was directly focused on the metal subtarget at atmospheric pressure of He gas, a high-temperature He gas plasma was induced. It is assumed that the powder particles were vaporized to be effectively atomized and excited in the gas plasma region. This method has been employed in the rapid analyses of elements in organic and inorganic powder samples present in small quantities. Detection of trace elements of Cr and Pb has been successfully made by using the supplement powder and loam soil, respectively. The detection limits of Pb in loam soil were approximately 20 mg/kg.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10812-017-0408-4</doi><tpages>7</tpages></addata></record> |
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| subjects | Analytical Chemistry Atmospheric pressure Atomic/Molecular Structure and Spectra Atomizing Carbon dioxide lasers Lead Loam soils Physics Physics and Astronomy Plasma Plasmas (physics) TEA lasers Trace elements VDTs Video display terminals |
| title | Metal-Assisted Laser-Induced Gas Plasma for the Direct Analysis of Powder Using Pulse CO2 Laser |
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