Heat-shock properties in yttrium-oxide films synthesized from metal–ethylenediamine tetraacetic acid complex through flame-spray apparatus

Recently, a new deposition technique using a metal–ethylenediamine tetraacetic acid (EDTA) complex has been developed. In this study, the heat-shock properties of metal-oxide films synthesized from a metal–EDTA complex were investigated. Y 2 O 3 films were synthesized on stainless-steel (SUS) substr...

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Veröffentlicht in:Applied physics. A, Materials science & processing Materials science & processing, 2017-03, Vol.123 (3), p.1-7, Article 194
Hauptverfasser: Xin, D. Y., Komatsu, Keiji, Abe, Keita, Costa, Takashi, Ikeda, Yutaka, Nakamura, Atsushi, Ohshio, Shigeo, Saitoh, Hidetoshi
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container_issue 3
container_start_page 1
container_title Applied physics. A, Materials science & processing
container_volume 123
creator Xin, D. Y.
Komatsu, Keiji
Abe, Keita
Costa, Takashi
Ikeda, Yutaka
Nakamura, Atsushi
Ohshio, Shigeo
Saitoh, Hidetoshi
description Recently, a new deposition technique using a metal–ethylenediamine tetraacetic acid (EDTA) complex has been developed. In this study, the heat-shock properties of metal-oxide films synthesized from a metal–EDTA complex were investigated. Y 2 O 3 films were synthesized on stainless-steel (SUS) substrate from EDTA∙Y∙H through the combustion of H 2 –O 2 gas. A cyclic heat-shock test was conducted on the fabricated Y 2 O 3 films through exposure to the H 2 -O 2 flame. The existence of Y 2 O 3 crystals was confirmed. Surface cracks or damages were not observed in the samples after the cyclic thermal test. Although the number of cross-sectional cracks, crack lengths, and cracks per unit area was increased by the heat shock, delaminations were not observed in the Y 2 O 3 films. The results show that the prepared Y 2 O 3 films have high thermal-shock resistance and are suitable for use as thermal barrier coatings.
doi_str_mv 10.1007/s00339-017-0839-z
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Although the number of cross-sectional cracks, crack lengths, and cracks per unit area was increased by the heat shock, delaminations were not observed in the Y 2 O 3 films. 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subjects Applied physics
Characterization and Evaluation of Materials
Condensed Matter Physics
Coordination compounds
Cracks
Ethylenediamine
Ethylenediaminetetraacetic acids
Fire damage
Heat shock
Machines
Manufacturing
Materials science
Metal oxides
Nanotechnology
Optical and Electronic Materials
Oxide coatings
Physics
Physics and Astronomy
Processes
Shock resistance
Shock tests
Stainless steels
Substrates
Surface cracks
Surfaces and Interfaces
Synthesis
Thermal barrier coatings
Thermal cycling
Thermal resistance
Thin Films
Yttrium oxide
title Heat-shock properties in yttrium-oxide films synthesized from metal–ethylenediamine tetraacetic acid complex through flame-spray apparatus
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