Phase formation in the BaCO3–PbO–Fe2O3–Nb2O5 system
Features of the formation of lead-ferroniobate compounds in the x BaCO 3 –(1 – x )PbO–Fe 2 O 3 –Nb 2 O 5 system by solid-phase synthesis are investigated. For perovskite-type lead-ferroniobate solid solution, a single-phase concentration region is revealed at 1233 K. The crystalline structures of th...
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Veröffentlicht in: | Surface investigation, x-ray, synchrotron and neutron techniques x-ray, synchrotron and neutron techniques, 2017, Vol.11 (1), p.87-91 |
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container_title | Surface investigation, x-ray, synchrotron and neutron techniques |
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creator | Lupitskaya, Yu. A. Kalganov, D. A. Abdrakhmanova, K. V. |
description | Features of the formation of lead-ferroniobate compounds in the
x
BaCO
3
–(1 –
x
)PbO–Fe
2
O
3
–Nb
2
O
5
system by solid-phase synthesis are investigated. For perovskite-type lead-ferroniobate solid solution, a single-phase concentration region is revealed at 1233 K. The crystalline structures of the synthesized compounds are refined using Rietveld analysis and the
Pm
3̅
m
and
R
3
m
space groups. Ceramic samples of lead ferroniobate are studied by scanning electron microscopy. |
doi_str_mv | 10.1134/S1027451016050347 |
format | Article |
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x
BaCO
3
–(1 –
x
)PbO–Fe
2
O
3
–Nb
2
O
5
system by solid-phase synthesis are investigated. For perovskite-type lead-ferroniobate solid solution, a single-phase concentration region is revealed at 1233 K. The crystalline structures of the synthesized compounds are refined using Rietveld analysis and the
Pm
3̅
m
and
R
3
m
space groups. Ceramic samples of lead ferroniobate are studied by scanning electron microscopy.</description><identifier>ISSN: 1027-4510</identifier><identifier>EISSN: 1819-7094</identifier><identifier>DOI: 10.1134/S1027451016050347</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Chemistry and Materials Science ; Materials Science ; Niobium oxides ; Perovskites ; Solid phase synthesis ; Solid solutions ; Surfaces and Interfaces ; Thin Films</subject><ispartof>Surface investigation, x-ray, synchrotron and neutron techniques, 2017, Vol.11 (1), p.87-91</ispartof><rights>Pleiades Publishing, Ltd. 2017</rights><rights>Copyright Springer Science & Business Media 2017</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c316t-a415f01d0f271355714f02fa62f99f5cebf9428a220b5514deb58dba2b75a4683</citedby><cites>FETCH-LOGICAL-c316t-a415f01d0f271355714f02fa62f99f5cebf9428a220b5514deb58dba2b75a4683</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S1027451016050347$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S1027451016050347$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Lupitskaya, Yu. A.</creatorcontrib><creatorcontrib>Kalganov, D. A.</creatorcontrib><creatorcontrib>Abdrakhmanova, K. V.</creatorcontrib><title>Phase formation in the BaCO3–PbO–Fe2O3–Nb2O5 system</title><title>Surface investigation, x-ray, synchrotron and neutron techniques</title><addtitle>J. Synch. Investig</addtitle><description>Features of the formation of lead-ferroniobate compounds in the
x
BaCO
3
–(1 –
x
)PbO–Fe
2
O
3
–Nb
2
O
5
system by solid-phase synthesis are investigated. For perovskite-type lead-ferroniobate solid solution, a single-phase concentration region is revealed at 1233 K. The crystalline structures of the synthesized compounds are refined using Rietveld analysis and the
Pm
3̅
m
and
R
3
m
space groups. Ceramic samples of lead ferroniobate are studied by scanning electron microscopy.</description><subject>Chemistry and Materials Science</subject><subject>Materials Science</subject><subject>Niobium oxides</subject><subject>Perovskites</subject><subject>Solid phase synthesis</subject><subject>Solid solutions</subject><subject>Surfaces and Interfaces</subject><subject>Thin Films</subject><issn>1027-4510</issn><issn>1819-7094</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2017</creationdate><recordtype>article</recordtype><recordid>eNp1UM1KAzEQDqJgrT6AtwXPqzNJZrM5arFVKG5BPS9Jm9gWu1uT7aE338E39ElMrQdBvMwP388wH2PnCJeIQl49InAlCQELIBBSHbAelqhzBVoepjnB-Q4_ZicxLgFICSp6TE_mJrrMt2FlukXbZIsm6-YuuzGDSny-f0xslerQ8e_twfKKsriNnVudsiNvXqM7--l99jy8fRrc5eNqdD-4HudTgUWXG4nkAWfguUJBpFB64N4U3Gvtaeqs15KXhnOwRChnzlI5s4ZbRUYWpeizi73vOrRvGxe7etluQpNO1liWkJ7Wqkgs3LOmoY0xOF-vw2JlwrZGqHcJ1X8SShq-18TEbV5c-OX8r-gLat5m1A</recordid><startdate>2017</startdate><enddate>2017</enddate><creator>Lupitskaya, Yu. A.</creator><creator>Kalganov, D. A.</creator><creator>Abdrakhmanova, K. V.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>2017</creationdate><title>Phase formation in the BaCO3–PbO–Fe2O3–Nb2O5 system</title><author>Lupitskaya, Yu. A. ; Kalganov, D. A. ; Abdrakhmanova, K. V.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c316t-a415f01d0f271355714f02fa62f99f5cebf9428a220b5514deb58dba2b75a4683</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2017</creationdate><topic>Chemistry and Materials Science</topic><topic>Materials Science</topic><topic>Niobium oxides</topic><topic>Perovskites</topic><topic>Solid phase synthesis</topic><topic>Solid solutions</topic><topic>Surfaces and Interfaces</topic><topic>Thin Films</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lupitskaya, Yu. A.</creatorcontrib><creatorcontrib>Kalganov, D. A.</creatorcontrib><creatorcontrib>Abdrakhmanova, K. V.</creatorcontrib><collection>CrossRef</collection><jtitle>Surface investigation, x-ray, synchrotron and neutron techniques</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lupitskaya, Yu. A.</au><au>Kalganov, D. A.</au><au>Abdrakhmanova, K. V.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Phase formation in the BaCO3–PbO–Fe2O3–Nb2O5 system</atitle><jtitle>Surface investigation, x-ray, synchrotron and neutron techniques</jtitle><stitle>J. Synch. Investig</stitle><date>2017</date><risdate>2017</risdate><volume>11</volume><issue>1</issue><spage>87</spage><epage>91</epage><pages>87-91</pages><issn>1027-4510</issn><eissn>1819-7094</eissn><abstract>Features of the formation of lead-ferroniobate compounds in the
x
BaCO
3
–(1 –
x
)PbO–Fe
2
O
3
–Nb
2
O
5
system by solid-phase synthesis are investigated. For perovskite-type lead-ferroniobate solid solution, a single-phase concentration region is revealed at 1233 K. The crystalline structures of the synthesized compounds are refined using Rietveld analysis and the
Pm
3̅
m
and
R
3
m
space groups. Ceramic samples of lead ferroniobate are studied by scanning electron microscopy.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S1027451016050347</doi><tpages>5</tpages></addata></record> |
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language | eng |
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source | SpringerLink Journals |
subjects | Chemistry and Materials Science Materials Science Niobium oxides Perovskites Solid phase synthesis Solid solutions Surfaces and Interfaces Thin Films |
title | Phase formation in the BaCO3–PbO–Fe2O3–Nb2O5 system |
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