Magnetic and Structural Properties of Cobalt- and Zinc-Substituted Nickel Ferrite Synthesized by Microwave-Assisted Hydrothermal Method
Ceramic spinel-based ferrites of cobalt, nickel and zinc were prepared by means of the microwave-assisted hydrothermal method. All samples were thoroughly characterized using different techniques for their structural, compositional, phonic and magnetic properties. The Rietveld analysis of x-ray powd...
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| Veröffentlicht in: | Journal of electronic materials 2017-02, Vol.46 (2), p.1145-1154 |
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| creator | Sinfrônio, F. S. M. Santana, P. Y. C. Coelho, S. F. N. Silva, F. C. de Menezes, A. S. Sharma, S. K. |
| description | Ceramic spinel-based ferrites of cobalt, nickel and zinc were prepared by means of the microwave-assisted hydrothermal method. All samples were thoroughly characterized using different techniques for their structural, compositional, phonic and magnetic properties. The Rietveld analysis of x-ray powder diffraction data revealed the crystallinity as well single-phase partially inverse spinel structure. Wavelength dispersive x-ray fluorescence measurement indicates a good correlation between the empirical stoichiometry. The estimated average crystallite size varies between 9 nm and 13 nm (XRPD) and 6 and 14 nm for high-resolution transmission electron microscopy measurements. In addition, the observed micro-strain varies in the range of 0.01–0.6%. All samples show a quasi-spherical morphology and slight agglomeration. Infrared and Raman data spectra exhibit characteristic modes for spinel-based ferrites. Direct current magnetic measurements indicate behavior typical of magnetically soft materials system at 300 K. |
| doi_str_mv | 10.1007/s11664-016-5081-5 |
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S. M. ; Santana, P. Y. C. ; Coelho, S. F. N. ; Silva, F. C. ; de Menezes, A. S. ; Sharma, S. K.</creator><creatorcontrib>Sinfrônio, F. S. M. ; Santana, P. Y. C. ; Coelho, S. F. N. ; Silva, F. C. ; de Menezes, A. S. ; Sharma, S. K.</creatorcontrib><description>Ceramic spinel-based ferrites of cobalt, nickel and zinc were prepared by means of the microwave-assisted hydrothermal method. All samples were thoroughly characterized using different techniques for their structural, compositional, phonic and magnetic properties. The Rietveld analysis of x-ray powder diffraction data revealed the crystallinity as well single-phase partially inverse spinel structure. Wavelength dispersive x-ray fluorescence measurement indicates a good correlation between the empirical stoichiometry. The estimated average crystallite size varies between 9 nm and 13 nm (XRPD) and 6 and 14 nm for high-resolution transmission electron microscopy measurements. In addition, the observed micro-strain varies in the range of 0.01–0.6%. All samples show a quasi-spherical morphology and slight agglomeration. Infrared and Raman data spectra exhibit characteristic modes for spinel-based ferrites. 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Wavelength dispersive x-ray fluorescence measurement indicates a good correlation between the empirical stoichiometry. The estimated average crystallite size varies between 9 nm and 13 nm (XRPD) and 6 and 14 nm for high-resolution transmission electron microscopy measurements. In addition, the observed micro-strain varies in the range of 0.01–0.6%. All samples show a quasi-spherical morphology and slight agglomeration. Infrared and Raman data spectra exhibit characteristic modes for spinel-based ferrites. 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S. M.</au><au>Santana, P. Y. C.</au><au>Coelho, S. F. N.</au><au>Silva, F. C.</au><au>de Menezes, A. S.</au><au>Sharma, S. K.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Magnetic and Structural Properties of Cobalt- and Zinc-Substituted Nickel Ferrite Synthesized by Microwave-Assisted Hydrothermal Method</atitle><jtitle>Journal of electronic materials</jtitle><stitle>Journal of Elec Materi</stitle><date>2017-02-01</date><risdate>2017</risdate><volume>46</volume><issue>2</issue><spage>1145</spage><epage>1154</epage><pages>1145-1154</pages><issn>0361-5235</issn><eissn>1543-186X</eissn><coden>JECMA5</coden><abstract>Ceramic spinel-based ferrites of cobalt, nickel and zinc were prepared by means of the microwave-assisted hydrothermal method. All samples were thoroughly characterized using different techniques for their structural, compositional, phonic and magnetic properties. 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| subjects | Characterization and Evaluation of Materials Chemical synthesis Chemistry and Materials Science Electronics and Microelectronics Ferrites Instrumentation Magnetism Materials Science Microwave heating Optical and Electronic Materials Solid State Physics |
| title | Magnetic and Structural Properties of Cobalt- and Zinc-Substituted Nickel Ferrite Synthesized by Microwave-Assisted Hydrothermal Method |
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